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1. 发明授权

US08876952B2 Method of removing mercury from a fluid stream using high capacity copper adsorbents 有权
标题翻译：使用高容量铜吸附剂从流体流中除去汞的方法
公开(公告)号：US08876952B2
公开(公告)日：2014-11-04
申请号：US13367219
申请日：2012-02-06
申请人： Dante A. Simonetti , Vladislav I. Kanazirev , Thomas J. Traynor
发明人： Dante A. Simonetti , Vladislav I. Kanazirev , Thomas J. Traynor
IPC分类号： B01D53/02
CPC分类号： C10L3/101 , B01J20/0237 , B01J20/0285 , B01J20/08 , B01J20/28004 , B01J20/28011 , B01J20/28069 , B01J2220/42 , C10G25/003 , C10G2300/201
摘要： A method of removing mercury from a fluid stream comprising contacting the fluid stream with a sorbent comprising cupric sulfide. The cupric sulfide is formed from direct sulfidation of copper carbonate, without thermal decomposition of the copper carbonate to an oxide, at a temperature less than about 150° C.
摘要翻译：一种从流体流中除去汞的方法，包括使流体流与包含硫化铜的吸附剂接触。在低于约150℃的温度下，硫酸铜是由碳酸铜的直接硫化形成的，而不会将碳酸铜热分解成氧化物。

2. 发明申请

US20120004480A1 ADSORBENT FOR FEED AND PRODUCTS PURIFICATION IN BENZENE SATURATION PROCESS 有权
标题翻译：用于进料和产品的添加剂在苯酐饱和过程中的纯化
公开(公告)号：US20120004480A1
公开(公告)日：2012-01-05
申请号：US13151449
申请日：2011-06-02
申请人： Vladislav I. Kanazirev , Jayant K. Gorawara , Dana K. Sullivan , Richard R. Rosin
发明人： Vladislav I. Kanazirev , Jayant K. Gorawara , Dana K. Sullivan , Richard R. Rosin
IPC分类号： C07C5/10
CPC分类号： C07C7/12 , C07C15/04
摘要： The service life and deactivation rate of a benzene saturation catalyst is improved through use of a new sulfur guard bed containing a chloride additive. This sulfur guard bed, which contains supported CuO material having an increased resistance to reduction, shows such improvement. Thus, the danger of run-away reduction followed by a massive release of water and deactivation of an isomerization catalyst is practically eliminated. The fact that the guard bed material preserves the active metal phase-copper in an active (oxide) form is an important advantage leading to very low sulfur content in the product stream. The sulfur capacity per unit weight of sorbent is also significantly increased, making this sorbent a superior cost effective sulfur guard product. The guard bed is effective in treating mixed phase feed streams.
摘要翻译：通过使用含有氯化物添加剂的新型硫磺保护床，可提高苯饱和催化剂的使用寿命和失活率。这种含有具有增加的还原性能的负载型CuO材料的硫磺保护床显示出这种改进。因此，实际上消除了逃逸减少的危险，随后大量释放水并使异构化催化剂失活。保护床材料以活性（氧化物）形式保留活性金属相铜的事实是导致产物流中硫含量非常低的重要优点。吸附剂每单位重量的硫含量也显着增加，使得该吸附剂成为一种优异的成本效益的硫磺防护产品。防护床在处理混合相进料物流中是有效的。

3. 发明授权

US08007760B2 Process for producing enhanced alumina 有权
标题翻译：生产增强型氧化铝的方法
公开(公告)号：US08007760B2
公开(公告)日：2011-08-30
申请号：US12332421
申请日：2008-12-11
申请人： Vladislav I. Kanazirev
发明人： Vladislav I. Kanazirev
IPC分类号： C01F7/02 , C01C1/26 , C01F7/00
CPC分类号： C01F7/021 , C01F7/004 , C01F7/30 , C01P2006/12 , C01P2006/14 , C01P2006/37
摘要： The present invention provides an essentially dry method for preparation of enhanced alumina powders. The first step involves rapid calcination of an aluminum compound to produce alumina powder. The alumina powder is mixed with solid ammonium carbonate and a small amount of water. This mixture heats itself although some external heat is helpful to produce ammonium aluminum hydroxycarbonate (dawsonite-type) NH4AlCO3(OH)2 upon curing which is then decomposed to produce enhanced alumina having a specific desired morphology and nano-sized dimensions.
摘要翻译：本发明提供了用于制备增强氧化铝粉末的基本上干燥的方法。第一步涉及铝化合物的快速煅烧以生产氧化铝粉末。氧化铝粉末与固体碳酸铵和少量的水混合。该混合物自身加热，尽管一些外部热量有助于在固化时产生羟基碳酸铵（片钠铝型）NH 4 AlCO 3（OH）2，然后将其分解以产生具有特定所需形态和纳米尺寸尺寸的增强氧化铝。

4. 发明授权

US07758837B2 Scavengers for removal of acid gases from fluid streams 有权
标题翻译：用于从流体流中除去酸性气体的清除剂
公开(公告)号：US07758837B2
公开(公告)日：2010-07-20
申请号：US11123642
申请日：2005-05-06
申请人： Vladislav I. Kanazirev
发明人： Vladislav I. Kanazirev
IPC分类号： B01D53/12 , B01D53/68 , B01J20/08
CPC分类号： B01J20/08 , B01D53/02 , B01D2253/104 , B01D2257/2045 , B01J20/0277 , B01J2220/44 , C01F7/004 , C01P2002/60 , C01P2002/82 , C01P2006/10 , C01P2006/80 , C01P2006/82
摘要： A composite sorbent is formed which is the reaction product of a solid alkali metal carbonate, rehydratable alumina and water or an aqueous solution of a metal salt. The reaction between the components occurs while forming particulates followed by curing and activation. In one embodiment, the composite contains an appreciable amount of a Dawsonite-type hydroxycarbonate as a final product or as an intermediate in at least one of the production stages. The alkali metal in the sorbent exhibits a highly reactive and accessible state that is very favorable for various sorption applications. The sorbent is especially useful for removal of HCl and other acid contaminants from gas and liquid hydrocarbon streams. It combines a high capacity for the contaminants with a low reactivity towards the hydrocarbon components of the main stream.
摘要翻译：形成复合吸附剂，其是固体碱金属碳酸盐，可再水化的氧化铝和水或金属盐的水溶液的反应产物。组分之间的反应在形成颗粒之后发生，随后固化和活化。在一个实施方案中，所述复合材料在至少一个生产阶段中含有可观量的作为最终产物的道亚逊型羟基碳酸酯或中间体。吸附剂中的碱金属表现出非常有利于各种吸附应用的高反应性和可接近的状态。吸附剂特别适用于从气体和液态烃流中去除HCl和其他酸性污染物。它将高容量的污染物与对主流的烃组分具有低反应性相结合。

5. 发明授权

US6159898A Alumina bodies containing alkali or alkaline earth metal compounds 有权
标题翻译：含碱金属或碱土金属化合物的氧化铝体
公开(公告)号：US6159898A
公开(公告)日：2000-12-12
申请号：US215761
申请日：1998-12-19
申请人： Vladislav I. Kanazirev
发明人： Vladislav I. Kanazirev
IPC分类号： B01J20/04 , B01J20/08 , B01J20/00
CPC分类号： B01J20/08 , B01J20/041 , B01J20/3007 , B01J20/3078 , B01J20/3204 , B01J20/3236
摘要： A method of producing activated alumina bodies having alkali or alkaline earth metal compounds incorporated therein, the bodies suitable for adsorption and having increased capacity for adsorption of gases and the like. The method comprises providing a source of activated alumina powder and further providing an aqueous solution having an alkali or alkaline earth metal hydroxide and a water soluble alkali or alkaline earth metal salt of an organic compound dissolved therein. The activated alumina powder is formed into bodies which are treated with the aqueous solution to provide alumina bodies having alkali or alkaline earth metal compounds incorporated therein. The alumina bodies are heated for purposes of activation to provide said activated alumina bodies capable of having increased adsorption capacity.
摘要翻译：一种生产具有掺入其中的碱金属或碱土金属化合物的活性氧化铝体的方法，适用于吸附并具有增加的气体吸附能力等的物质。该方法包括提供活性氧化铝粉末源，并进一步提供其中溶解有有机化合物的碱金属或碱土金属氢氧化物和水溶性碱金属或碱土金属盐的水溶液。活性氧化铝粉末形成为用水溶液处理以提供掺入其中的碱金属或碱土金属化合物的氧化铝体的体。氧化铝体被加热以用于活化，以提供能够增加吸附能力的所述活化氧化铝体。

6. 发明授权

US5935894A Alumina based adsorbent containing alkali metal compounds 失效
标题翻译：基于氧化铝的吸附剂含有碱金属化合物
公开(公告)号：US5935894A
公开(公告)日：1999-08-10
申请号：US886993
申请日：1997-07-02
申请人： Vladislav I. Kanazirev
发明人： Vladislav I. Kanazirev
IPC分类号： B01J20/08 , B01J23/02 , B01J23/04 , B01J20/04 , B01J21/04
CPC分类号： B01J20/08 , B01J23/02 , B01J23/04
摘要： A method of preparing an alumina-based bodies suitable for use as an adsorbent or catalyst, the method comprising providing a source of activated alumina powder for forming into bodies and providing an aqueous solution containing at least two different alkali metals, at least one alkali metal derived from a soluble carboxylic acid alkali metal salt. As said powder is formed into said bodies, the bodies are contacted or sprayed with the aqueous solution to provide composite bodies containing the alumina powder and the alkali metals and the soluble carboxylic acid alkali metal salt. Alternatively, the alumina bodies may be formed first and then contacted, e.g., soaked in the aqueous solution. Or, a viscous slurry of the activated alumina powder and the aqueous solution may be made. The viscous slurry may be made into bodies by extrusion or by the oil drop method. Thereafter, the bodies are thermally treated to activate alumina therein and remove or decompose the organic part, e.g., carboxylic acid, of the soluble carboxylic acid alkali metal salt.
摘要翻译：一种制备适合用作吸附剂或催化剂的氧化铝基体的方法，所述方法包括提供用于形成体的活性氧化铝粉末源，并提供含有至少两种不同碱金属的水溶液，至少一种碱金属衍生自可溶性羧酸碱金属盐。当所述粉末形成所述体时，将体与水溶液接触或喷雾，以提供含有氧化铝粉末和碱金属和可溶性羧酸碱金属盐的复合体。或者，可以首先形成氧化铝体，然后接触，例如浸泡在水溶液中。或者，可以制备活性氧化铝粉末和水溶液的粘稠浆液。粘稠浆料可以通过挤压或油滴法制成体内。此后，将物体热处理以在其中活化氧化铝，并除去或分解可溶性羧酸碱金属盐的有机部分，例如羧酸。

7. 发明申请

US20130202511A1 Method for Removal of Heterocyclic Sulfur using Metallic Copper 审中-公开
标题翻译：使用金属铜去除杂环硫的方法
公开(公告)号：US20130202511A1
公开(公告)日：2013-08-08
申请号：US13367174
申请日：2012-02-06
申请人： Vladislav I. Kanazirev , Jayant K. Gorawara
发明人： Vladislav I. Kanazirev , Jayant K. Gorawara
IPC分类号： B01D53/48 , B01D15/00 , B01D53/52
CPC分类号： B01D53/48 , B01D53/02 , B01D2253/1122 , B01D2253/1124 , B01D2255/20761 , B01D2257/304 , B01D2257/306 , B01D2257/308 , B01J20/0237 , B01J20/0277 , B01J20/046 , B01J20/06 , B01J20/28004 , B01J20/3078 , B01J20/3204 , B01J20/3236 , C10G25/003 , C10G2300/202 , C10L3/104
摘要： A method of removing mercaptans, heterocyclic sulfur compounds, and/or COS from a fluid stream comprising contacting the fluid stream with a sorbent comprising a mixture of Cu2O and metallic copper.
摘要翻译：从流体流中除去硫醇，杂环硫化合物和/或COS的方法，包括使流体流与包含Cu 2 O和金属铜的混合物的吸附剂接触。

8. 发明授权

US07906088B2 Method of removing impurities from gas or liquid streams using copper oxide and halide salt 有权
标题翻译：使用氧化铜和卤化物盐从气体或液体流中除去杂质的方法
公开(公告)号：US07906088B2
公开(公告)日：2011-03-15
申请号：US12548223
申请日：2009-08-26
申请人： Vladislav I. Kanazirev , Peter Rumfola, III
发明人： Vladislav I. Kanazirev , Peter Rumfola, III
IPC分类号： B01D53/00
CPC分类号： C01G3/02 , B01D15/00 , B01D53/02 , B01D2253/112 , B01D2256/24 , B01D2257/304 , B01D2257/306 , B01D2257/308 , B01J20/046 , B01J20/06 , B01J20/3007 , B01J20/3078 , B01J20/3204 , B01J20/3236 , B01J2220/42 , C01P2002/52
摘要： Mixing small amounts of an inorganic halide, such as NaCl, to basic copper carbonate followed by calcination at a temperature sufficient to decompose the carbonate results in a significant improvement in resistance to reduction of the resulting copper oxide. The introduction of the halide can be also achieved during the precipitation of the carbonate precursor. These reduction resistant copper oxides can be in the form of composites with alumina and are especially useful for purification of gas or liquid streams containing hydrogen or other reducing agents. These reduction resistant copper oxides can function at near ambient temperatures.
摘要翻译：将少量无机卤化物如NaCl混合到碱式碳酸铜中，然后在足以分解碳酸酯的温度下煅烧导致所得到的氧化铜的还原性的显着提高。在碳酸盐前体的沉淀过程中也可以实现卤化物的引入。这些还原性铜氧化物可以是与氧化铝的复合物的形式，并且特别可用于纯化含有氢或其它还原剂的气体或液体流。这些还原性铜氧化物可以在接近环境温度下起作用。

9. 发明申请

US20100150820A1 Process for Producing Enhanced Alumina 有权
标题翻译：生产增强型氧化铝的工艺
公开(公告)号：US20100150820A1
公开(公告)日：2010-06-17
申请号：US12332421
申请日：2008-12-11
申请人： Vladislav I. Kanazirev
发明人： Vladislav I. Kanazirev
IPC分类号： C01F7/30
CPC分类号： C01F7/021 , C01F7/004 , C01F7/30 , C01P2006/12 , C01P2006/14 , C01P2006/37
摘要： The present invention provides an essentially dry method for preparation of enhanced alumina powders. The first step involves rapid calcination of an aluminum compound to produce alumina powder. The alumina powder is mixed with solid ammonium carbonate and a small amount of water. This mixture heats itself although some external heat is helpful to produce ammonium aluminum hydroxycarbonate (dawsonite-type) NH4AlCO3(OH)2 upon curing which is then decomposed to produce enhanced alumina having a specific desired morphology and nano-sized dimensions.
摘要翻译：本发明提供了用于制备增强氧化铝粉末的基本上干燥的方法。第一步涉及铝化合物的快速煅烧以生产氧化铝粉末。氧化铝粉末与固体碳酸铵和少量的水混合。该混合物自身加热，尽管一些外部热量有助于在固化时产生羟基碳酸铵（片钠铝型）NH 4 AlCO 3（OH）2，然后将其分解以产生具有特定所需形态和纳米尺寸尺寸的增强氧化铝。

10. 发明授权

US07645306B2 Removal of mercury from fluids by supported metal oxides 有权
标题翻译：通过负载金属氧化物去除流体中的汞
公开(公告)号：US07645306B2
公开(公告)日：2010-01-12
申请号：US11955470
申请日：2007-12-13
申请人： Vladislav I. Kanazirev
发明人： Vladislav I. Kanazirev
IPC分类号： C10L3/10
CPC分类号： C10G25/003 , C10G2300/1025 , C10G2300/202 , C10G2300/205 , C10G2300/207
摘要： This invention relates to the use of a copper oxide adsorbent to remove mercury from a feed stream. When the feed stream is low in sulfur content, a sulfidation agent such as hydrogen sulfide should be added to the feed stream.
摘要翻译：本发明涉及使用氧化铜吸附剂从进料流中除去汞。当进料流的硫含量低时，应将硫化剂如硫化氢加入进料流中。

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