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1. 发明授权

US4255406A Treatment of ammonia synthesis purge gas 失效
标题翻译：处理氨合成吹扫气
公开(公告)号：US4255406A
公开(公告)日：1981-03-10
申请号：US83952
申请日：1979-10-10
申请人： Wieslaw H. Isalski , Terence R. Tomlinson
发明人： Wieslaw H. Isalski , Terence R. Tomlinson
IPC分类号： C01B3/50 , C01C1/04 , F25J3/06 , B01D51/00
CPC分类号： C01C1/0476 , C01B3/506 , F25J3/062 , F25J3/068 , C01B2203/0465 , C01B2203/048 , F25J2210/20 , F25J2245/02 , F25J2270/90 , F25J2280/02 , Y02P20/52
摘要： A process is disclosed for recovering hydrogen from an ammonia synthesis plant comprising(a) cooling a high pressure stream of said purge gas to a sub-ambient temperature at which substantially all of the methane and argon contained in said purge gas stream and a portion of the nitrogen condense,(b) expanding liquid and vapor components of the cooled high pressure stream to an intermediate pressure,(c) phase separating liquid and vapor components of the cooled and expanded purge gas stream,(d) expanding separated liquid component from step (c), and(e) heating expanded separated liquid component from step (d) and separated vapor component from step (c) in heat exchange with said high pressure stream of purge gas to cool the latter.
摘要翻译：公开了一种用于从氨合成装置回收氢气的方法，其包括（a）将所述吹扫气体的高压流冷却至低于所述吹扫气流中所含的基本上所有的甲烷和氩气的一部分，氮气冷凝，（b）将冷却的高压气流的液体和蒸汽组分膨胀到中间压力，（c）分离冷却和扩展的吹扫气体流的液体和蒸汽组分;（d）将分离的液体组分从步骤（c），和（e）从步骤（d）中加热膨胀的分离的液体组分和将步骤（c）中分离的蒸气组分与所述高压吹扫气体流热交换以冷却。

2. 发明授权

US4380461A Recovery of hydrogen from ammonia synthesis purge gas 失效
标题翻译：从氨合成吹扫气中回收氢气
公开(公告)号：US4380461A
公开(公告)日：1983-04-19
申请号：US208940
申请日：1980-11-21
申请人： Alan A. Haslam , Wieslaw H. Isalski , Terence R. Tomlinson
发明人： Alan A. Haslam , Wieslaw H. Isalski , Terence R. Tomlinson
IPC分类号： F25J3/06 , F25J3/00
CPC分类号： F25J3/062 , F25J3/068 , F25J2210/06 , F25J2210/20 , F25J2245/02 , F25J2280/02 , Y10S62/934
摘要： In a process for the recovery of hydrogen from compressed purge gas withdrawn from a recyling gas stream of an ammonia synthesis wherein the hydrogen is separated from the purge gas by partial condensation at cryogenic temperatures, refrigeration is provided by expanding and evaporating the condensate so formed, and the partial pressure of the expanded condensate is lowered by withdrawing a bleed stream from said uncondensed gas, expanding said bleed stream and injecting it into said expanded condensate, condensation of nitrogen employed to purge the cold box for the cryogenic process is avoided by either injecting into the bleed stream a warmer gas provided from the uncondensed gas and/or the purge gas or expanding the condensate and bleed stream in stages with separate expansion thereof in an initial stage and injection of the bleed stream into the condensate prior to the final stage.
摘要翻译：在从氨合成的再生气流中抽出的压缩吹扫气体回收氢气的过程中，其中通过在低温下部分冷凝将氢气与吹扫气体分离，通过膨胀和蒸发形成的冷凝物来提供制冷，并且通过从所述未冷凝的气体中抽出出口流，膨胀所述排放流并将其注入到所述膨胀的冷凝物中来降低膨胀的冷凝物的分压，通过注入来避免用于清除低温过程的冷箱的氮的冷凝从未冷凝的气体和/或吹扫气体中提供较热的气体，或者在初始阶段以分离的膨胀步骤逐步扩张冷凝物和排出流，并在最后阶段将排出流注入冷凝物中。

3. 发明授权

US4312851A Treatment of ammonia synthesis purge gas 失效
标题翻译：处理氨合成吹扫气
公开(公告)号：US4312851A
公开(公告)日：1982-01-26
申请号：US83827
申请日：1979-10-11
申请人： Wieslaw H. Isalski , Terence R. Tomlinson
发明人： Wieslaw H. Isalski , Terence R. Tomlinson
IPC分类号： C01C1/04 , F25J3/06
CPC分类号： F25J3/068 , C01C1/0476 , F25J3/062 , F25J2210/20 , F25J2230/20 , F25J2240/02 , Y02P20/52
摘要： A method of synthesizing ammonia by reacting a synthesis gas comprising nitrogen and hydrogen at superatmospheric pressure in a synthesis reaction zone with recycling of unreacting gas to the reacting zone is disclosed in which a purge gas stream is withdrawn at superatmospheric pressure and subjected to the steps of: (a) work expansion, (b) separation of methane and argon to form a gaseous product stream comprising nitrogen and hydrogen, (c) recompression of at least a portion of the gaseous product stream from step (b) using work generated in step (a), and (d) recycling of at least a portion of the recompressed product from step (c) to the reaction zone.Apparatus for effecting said process is also claimed.
摘要翻译：公开了一种合成氨的方法，该方法是通过在合成反应区中使含氮和氢的合成气在超大气压下反应而将反应气体再循环到反应区，其中吹扫气流在超大气压下被排出，：（a）工作膨胀，（b）分离甲烷和氩气以形成包含氮气和氢气的气态产物流，（c）使用在步骤（b）中产生的工作来重新压缩来自步骤（b）的气态产物流的至少一部分（a）和（d）将来自步骤（c）的再压缩产物的至少一部分再循环到反应区。还要求用于实现所述方法的装置。

4. 发明授权

US4622053A Separation of hydrocarbon mixtures 失效
标题翻译：烃混合物的分离
公开(公告)号：US4622053A
公开(公告)日：1986-11-11
申请号：US650724
申请日：1984-09-14
申请人： Terence R. Tomlinson , Donald R. Cummings
发明人： Terence R. Tomlinson , Donald R. Cummings
IPC分类号： C10G5/06 , C07C7/09 , C10G31/06 , F25J3/02
CPC分类号： F25J3/0252 , C07C7/09 , F25J3/0209 , F25J3/0233 , F25J3/0238 , F25J3/0242 , F25J2200/02 , F25J2200/04 , F25J2200/80 , F25J2210/04 , F25J2230/60 , F25J2235/60 , F25J2245/02 , F25J2270/04 , F25J2270/12 , F25J2270/60 , F25J2270/66 , F25J2270/902
摘要： In the process for the recovery of e.g. LPG or NGL and sales gas from a gaseous hydrocarbon feed 11 by partially condensing the feed in heat exchanger 1 at superatmospheric pressure, separating the condensate from the uncondensed gas in gas/liquid separator 2, rectifying the uncondensed gas to produce the sales gas and stripping the condensate to produce the LPG or NGL, substantially power savings are obtained if the rectification is effected in a reflux exchanger 103 and the stripping is effected in a separate distillation column 203.
摘要翻译：在回收例如 LPG或NGL和来自气态烃进料11的气体，通过在高压大气压下部分地冷凝热交换器1中的进料，将冷凝物从气体/液体分离器2中的未冷凝气体分离出来，对未冷凝的气体进行整流以产生销售气体和汽提如果在回流交换器103中进行精馏并且在单独的蒸馏塔203中进行汽提，则产生LPG或NGL的冷凝物基本上能够节省能源。

5. 发明授权

US4846863A Separation of hydrocarbon mixtures 失效
标题翻译：烃混合物的分离
公开(公告)号：US4846863A
公开(公告)日：1989-07-11
申请号：US158264
申请日：1988-02-18
申请人： Terence R. Tomlinson , Bogdan Czarnecki
发明人： Terence R. Tomlinson , Bogdan Czarnecki
IPC分类号： F25J3/02
CPC分类号： F25J3/0252 , F25J3/0209 , F25J3/0219 , F25J3/0233 , F25J3/0238 , F25J3/0242 , F25J2200/02 , F25J2200/04 , F25J2200/72 , F25J2200/74 , F25J2200/80 , F25J2205/04 , F25J2210/12 , F25J2230/08 , F25J2235/60 , F25J2240/02 , F25J2270/02 , F25J2270/12 , F25J2270/60 , F25J2270/66
摘要： In the method of separating a methane-containing light gas from a feed gas containing heavier hydrocarbons by (i) cooling the feed gas at superatmospheric pressure to partially condense it, (ii) separating a first condensate from the uncondensed gas, (iii) rectifying the uncondensed gas to produce the light gas and a second condensate (preferably by further cooling the uncondensed gas in a refluxing heat exchanger), and (iv) stripping at least one of the condensates in a distillation column to obtain an overhead stream and a liquid product stream, the power requirement is reduced by providing at least part of the cooling for step (i) by expanding at least a part of the feed gas in a turbo-expander which provides energy for compression of product gas comprising said light gas and/or uncondensed gas from the overhead from the distillation column.
摘要翻译：在通过（i）在超大气压下冷却进料气体以使其部分冷凝的方法中，从含有较重烃的原料气中分离含甲烷的轻质气体，（ii）从未冷凝的气体中分离出第一冷凝物，（iii）用于产生轻质气体的未冷凝气体和第二冷凝物（优选通过在回流热交换器中进一步冷却未冷凝气体），和（iv）在蒸馏塔中汽提至少一种冷凝物以获得塔顶馏出物流和液体通过在涡轮膨胀器中扩展至少一部分进料气体来提供步骤（i）的至少一部分冷却来降低功率需求，所述涡轮膨胀器提供用于压缩包括所述轻质气体和/ 或来自蒸馏塔的顶部的未冷凝气体。

6. 发明授权

US06581410B1 Low temperature separation of hydrocarbon gas 有权
标题翻译：碳氢化合物气体的低温分离
公开(公告)号：US06581410B1
公开(公告)日：2003-06-24
申请号：US09857598
申请日：2001-09-04
申请人： Grant L. Johnson , Adrian J. Finn , Terence R. Tomlinson
发明人： Grant L. Johnson , Adrian J. Finn , Terence R. Tomlinson
IPC分类号： F25J300
CPC分类号： C07C7/09 , F25J3/0209 , F25J3/0219 , F25J3/0233 , F25J3/0242 , F25J2200/04 , F25J2200/74 , F25J2200/78 , F25J2205/02 , F25J2205/04 , F25J2210/12 , F25J2235/60 , F25J2240/02
摘要： The invention provides a process for the separation of a heavier hydrocarbon fraction from a gaseous feed comprising a mixture of hydrocarbons, which process comprises subjecting the feed to a first fractionation to form a condensed product; subjecting the condensed product to a second fractionation, at a lower pressure than the first fractionation pressure, to provide the heavier hydrocarbon fraction and distillate fraction; and withdrawing the produced heavier fraction wherein the distillate from the second fractionation is partially condensed to provide reflux streams for both the first and second fractionations. Running the second fractionation at a lower pressure than the first means that there is phased let-down of pressure in two stages, leading to an increased pressure at the suction of the residue gas compressor and reduces power consumption. It also allows more efficient performance of the heat exchanger used to partially condense the reflux streams and simplifies the process, affording opportunities to better integrate process cooling and warming streams so increasing process efficiency. Increasing process efficiency reduces process power requirements or increases recovery of the desired heavier hydrocarbons or realizes both of these effects.
摘要翻译：本发明提供了一种从包含烃混合物的气态进料分离较重烃馏分的方法，该方法包括使进料进行第一分馏以形成冷凝产物; 在比第一分馏压力低的压力下使冷凝产物进行第二分馏，以提供较重的烃馏分和馏出馏分; 并且抽出所产生的较重的馏分，其中来自第二分馏的馏出物被部分冷凝以提供第一和第二分馏的回流。在比第一分压更低的压力下运行第二分馏意味着在两个阶段中分阶段降压，导致在残留气体压缩机抽吸时增加的压力并降低功率消耗。它还允许用于部分冷凝回流的热交换器的更有效的性能，并且简化了工艺，提供了更好地整合工艺冷却和升温流的机会，从而提高了工艺效率。提高工艺效率可降低工艺能力要求或提高所需较重碳氢化合物的回收率或实现这两种效果。

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