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1. 发明授权

US08956520B2 Electrochemical process to prepare chemicals using a cyanide salt 有权
标题翻译：使用氰化物盐制备化学品的电化学工艺
公开(公告)号：US08956520B2
公开(公告)日：2015-02-17
申请号：US13322702
申请日：2010-06-03
申请人： Wilhelmus Joannes Theodorus Maria Appelman , Hans Lammers , Arie Volmer , Tjerk Oedse Boonstra , Adrianus Maria Reichwein
发明人： Wilhelmus Joannes Theodorus Maria Appelman , Hans Lammers , Arie Volmer , Tjerk Oedse Boonstra , Adrianus Maria Reichwein
IPC分类号： B01D61/44 , C07C227/18
CPC分类号： C07C227/18 , B01D61/44 , C07C229/16
摘要： The present invention relates to a process comprising the reaction of a cyanide with a hydrogen cyanide-reactive compound, characterized in that the cyanide is a cyanide salt and the process is an electrochemical process involving the transporting of a reaction mixture to which cyanide salt has been added through an electrochemical cell, in which process the cyanide salt reacts with the hydrogen cyanide-reactive compound while at least partly under the influence of an electric current the cyanide salt is acidified and the salt cation content is reduced.
摘要翻译：本发明涉及一种包括氰化物与氰化氢反应性化合物的反应的方法，其特征在于氰化物是氰化物盐，该方法是一种电化学方法，涉及运输已经将氰化物盐的反应混合物通过电化学电池添加，其中氰化物盐与氰化氢反应性化合物反应，同时至少部分地在电流的影响下，氰化物盐被酸化并且盐阳离子含量降低。

2. 发明申请

US20120132536A1 AN ELECTROCHEMICAL PROCESS TO PREPARE CHEMICALS USING A CYANIDE SALT 有权
标题翻译：使用氰化物盐制备化学品的电化学工艺
公开(公告)号：US20120132536A1
公开(公告)日：2012-05-31
申请号：US13322702
申请日：2010-06-03
申请人： Wilhelmus Joannes Theodorus Maria Appelman , Hans Lammers , Tjerk Oedse Boonstra , Adrianus Maria Reichwein
发明人： Wilhelmus Joannes Theodorus Maria Appelman , Hans Lammers , Tjerk Oedse Boonstra , Adrianus Maria Reichwein
IPC分类号： C25B1/22 , C25B13/00
CPC分类号： C07C227/18 , B01D61/44 , C07C229/16
摘要： The present invention relates to a process comprising the reaction of a cyanide with a hydrogen cyanide-reactive compound, characterized in that the cyanide is a cyanide salt and the process is an electrochemical process involving the transporting of a reaction mixture to which cyanide salt has been added through an electrochemical cell, in which process the cyanide salt reacts with the hydrogen cyanide-reactive compound while at least partly under the influence of an electric current the cyanide salt is acidified and the salt cation content is reduced.
摘要翻译：本发明涉及一种包括氰化物与氰化氢反应性化合物的反应的方法，其特征在于氰化物是氰化物盐，该方法是一种电化学方法，涉及运输已经将氰化物盐的反应混合物通过电化学电池添加，其中氰化物盐与氰化氢反应性化合物反应，同时至少部分地在电流的影响下，氰化物盐被酸化并且盐阳离子含量降低。

3. 发明授权

US09334232B2 Process to prepare a chelating agent or precursor thereof using a cyanide salt 有权
标题翻译：使用氰化物盐制备螯合剂或其前体的方法
公开(公告)号：US09334232B2
公开(公告)日：2016-05-10
申请号：US13322720
申请日：2010-06-03
申请人： Hans Lammers , Martin Heus , Tjerk Oedse Boonstra , Adrianus Maria Reichwein
发明人： Hans Lammers , Martin Heus , Tjerk Oedse Boonstra , Adrianus Maria Reichwein
IPC分类号： C07C227/18 , C07C253/30 , C07C253/08 , C07C229/24
CPC分类号： C07C253/08 , C07C229/24 , C07C255/25
摘要： The present invention relates to a process comprising the reaction of a cyanide with an amino acid and an aldehyde, characterized in that the cyanide is a cyanide salt, the amino acid is aspartic acid and/or glutamic acid in the acidic form, and the process is performed under acidic pH by the addition of between 0 and 1 equivalent of an acid based on the amount of aspartic or glutamic acid.
摘要翻译：本发明涉及氰化物与氨基酸和醛的反应的方法，其特征在于氰化物是氰化物盐，氨基酸是酸性形式的天冬氨酸和/或谷氨酸，该方法通过加入基于天冬氨酸或谷氨酸的量的0至1当量的酸在酸性pH下进行。

4. 发明授权

US08551312B2 Process to prepare amino acid-N, N-diacetic acid compounds 有权
标题翻译：制备氨基酸-N，N-二乙酸化合物的方法
公开(公告)号：US08551312B2
公开(公告)日：2013-10-08
申请号：US12516911
申请日：2007-11-27
申请人： Martin Heus , Hans Lammers , Arie Volmer
发明人： Martin Heus , Hans Lammers , Arie Volmer
IPC分类号： B01D61/42
CPC分类号： C07C227/40 , B01D61/44 , C07C229/16 , C07C229/24
摘要： The invention relates to a process for the production of an amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups or its salt with less than an equivalent of alkaline metal based on the number of carboxyl groups, said process comprising reducing alkali metal ions from an aqueous solution of an alkali metal salt of an amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups and acidifying the amino carboxylate starting material by first performing a chemical acidification step using an organic or inorganic acid to get a compound in which at least one of the groups is protonated, and in a subsequent step further acidifying the amino carboxylate starting material and reducing alkali metal ions from an aqueous solution of the partially acidified alkali metal salt of the amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups by electrodialysis, wherein the electrodialysis is performed using a hydrogen ion permselective membrane on the anode side and a cation-permeable membrane on the cathode side.
摘要翻译：本发明涉及一种制备具有至少一个仲氨基或叔氨基和三个或更多个羧基的氨基酸的方法或其盐，其基于羧基数目少于等于碱当量，所述方法包括从具有至少一个仲或叔氨基和三个或多个羧基的氨基酸的碱金属盐的水溶液中还原碱金属离子，并且通过首先使用有机或不饱和羧酸盐进行化学酸化步骤酸化氨基羧酸盐原料无机酸，得到其中至少一个基团被质子化的化合物，并且在随后的步骤中，进一步酸化氨基羧酸酯起始原料并从部分酸化的氨基酸的碱金属盐的水溶液中还原碱金属离子，其具有至少一个仲或叔氨基和三个或更多个羧基通过电渗析，其中选使用阳极侧的氢离子选择性膜和阴极侧的阳离子透过膜进行透析。

5. 发明申请

US20100126864A1 PROCESS TO PREPARE AMINO ACID-N, N-DIACETIC ACID COMPOUNDS 有权
标题翻译：制备氨基酸-N，N-二酸化合物的方法
公开(公告)号：US20100126864A1
公开(公告)日：2010-05-27
申请号：US12516911
申请日：2007-11-27
申请人： Martin Heus , Hans Lammers , Arie Volmer
发明人： Martin Heus , Hans Lammers , Arie Volmer
IPC分类号： C07C227/40
CPC分类号： C07C227/40 , B01D61/44 , C07C229/16 , C07C229/24
摘要： The invention relates to a process for the production of an amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups or its salt with less than an equivalent of alkaline metal based on the number of carboxyl groups, said process comprising reducing alkali metal ions from an aqueous solution of an alkali metal salt of an amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups and acidifying the amino carboxylate starting material by first performing a chemical acidification step using an organic or inorganic acid to get a compound in which at least one of the groups is protonated, and in a subsequent step further acidifying the amino carboxylate starting material and reducing alkali metal ions from an aqueous solution of the partially acidified alkali metal salt of the amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups by electrodialysis, wherein the electrodialysis is performed using a hydrogen ion permselective membrane on the anode side and a cation-permeable membrane on the cathode side.
摘要翻译：本发明涉及一种制备具有至少一个仲氨基或叔氨基和三个或更多个羧基的氨基酸的方法或其盐，其基于羧基数目少于等于碱当量，所述方法包括从具有至少一个仲或叔氨基和三个或多个羧基的氨基酸的碱金属盐的水溶液中还原碱金属离子，并且通过首先使用有机或不饱和羧酸盐进行化学酸化步骤酸化氨基羧酸盐原料无机酸，得到其中至少一个基团被质子化的化合物，并且在随后的步骤中，进一步酸化氨基羧酸酯起始原料并从部分酸化的氨基酸的碱金属盐的水溶液中还原碱金属离子，其具有至少一个仲或叔氨基和三个或更多个羧基通过电渗析，其中选使用阳极侧的氢离子选择性膜和阴极侧的阳离子透过膜进行透析。

6. 发明授权

US07918987B2 Electrochemical process to prepare a halogenated carbonyl group-containing compound 有权
标题翻译：电化学工艺制备含卤代羰基的化合物
公开(公告)号：US07918987B2
公开(公告)日：2011-04-05
申请号：US12300621
申请日：2007-05-11
申请人： Hans Lammers , Willem Koelewijn , Johannes Wilhelmus Franciscus Lucas Seetz , Joldert Faber
发明人： Hans Lammers , Willem Koelewijn , Johannes Wilhelmus Franciscus Lucas Seetz , Joldert Faber
IPC分类号： C25B3/06
CPC分类号： C25B3/06
摘要： The present invention provides a process to prepare a halogenated carbonyl group-containing compound by electrochemically reacting the corresponding carbonyl group-containing compound with a hydrogen halide H—X, an organic halide R′—X and/or a halide salt Mn+—Xn− under substantially water-free conditions, wherein X is a chlorine, bromine or iodine atom, R′ is an alkyl or aryl group that may be linear or branched, optionally containing one or more heteroatoms such as oxygen, nitrogen, chloride, bromide, fluoride or iodide of which the halogen atom X can be electrochemically split off, Mn+ is a quaternary ammonium, alkaline earth metal, alkali metal or metal cation, and n is an integer of 1 to 5, depending on the valency of the metal cation Mn+.
摘要翻译：本发明提供通过使相应的含羰基化合物与卤化氢H-X，有机卤化物R'-X和/或卤化物盐Mn + -Xn-的化合物电化学反应来制备含卤代羰基化合物的方法，在基本上无水条件下，其中X是氯，溴或碘原子，R'是可以是直链或支链的烷基或芳基，任选地含有一个或多个杂原子如氧，氮，氯，溴，氟或其卤素原子X可以电化学分解的碘化物，Mn +是季铵，碱土金属，碱金属或金属阳离子，n是1至5的整数，这取决于金属阳离子Mn +的化合价。

7. 发明申请

US20090107849A1 ELECTROCHEMICAL PROCESS TO PREPARE A HALOGENATED CARBONYL GROUP-CONTAINING COMPOUND 有权
标题翻译：电化学工艺制备含有羰基的含碳基团的化合物
公开(公告)号：US20090107849A1
公开(公告)日：2009-04-30
申请号：US12300621
申请日：2007-05-11
申请人： Hans Lammers , Willem Koelewijn , Johannes Wilhelmus Franciscus Lucas Seetz , Joldert Faber
发明人： Hans Lammers , Willem Koelewijn , Johannes Wilhelmus Franciscus Lucas Seetz , Joldert Faber
IPC分类号： C25B3/06
CPC分类号： C25B3/06
摘要： The present invention provides a process to prepare a halogenated carbonyl group-containing compound by electrochemically reacting the corresponding carbonyl group-containing compound with a hydrogen halide H—X, an organic halide R′—X and/or a halide salt Mn+—Xn− under substantially water-free conditions, wherein X is a chlorine, bromine or iodine atom, R′ is an alkyl or aryl group that may be linear or branched, optionally containing one or more heteroatoms such as oxygen, nitrogen, chloride, bromide, fluoride or iodide of which the halogen atom X can be electrochemically split off, Mn+ is a quaternary ammonium, alkaline earth metal, alkali metal or metal cation, and n is an integer of 1 to 5, depending on the valency of the metal cation Mn+.
摘要翻译：本发明提供了一种通过使相应的含羰基化合物与卤化氢HX，有机卤化物R'-X和/或卤化物盐Mn + -Xn-在实质上相互电化学反应来制备含卤代羰基化合物的方法无水条件，其中X是氯，溴或碘原子，R'是可以是直链或支链的烷基或芳基，任选地含有一个或多个杂原子如氧，氮，氯，溴，氟或碘其中卤素原子X可以电化学分解，Mn +是季铵，碱土金属，碱金属或金属阳离子，n是1至5的整数，这取决于金属阳离子Mn +的化合价。

8. 发明授权

US07211682B2 Aqueous solution of a sodium salt of HEDTA 有权
标题翻译： HEDTA钠盐水溶液
公开(公告)号：US07211682B2
公开(公告)日：2007-05-01
申请号：US10563762
申请日：2004-07-13
申请人： Martin Heus , Hans Lammers , Jim Lepage
发明人： Martin Heus , Hans Lammers , Jim Lepage
IPC分类号： C07F15/00 , C07C229/00 , C09K3/00
CPC分类号： C07C227/18 , B01D61/445 , C02F1/683 , C02F2101/203 , C07C229/12 , C07C229/76
摘要： The invention pertains to an aqueous solution of a sodium salt xNa+ yH+ of the chelating compound of formula I: wherein x=2.1–2.7, y=0.9–0.3, and x+y=3. The invention further pertains to a container comprising at least 0.5 kg of said aqueous solution and to a method of preparing an aqueous solution comprising at least 45 wt % of the sodium salt xNa+ yH+ of the chelating compound of formula I from Na3-HEDTA, comprising the steps of electrodialysing an aqueous solution containing less than 42 wt % of Na3-HEDTA using a bipolar membrane, thereby converting the trisodium salt solution to the solution of the sodium salt of formula I with x=2.1–2.7, y=0.9–0.3, and x+y=3.
摘要翻译：本发明涉及式I的螯合化合物的钠盐水溶液，其中x = 2.1-2.7，y = 0.9-0.3， x + y = 3。本发明还涉及包含至少0.5kg所述水溶液的容器和一种制备水溶液的方法，该水溶液包含至少45wt％的钠盐x Na +，H 2 O，该方法包括以下步骤：使用含有少于42重量％的Na 3 -HEDTA的水溶液进行电渗析，步骤由此将三钠盐溶液转化为式I的钠盐溶液，其中x = 2.1-2.7，y = 0.9-0.3，x + y = 3。

9. 发明申请

US20070015930A1 Aqueous solution of a sodium salt of hedta 有权
标题翻译： hedta的钠盐水溶液
公开(公告)号：US20070015930A1
公开(公告)日：2007-01-18
申请号：US10563762
申请日：2004-07-13
申请人： Martin Heus , Hans Lammers , Jim Lepage
发明人： Martin Heus , Hans Lammers , Jim Lepage
IPC分类号： C07F15/02 , C07C229/24
CPC分类号： C07C227/18 , B01D61/445 , C02F1/683 , C02F2101/203 , C07C229/12 , C07C229/76
摘要： The invention pertains to an aqueous solution of a sodium salt xNa+ yH+ of the chelating compound of formula I: wherein x=2.1−2.7, y=0.9−0.3, and x+y=3. The invention further pertains to a container comprising at least 0.5 kg of said aqueous solution and to a method of preparing an aqueous solution comprising at least 45 wt % of the sodium salt xNa+ yH+ of the chelating compound of formula I from Na3-HEDTA, comprising the steps of electrodialysing an aqueous solution containing less than 42 wt % of Na3-HEDTA using a bipolar membrane, thereby converting the trisodium salt solution to the solution of the sodium salt of formula I with x=2.1−2.7, y=0.9−0.3, and x+y=3.
摘要翻译：本发明涉及式I的螯合化合物的钠盐水溶液，其中x = 2.1-2.7，y = 0.9-0.3， x + y = 3。本发明还涉及一种包含至少0.5kg所述水溶液的容器以及一种制备包含至少45wt％的钠盐x Na + 该方法包括以下步骤：使用含有少于42重量％的Na 3 -HEDTA的水溶液进行电渗析，步骤由此将三钠盐溶液转化为式I的钠盐溶液，其中x = 2.1-2.7，y = 0.9-0.3，x + y = 3。

10. 发明授权

US06672164B1 Process for determining the polymer concentration in a spinning dope solution 失效
标题翻译：测定纺丝原液中聚合物浓度的方法
公开(公告)号：US06672164B1
公开(公告)日：2004-01-06
申请号：US10009804
申请日：2001-12-13
申请人： Willem G. Haanstra , Hendrikus J. M. Busschers , Hans Lammers
发明人： Willem G. Haanstra , Hendrikus J. M. Busschers , Hans Lammers
IPC分类号： G01N2904
CPC分类号： G01N29/024 , G01N29/30 , G01N2291/0224 , G01N2291/02809 , G01N2291/02818 , G01N2291/102
摘要： A process for determining the polymer concentration in a spinning dope solution involves measuring the propagation velocity of ultrasonic sound in the solution. The process prevents fluctuations in the polymer concentration as much as possible, and is therefore highly suitable for application in the production of fibers with consistent properties. An ultrasonic device used in the process is easier to clean, install, and calibrate than other presently commercially available devices.
摘要翻译：用于测定纺丝原液中聚合物浓度的方法包括测量溶液中超声波的传播速度。该方法尽可能地防止聚合物浓度的波动，因此高度适用于生产具有一致性能的纤维。在该方法中使用的超声波装置比其他目前市售的装置更容易清洁，安装和校准。

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