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1. 发明申请

US20070196645A1 Method for high density data storage and imaging 有权
标题翻译：高密度数据存储和成像方法
公开(公告)号：US20070196645A1
公开(公告)日：2007-08-23
申请号：US11358774
申请日：2006-02-21
申请人： Urs Duerig , Jane Frommer , Bernd Gotsmann , Erik Hagberg , James Hedrick , Armin Knoll , Victor Lee , Teddie Magbitang , Robert Miller , Russell Pratt , Charles Wade , Johannes Windeln
发明人： Urs Duerig , Jane Frommer , Bernd Gotsmann , Erik Hagberg , James Hedrick , Armin Knoll , Victor Lee , Teddie Magbitang , Robert Miller , Russell Pratt , Charles Wade , Johannes Windeln
IPC分类号： B32B27/00
CPC分类号： G11B9/149 , B82Y10/00 , G11B9/1454 , Y10T428/265 , Y10T428/31721
摘要： An approach is presented for designing a polymeric layer for nanometer scale thermo-mechanical storage devices. Cross-linked polyimide oligomers are used as the recording layers in atomic force data storage device, giving significantly improved performance when compared to previously reported cross-linked and linear polymers. The cross-linking of the polyimide oligomers may be tuned to match thermal and force parameters required in read-write-erase cycles. Additionally, the cross-linked polyimide oligomers are suitable for use in nano-scale imaging.
摘要翻译：提出了一种用于设计用于纳米级热机械存储装置的聚合物层的方法。交联聚酰亚胺低聚物用作原子力数据存储装置中的记录层，与先前报道的交联和线性聚合物相比，显着提高了性能。可以调整聚酰亚胺低聚物的交联以匹配读写擦除周期中所需的热和强度参数。另外，交联聚酰亚胺低聚物适用于纳米级成像。

2. 发明申请

US20140113999A1 REDUCED COLOR EPOXIDIZED ESTERS FROM EPOXIDIZED NATURAL FATS AND OILS 审中-公开
标题翻译：从环氧化天然脂肪和油中减少颜色的环氧化酯
公开(公告)号：US20140113999A1
公开(公告)日：2014-04-24
申请号：US14125602
申请日：2012-05-21
申请人： Stephen Howard , Erik Hagberg , George Poppe
发明人： Stephen Howard , Erik Hagberg , George Poppe
IPC分类号： C11C3/10 , C08K5/10
CPC分类号： C11C3/10 , C07D303/42 , C08K5/10 , C11B3/02 , C11C1/08
摘要： Reduced color epoxidized fatty acid esters are provided which may be used as primary plasticizers for PVC, in replacement of phthalate plasticizers. The reduced color epoxidized fatty acid esters are prepared from natural fats or oils by transesterification and interesterification processes, whereby through the use of borohydride, materials having Pt-Co colors according to ASTM D1209 on the order of 50 and lower are possible.
摘要翻译：提供了减少颜色的环氧化脂肪酸酯，其可用作PVC的主要增塑剂，以替代邻苯二甲酸酯增塑剂。通过酯交换和酯交换方法由天然脂肪或油制备还原型环氧化脂肪酸酯，由此通过使用硼氢化物，可以使用根据ASTM D1209的Pt-Co颜色的数量级为50以下的材料。

3. 发明申请

US20070299188A1 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：US20070299188A1
公开(公告)日：2007-12-27
申请号：US11766423
申请日：2007-06-21
申请人： Kwok Chan , Erik Hagberg , Tara Mullen , Roy Odle , James White , Norimitsu Yamaguchi
发明人： Kwok Chan , Erik Hagberg , Tara Mullen , Roy Odle , James White , Norimitsu Yamaguchi
IPC分类号： C08K9/04 , C08K5/50
CPC分类号： C08J3/201 , B82Y30/00 , C01B33/44 , C08J5/005 , C08K3/346 , C08K5/50 , C08K9/04
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a method of making a polymer-organoclay composite composition, said method comprising melt mixing a quaternary organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary organic cation with a polymeric resin comprising at least one polymer selected from the group consisting of polyamides, polyesters, polyarylene sulfides, polyarylene ethers, polyether sulfones, polyether ketones, polyether ether ketones, polyphenylenes, and polycarbonates, said polymeric resin being substantially free of polyetherimides; said melt mixing being carried out at a temperature in a range between about 300° C. and about 450° C. to provide a polymer-organoclay composite composition, said polymer-organoclay composite composition being characterized by a percent exfoliation of at least 10 percent.
摘要翻译：本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合材料组合物和制备聚合物纳米复合材料的方法的有机盐组合物。在一个实施方案中，本发明提供了制备聚合物 - 有机粘土复合材料组合物的方法，所述方法包括熔融混合包含交替的无机硅酸盐层和有机层的季有机粘土组合物，所述有机层包含季铵有机阳离子与聚合树脂，选自聚酰胺，聚酯，聚亚芳基硫醚，聚亚芳基醚，聚醚砜，聚醚酮，聚醚醚酮，聚苯基和聚碳酸酯的至少一种聚合物，所述聚合物树脂基本上不含聚醚酰亚胺; 所述熔体混合在约300℃至约450℃之间的温度下进行，以提供聚合物 - 有机粘土复合材料组合物，所述聚合物 - 有机粘土复合组合物的特征在于至少10％的剥离百分比。

4. 发明申请

US20080044639A1 POLYIMIDE SOLVENT CAST FILMS HAVING A LOW COEFFICIENT OF THERMAL EXPANSION AND METHOD OF MANUFACTURE THEREOF 审中-公开
标题翻译：具有低热膨胀系数的聚酰亚胺溶剂型薄膜及其制造方法
公开(公告)号：US20080044639A1
公开(公告)日：2008-02-21
申请号：US11758782
申请日：2007-06-06
申请人： Kwok Pong Chan , Erik Hagberg , Tara J. Mullen , Roy Ray Odle
发明人： Kwok Pong Chan , Erik Hagberg , Tara J. Mullen , Roy Ray Odle
IPC分类号： C08G69/26 , B32B5/00 , C08K3/34
CPC分类号： H05K1/0346 , B82Y30/00 , C08G73/1007 , C08J5/005 , C08J5/18 , C08J2379/08 , H05K1/0373 , H05K2201/0154 , H05K2201/0209 , H05K2201/0257 , H05K2201/068
摘要： A solvent cast film comprises a polyimide comprising structural units derived from polymerization of a dianhydride component comprising a dianhydride selected from the group consisting of 3,4′-oxydiphthalic dianhydride, 3,3′-oxydiphthalic dianhydride, 4,4′-oxydiphthalic dianhydride, and combinations thereof, with a diamine component wherein the polyimide has a glass transition temperature of at least 190° C.; wherein the film has a coefficient of thermal expansion of less than 60 ppm/° C., a thickness from 0.1 to 250 micrometers, and less than 5% residual solvent by weight; wherein the polyimide has less than 15 molar % of structural units derived from a member selected from the group consisting of biphenyltetracarboxylic acid, a dianhydride of biphenyltetracarboxylic acid, an ester of biphenyltetracarboxylic acid, and a combination thereof.
摘要翻译：溶剂流延膜包括聚酰亚胺，其包含衍生自二酐组分的聚合的结构单元，所述二酐组分包含二酐，其选自3,4'-氧二邻苯二甲酸二酐，3,3'-氧联二邻苯二甲酸二酐，4,4'-氧联二邻苯二甲酸二酐，和其组合与二胺组分，其中聚酰亚胺的玻璃化转变温度至少为190℃; 其中所述膜具有小于60ppm /℃的热膨胀系数，0.1至250微米的厚度和小于5重量％的残留溶剂; 其中所述聚酰亚胺具有少于15摩尔％的衍生自选自联苯四羧酸，联苯四羧酸的二酐，联苯四羧酸的酯及其组合的成员的结构单元。

5. 发明申请

US20080004391A1 METHODS OF PREPARING POLYMER-ORGANOCLAY COMPOSITES AND ARTICLES DERIVED THEREFROM 失效
标题翻译：制备聚合物 - 组织复合材料的方法及其衍生物
公开(公告)号：US20080004391A1
公开(公告)日：2008-01-03
申请号：US11766456
申请日：2007-06-21
申请人： Kwok Chan , Sarah Genovese , Erik Hagberg , David Hall , John Maxam , Tara Mullen , Roy Odle , Albert Stella , James White
发明人： Kwok Chan , Sarah Genovese , Erik Hagberg , David Hall , John Maxam , Tara Mullen , Roy Odle , Albert Stella , James White
IPC分类号： C08K9/04
CPC分类号： C08F2/44
摘要： A method for preparing a polymer-organoclay composite composition comprises combining a solvent and an unexfoliated organoclay to provide a first mixture, wherein the unexfoliated organoclay comprises alternating inorganic silicate layers and organic layers, and has an initial spacing between the silicate layers; exposing the first mixture to an energized condition of a sufficient intensity and duration to increase the initial spacing of the inorganic silicate layers, to provide a second mixture; contacting the second mixture with a polymer composition so that the polymer composition fills at least one region located between at least one pair of silicate layers, wherein the polymer composition is at least partially soluble in the solvent; and removing at least a portion of the solvent from the second mixture, wherein the inorganic silicate layers remain separated by the polymer after removal of the solvent.
摘要翻译：一种制备聚合物 - 有机粘土复合材料组合物的方法，包括将溶剂和未剥离的有机粘土组合以提供第一混合物，其中未剥离的有机粘土包含交替的无机硅酸盐层和有机层，并且在硅酸盐层之间具有初始间隔; 将第一混合物暴露于足够强度和持续时间的通电状态以增加无机硅酸盐层的初始间隔，以提供第二混合物; 使所述第二混合物与聚合物组合物接触，使得所述聚合物组合物填充位于至少一对硅酸盐层之间的至少一个区域，其中所述聚合物组合物至少部分地可溶于所述溶剂中; 以及从所述第二混合物中除去至少一部分所述溶剂，其中在去除所述溶剂之后，所述无机硅酸盐层保持被所述聚合物分离。

6. 发明申请

US20150225358A1 PROCESS FOR MAKING CERTAIN EPOXIDIZED FATTY ACID ESTER PLASTICIZERS 审中-公开
标题翻译：制备某些环氧化脂肪酸酯类增塑剂的方法
公开(公告)号：US20150225358A1
公开(公告)日：2015-08-13
申请号：US14178692
申请日：2014-02-12
申请人： Stephen Howard , Erik Hagberg
发明人： Stephen Howard , Erik Hagberg
IPC分类号： C07D301/00
CPC分类号： C07D301/00
摘要： A process is described for making an epoxidized fatty acid ester material useful as a plasticizer for flexible PVC applications, comprising: transesterifying a low moisture epoxidized natural fat or oil with a first alcohol in a first transesterification step; then, after the resultant product mixture phase separates into an epoxidized fatty acid ester phase and a second phase comprising byproduct glycerol, substantially removing the second phase; combining epoxidized fatty acid esters in the epoxidized fatty acid ester phase with more of the first alcohol and with a second alcohol which includes 5 to 7 members in a ring structure and carrying out a second transesterification step, while continuously removing first alcohol during the second transesterification step in order to drive the reaction with the second alcohol toward the desired epoxidized fatty acid ester material from the second alcohol, but without large molar excesses of the second alcohol being required.
摘要翻译：描述了一种制备用作柔性PVC应用的增塑剂的环氧化脂肪酸酯材料的方法，其包括：在第一酯交换步骤中将低水分环氧化天然油脂与第一醇酯交换; 然后，在所得产物混合物相分离成环氧化脂肪酸酯相和包含副产物甘油的第二相后，基本上除去第二相; 将环氧化脂肪酸酯相中的环氧化脂肪酸酯与更多的第一醇和第二醇组合，其中第二醇在环结构中包含5至7个成员并进行第二酯交换步骤，同时在第二酯交换过程中连续除去第一醇步骤，以便使第二种醇与第二种醇向所需的环氧化脂肪酸酯物质的反应中驱动，但不需要大量摩尔过量的第二种醇。

7. 发明授权

US08703849B2 Processes for making high purity renewable source-based plasticizers and products made therefrom 有权
标题翻译：制造高纯度可再生源基增塑剂和由其制成的产品的方法
公开(公告)号：US08703849B2
公开(公告)日：2014-04-22
申请号：US13519956
申请日：2011-01-04
申请人： Erik Hagberg , Stephen Howard , George Poppe , Stephen D. Horton
发明人： Erik Hagberg , Stephen Howard , George Poppe , Stephen D. Horton
IPC分类号： C08K5/1515 , C11C1/06 , C07D301/02 , C07D301/00 , C08L27/06 , C11C3/10
CPC分类号： C07D303/42 , C07C67/03 , C07C67/60 , C07C69/52 , C08K5/1515 , C11C3/003 , C08L27/06
摘要： Presently disclosed are high purity unsaturated fatty acid esters with an ester moiety characterized by having from five to seven members in a ring structure, which esters when epoxidized find particular utility as primary plasticizers in flexible polyvinyl halide applications. Also disclosed are processes for making the high purity esters.
摘要翻译：目前公开的是具有酯部分的高纯度不饱和脂肪酸酯，其特征在于在环结构中具有5-7个成员，当环氧化时，该酯特别用作柔性聚卤乙烯应用中的主要增塑剂。还公开了制备高纯度酯的方法。

8. 发明申请

US20080044683A1 POLYIMIDE SOLVENT CAST FILMS HAVING A LOW COEFFICIENT OF THERMAL EXPANSION AND METHOD OF MANUFACTURE THEREOF 有权
标题翻译：具有低热膨胀系数的聚酰亚胺溶剂型薄膜及其制造方法
公开(公告)号：US20080044683A1
公开(公告)日：2008-02-21
申请号：US11758796
申请日：2007-06-06
申请人： Kwok Pong Chan , Erik Hagberg , Tara J. Mullen , Roy Ray Odle
发明人： Kwok Pong Chan , Erik Hagberg , Tara J. Mullen , Roy Ray Odle
IPC分类号： B32B15/088 , B32B5/00 , C08G69/26 , C08K3/34
CPC分类号： H05K1/0346 , C08G73/1007 , C08J5/18 , C08J2379/08 , C08L79/08 , H05K1/0373 , H05K2201/0154 , H05K2201/0209 , H05K2201/0257 , H05K2201/068 , Y10T428/12569 , Y10T428/25 , Y10T428/31678 , Y10T428/31681 , Y10T428/31721
摘要： A solvent cast film comprises a polyimide comprising structural units derived from polymerization of a dianhydride component comprising a dianhydride selected from the group consisting of 3,4′-oxydiphthalic dianhydride, 3,3′-oxydiphthalic dianhydride, 4,4′-oxydiphthalic dianhydride, and combinations thereof, with a diamine component comprising 4,4′-diaminodiphenylsulfone; wherein the polyimide has a glass transition temperature from 190° C. to 400° C.; and wherein the film has a coefficient of thermal expansion of less than 60 ppm/° C., a thickness from 0.1 to 250 micrometers, endless than 5% residual solvent by weight.
摘要翻译：溶剂流延膜包括聚酰亚胺，其包含衍生自二酐组分的聚合的结构单元，所述二酐组分包含二酐，其选自3,4'-氧二邻苯二甲酸二酐，3,3'-氧联二邻苯二甲酸二酐，4,4'-氧联二邻苯二甲酸二酐，和其组合与二胺组分包含4,4'-二氨基二苯砜; 其中所述聚酰亚胺的玻璃化转变温度为190℃至400℃; 并且其中所述膜具有小于60ppm /℃的热膨胀系数，0.1至250微米的厚度，不超过5重量％的残留溶剂。

9. 发明申请

US20080044682A1 ARTICLES COMPRISING A POLYIMIDE SOLVENT CAST FILM HAVING A LOW COEFFICIENT OF THERMAL EXPANSION AND METHOD OF MANUFACTURE THEREOF 有权
标题翻译：包含具有低热膨胀系数的聚酰亚胺溶剂铸膜的制品及其制造方法
公开(公告)号：US20080044682A1
公开(公告)日：2008-02-21
申请号：US11758773
申请日：2007-06-06
申请人： Kwok Pong Chan , Erik Hagberg , Tara J. Mullen , Roy Ray Odle
发明人： Kwok Pong Chan , Erik Hagberg , Tara J. Mullen , Roy Ray Odle
IPC分类号： B32B15/088 , B32B17/10 , B32B25/08 , C08G69/28 , C08K3/34
CPC分类号： H05K1/0346 , B32B15/08 , C08G73/1007 , C08J5/18 , C08J2379/08 , C08K3/346 , C08L79/08 , H05K2201/0154 , H05K2201/068 , Y10T428/12569 , Y10T428/2938 , Y10T428/31765
摘要： An article comprises a solvent cast film comprising a polyetherimide comprising structural units derived from a dianhydride component selected from the group consisting of 3,4′-oxydiphthalic anhydride, 3,3′-oxydiphthalic anhydride, 4,4′-oxydiphthalic anhydride, and combinations thereof, and a diamine component. The polyetherimide has a glass transition temperature that is at least 190° C. The film has a coefficient of thermal expansion of less than 60 ppm/° C., a thickness from 0.1 to 250 micrometers, and less than 5% residual solvent by weight. The film has less than 15 molar % of a member selected from the group consisting of biphenyltetracarboxylic acid, dianhydrides of biphenyltetracarboxylic acid, esters of biphenyltetracarboxylic acid, and combinations thereof.
摘要翻译：一种制品包括含有聚醚酰亚胺的溶剂流延膜，该聚醚酰亚胺包含衍生自二酐组分的结构单元，所述二酐组分选自3,4'-氧联二邻苯二甲酸酐，3,3'-氧联二邻苯二甲酸酐，4,4'-氧联二邻苯二甲酸酐和组合和二胺组分。聚醚酰亚胺的玻璃化转变温度至少为190℃。该薄膜的热膨胀系数小于60ppm /℃，厚度为0.1至250微米，小于5％的残留溶剂重量。该膜具有少于15摩尔％的选自联苯四羧酸，联苯四羧酸的二酐，联苯四羧酸的酯及其组合的成员。

10. 发明授权

US09708571B2 Reduced color epoxidized esters from epoxidized natural fats and oils 有权
公开(公告)号：US09708571B2
公开(公告)日：2017-07-18
申请号：US14125602
申请日：2012-05-21
申请人： Stephen Howard , Erik Hagberg , George Poppe
发明人： Stephen Howard , Erik Hagberg , George Poppe
IPC分类号： C11C3/10 , C11C1/08 , C07D303/42 , C08K5/10 , C11B3/02
CPC分类号： C11C3/10 , C07D303/42 , C08K5/10 , C11B3/02 , C11C1/08
摘要： Reduced color epoxidized fatty acid esters are provided which may be used as primary plasticizers for PVC, in replacement of phthalate plasticizers. The reduced color epoxidized fatty acid esters are prepared from natural fats or oils by transesterification and interesterification processes, whereby through the use of borohydride, materials having Pt—Co colors according to ASTM D1209 on the order of 50 and lower are possible.

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