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1. 发明授权

US09302257B2 Process for the preparation of a titanium zeolite catalyst 有权
标题翻译：制备钛沸石催化剂的方法
公开(公告)号：US09302257B2
公开(公告)日：2016-04-05
申请号：US12954802
申请日：2010-11-26
申请人： Ulrich Müller , Peter Rudolf , Georg Krug , Rainer Senk
发明人： Ulrich Müller , Peter Rudolf , Georg Krug , Rainer Senk
IPC分类号： B01J29/04 , B01J29/89 , B01J37/00 , B01J37/08 , C07D301/12
CPC分类号： B01J29/89 , B01J37/0018 , B01J37/084 , B01J2229/42 , C07D301/12
摘要： A process for the preparation of a catalyst for the use in a hydrocarbon conversion reaction, said catalyst containing a titanium zeolite and carbonaceous material, the catalyst containing said carbonaceous material in an amount of from 0.01 to 0.5% by weight based on the total weight of titanium zeolite contained in the catalyst, the process comprising (i) preparing a catalyst containing the titanium zeolite and (ii) depositing carbonaceous material on the catalyst according to (i) in an amount of from 0.01 to 0.5% by weight based on the total weight of titanium zeolite contained in the catalyst by contacting said catalyst, prior to using the catalyst in said hydrocarbon conversion reaction, with a fluid containing at least one hydrocarbon in an inert atmosphere, to obtain the carbonaceous material containing catalyst, wherein in (ii), the catalyst is not contacted with an oxygen containing gas.
摘要翻译：一种用于制备用于烃转化反应的催化剂的方法，所述催化剂含有钛沸石和含碳材料，所述含碳材料的催化剂的含量为基于总重量的0.01-0.5重量％包含在催化剂中的钛沸石，该方法包括（i）制备含有钛沸石的催化剂和（ii）根据（i）在催化剂上沉积含碳材料，其量为基于总计的0.01至0.5重量％催化剂中含有的钛沸石的重量，在使用所述烃转化反应中的催化剂之前，使所述催化剂与在惰性气氛中含有至少一种烃的流体接触，得到含碳材料的催化剂，其中在（ii），催化剂不与含氧气体接触。

2. 发明申请

US20110130579A1 PROCESS FOR THE PREPARATION OF A TITANIUM ZEOLITE CATALYST 有权
标题翻译：制备钛酸钠催化剂的方法
公开(公告)号：US20110130579A1
公开(公告)日：2011-06-02
申请号：US12954802
申请日：2010-11-26
申请人： Ulrich MÜLLER , Peter Rudolf , Georg Krug , Rainer Senk
发明人： Ulrich MÜLLER , Peter Rudolf , Georg Krug , Rainer Senk
IPC分类号： C07D301/02 , B01J29/04 , B01J29/18 , B01J29/06
CPC分类号： B01J29/89 , B01J37/0018 , B01J37/084 , B01J2229/42 , C07D301/12
摘要： A process for the preparation of a catalyst for the use in a hydrocarbon conversion reaction, said catalyst containing a titanium zeolite and carbonaceous material, the catalyst containing said carbonaceous material in an amount of from 0.01 to 0.5% by weight based on the total weight of titanium zeolite contained in the catalyst, the process comprising (i) preparing a catalyst containing the titanium zeolite and (ii) depositing carbonaceous material on the catalyst according to (i) in an amount of from 0.01 to 0.5% by weight based on the total weight of titanium zeolite contained in the catalyst by contacting said catalyst, prior to using the catalyst in said hydrocarbon conversion reaction, with a fluid containing at least one hydrocarbon in an inert atmosphere, to obtain the carbonaceous material containing catalyst, wherein in (ii), the catalyst is not contacted with an oxygen containing gas.
摘要翻译：一种用于制备用于烃转化反应的催化剂的方法，所述催化剂含有钛沸石和含碳材料，所述含碳材料的催化剂的含量为基于总重量的0.01-0.5重量％包含在催化剂中的钛沸石，该方法包括（i）制备含有钛沸石的催化剂和（ii）根据（i）在催化剂上沉积含碳材料，其量为基于总计的0.01至0.5重量％催化剂中含有的钛沸石的重量，在使用所述烃转化反应中的催化剂之前，使所述催化剂与在惰性气氛中含有至少一种烃的流体接触，得到含碳材料的催化剂，其中在（ii），催化剂不与含氧气体接触。

3. 发明申请

US20100003173A1 METHOD FOR PRODUCING PROPYLENE OXIDE 有权
标题翻译：生产丙烯氧化物的方法
公开(公告)号：US20100003173A1
公开(公告)日：2010-01-07
申请号：US12556961
申请日：2009-09-10
申请人： Ulrich Müller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Göbbel , Peter Bassler
发明人： Ulrich Müller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Göbbel , Peter Bassler
IPC分类号： B01J8/02 , B01J29/06
CPC分类号： C07D301/12 , Y02P20/52
摘要： Process for preparing propylene oxide, which comprises at least the steps (i) and (ii): (i) providing a catalyst comprising at least one porous oxidic material; (ii) reacting propene with a hydroperoxide in at least one nitrile as solvent or in a solvent mixture comprising at least one nitrile in the presence of the catalyst of (i), wherein the at least one porous oxidic material is a zeolite which is assigned X-ray-crystallographically to the MWW type.
摘要翻译：制备环氧丙烷的方法，其至少包括步骤（i）和（ii）：（i）提供包含至少一种多孔氧化物质的催化剂; （ii）使丙烯与至少一种腈作为溶剂中的氢过氧化物反应或在包含至少一种腈的溶剂混合物中，在（i）的催化剂存在下反应，其中所述至少一种多孔氧化物质是被分配的沸石 X射线晶体学到MWW型。

4. 发明授权

US06884743B2 Catalyst for epoxidation reactions 失效
标题翻译：催化剂用于环氧化反应
公开(公告)号：US06884743B2
公开(公告)日：2005-04-26
申请号：US10243669
申请日：2002-09-16
申请人： Ulrich Müller , Georg Krug , Peter Bassler , Hans-Georg Göbbel , Peter Rudolf , Joaquim Henrique Teles
发明人： Ulrich Müller , Georg Krug , Peter Bassler , Hans-Georg Göbbel , Peter Rudolf , Joaquim Henrique Teles
IPC分类号： C07D303/04 , B01J29/89 , B01J37/04 , C01B39/06 , C01B39/40 , C07B61/00 , C07D301/12 , B01J29/06
CPC分类号： C07D301/12 , B01J29/89
摘要： The present invention relates to the manufacture of solid materials or shaped bodies containing at least one zeolite and being at least partly crystalline. Furthermore, the present invention relates to the solid materials or shaped bodies as such and to the use of these materials for reactions of compounds having at least one C—C double bond with at least one hydroperoxide. Specifically, the present invention relates to a process for the manufacture of a solid material containing at least one zeolite and being at least partly crystalline, wherein the synthesis of the said solid material involves at least one partial step of contacting at least one transition metal oxide source with at least one epoxide or hydrolysate thereof prior to or during the at least partial crystallization of said solid material.
摘要翻译：本发明涉及包含至少一种沸石并且至少部分结晶的固体材料或成形体的制造。此外，本发明还涉及固体材料或成形体，以及这些材料用于具有至少一个C-C双键的化合物与至少一种氢过氧化物的反应的用途。具体地说，本发明涉及制造含有至少一种沸石并且至少部分结晶的固体材料的方法，其中所述固体材料的合成涉及至少一个部分步骤，使至少一种过渡金属氧化物来源，其在所述固体材料的至少部分结晶之前或期间具有至少一种环氧化物或水解产物。

5. 发明授权

US08211822B2 Method for producing propylene oxide 有权
标题翻译：生产环氧丙烷的方法
公开(公告)号：US08211822B2
公开(公告)日：2012-07-03
申请号：US12556961
申请日：2009-09-10
申请人： Ulrich Mueller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Goebbel , Peter Bassler
发明人： Ulrich Mueller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Goebbel , Peter Bassler
IPC分类号： B01J21/06 , B01J21/08
CPC分类号： C07D301/12 , Y02P20/52
摘要： Process for preparing propylene oxide, which comprises at least the steps (i) and (ii): (i) providing a catalyst comprising at least one porous oxidic material; (ii) reacting propene with a hydroperoxide in at least one nitrile as solvent or in a solvent mixture comprising at least one nitrile in the presence of the catalyst of (i), wherein the at least one porous oxidic material is a zeolite which is assigned X-ray-crystallographically to the MWW type.
摘要翻译：制备环氧丙烷的方法，其至少包括步骤（i）和（ii）：（i）提供包含至少一种多孔氧化物质的催化剂; （ii）使丙烯与至少一种腈作为溶剂中的氢过氧化物反应或在包含至少一种腈的溶剂混合物中，在（i）的催化剂存在下反应，其中所述至少一种多孔氧化物质是被分配的沸石 X射线晶体学到MWW型。

6. 发明申请

US20050054865A1 Catalyst for epoxidation reactions 审中-公开
公开(公告)号：US20050054865A1
公开(公告)日：2005-03-10
申请号：US10938604
申请日：2004-09-13
申请人： Ulrich Muller , Georg Krug , Peter Bassler , Hans-Georg Gobbel , Peter Rudolf , Joaquim Teles
发明人： Ulrich Muller , Georg Krug , Peter Bassler , Hans-Georg Gobbel , Peter Rudolf , Joaquim Teles
IPC分类号： C07D303/04 , B01J29/89 , B01J37/04 , C01B39/06 , C01B39/40 , C07B61/00 , C07D301/12 , C07D301/06 , B01J29/04 , B01J29/87
CPC分类号： C07D301/12 , B01J29/89
摘要： The present invention relates to the manufacture of solid materials or shaped bodies containing at least one zeolite and being at least partly crystalline. Furthermore, the present invention relates to the solid materials or shaped bodies as such and to the use of these materials for reactions of compounds having at least one C—C double bond with at least one hydroperoxide. Specifically, the present invention relates to a process for the manufacture of a solid material containing at least one zeolite and being at least partly crystalline, wherein the synthesis of the said solid material involves at least one partial step of contacting at least one transition metal oxide source with at least one epoxide or hydrolysate thereof prior to or during the at least partial crystallization of said solid material.

7. 发明申请

US20060167286A1 Process for epoxidation and catalyst to be used therein 有权
标题翻译：环氧化方法和催化剂用于其中
公开(公告)号：US20060167286A1
公开(公告)日：2006-07-27
申请号：US10526939
申请日：2003-09-16
申请人： Ulrich Mueller , Georg Krug , Peter Bassler , Hans-Georg Gobbel , Peter Rudolf , Joaquim Teles
发明人： Ulrich Mueller , Georg Krug , Peter Bassler , Hans-Georg Gobbel , Peter Rudolf , Joaquim Teles
IPC分类号： B01J29/04 , C07D301/19
CPC分类号： C07D301/19 , B01J29/89 , B01J37/10 , B01J2229/36 , B01J2229/40 , C07D301/12 , Y02P20/125
摘要： The present invention relates to a process for treating a solid material containing at least one zeolite and being at least partly crystalline or treating a shaped body obtained from said solid material wherein said solid material or shaped body is brought in contact with a composition containing water after at least one of the following steps of an integrated process for producing a solid material or a shaped body containing at least one zeolite: (i) after step (II) of separating the at least partly crystalline solid material from its mother liquor or (ii) after step (S) of shaping said solid material into a shaped body or (iii) after a step (C) of calcining said solid material or said shaped body. The present invention furthermore relates to the solid material obtainable by the inventive process and the shaped body obtainable by the inventive process. The present invention also relates to the use of the solid material or the shaped body as mentioned above as a catalyst in chemical reactions, in particular in reactions of compounds containing at least one C-C double bond with at least one hydroperoxide.
摘要翻译：本发明涉及一种用于处理含有至少一种沸石并且至少部分结晶的固体材料或处理由所述固体材料获得的成形体的方法，其中所述固体材料或成形体与含有水的组合物接触用于生产固体材料或含有至少一种沸石的成形体的整合方法中的至少一个步骤：（i）在从母液中分离出至少部分结晶固体材料的步骤（II）之后，或（ii ）在将所述固体材料成形为成形体的步骤（S）之后或（iii）在煅烧所述固体材料或所述成形体的步骤（C）之后。本发明还涉及可通过本发明方法获得的固体材料和通过本发明方法获得的成形体。本发明还涉及如上所述的固体材料或成形体作为化学反应中的催化剂，特别是在含有至少一个C-C双键的化合物与至少一种氢过氧化物的反应中的用途。

8. 发明授权

US08119550B2 Process for epoxidation and catalyst to be used therein 有权
标题翻译：环氧化方法和催化剂用于其中
公开(公告)号：US08119550B2
公开(公告)日：2012-02-21
申请号：US10526939
申请日：2003-09-16
申请人： Ulrich Mueller , Georg Krug , Peter Bassler , Hans-Georg Goebbel , Peter Rudolf , Joaquim Henrique Teles
发明人： Ulrich Mueller , Georg Krug , Peter Bassler , Hans-Georg Goebbel , Peter Rudolf , Joaquim Henrique Teles
IPC分类号： B01J29/06 , C07D301/19
CPC分类号： C07D301/19 , B01J29/89 , B01J37/10 , B01J2229/36 , B01J2229/40 , C07D301/12 , Y02P20/125
摘要： The present invention relates to a process for treating a solid material containing at least one zeolite and being at least partly crystalline or treating a shaped body obtained from said solid material wherein said solid material or shaped body is brought in contact with a composition containing water after at least one of the following steps of an integrated process for producing a solid material or a shaped body containing at least one zeolite: (i) after step (II) of separating the at least partly crystalline solid material from its mother liquor or (ii) after step (S) of shaping said solid material into a shaped body or (iii) after a step (C) of calcining said solid material or said shaped body. The present invention furthermore relates to the solid material obtainable by the inventive process and the shaped body obtainable by the inventive process. The present invention also relates to the use of the solid material or the shaped body as mentioned above as a catalyst in chemical reactions, in particular in reactions of compounds containing at least one C-C double bond with at least one hydroperoxide.
摘要翻译：本发明涉及一种用于处理含有至少一种沸石并且至少部分结晶的固体材料或处理由所述固体材料获得的成形体的方法，其中所述固体材料或成形体与含有水的组合物接触用于生产固体材料或含有至少一种沸石的成形体的整合方法中的至少一个步骤：（i）在从母液中分离出至少部分结晶固体材料的步骤（II）之后，或（ii ）在将所述固体材料成形为成形体的步骤（S）之后或（iii）在煅烧所述固体材料或所述成形体的步骤（C）之后。本发明还涉及可通过本发明方法获得的固体材料和通过本发明方法获得的成形体。本发明还涉及如上所述的固体材料或成形体作为化学反应中的催化剂，特别是在含有至少一个C-C双键的化合物与至少一种氢过氧化物的反应中的用途。

9. 发明授权

US07608728B2 Method for producing propylene oxide 有权
标题翻译：生产环氧丙烷的方法
公开(公告)号：US07608728B2
公开(公告)日：2009-10-27
申请号：US10555961
申请日：2004-05-10
申请人： Ulrich Mueller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Goebbel , Peter Bassler
发明人： Ulrich Mueller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Goebbel , Peter Bassler
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , Y02P20/52
摘要： Process for preparing propylene oxide, which comprises at least the steps (i) and (ii): (i) providing a catalyst comprising at least one porous oxidic material; (ii) reacting propene with a hydroperoxide in at least one nitrile as solvent or in a solvent mixture comprising at least one nitrile in the presence of the catalyst of (i), wherein the at least one porous oxidic material is a zeolite which is assigned X-ray-crystallographically to the MWW type.
摘要翻译：制备环氧丙烷的方法，其至少包括步骤（i）和（ii）：（i）提供包含至少一种多孔氧化物质的催化剂; （ii）使丙烯与至少一种腈作为溶剂中的氢过氧化物反应或在包含至少一种腈的溶剂混合物中，在（i）的催化剂存在下反应，其中所述至少一种多孔氧化物质是被分配的沸石 X射线晶体学到MWW型。

10. 发明申请

US20070043226A1 Method for producing propylene oxide 有权
标题翻译：生产环氧丙烷的方法
公开(公告)号：US20070043226A1
公开(公告)日：2007-02-22
申请号：US10555961
申请日：2004-05-10
申请人： Ulrich Muller , Georg Krug , Peter Rudolf , Joaquim Teles , Hans-Georg Gobbel , Peter Bassler
发明人： Ulrich Muller , Georg Krug , Peter Rudolf , Joaquim Teles , Hans-Georg Gobbel , Peter Bassler
IPC分类号： C07D301/19
CPC分类号： C07D301/12 , Y02P20/52
摘要： Process for preparing propylene oxide, which comprises at least the steps (i) and (ii): (i) providing a catalyst comprising at least one porous oxidic material; (ii) reacting propene with a hydroperoxide in at least one nitrile as solvent or in a solvent mixture comprising at least one nitrile in the presence of the catalyst of (i), wherein the at least one porous oxidic material is a zeolite which is assigned X-ray-crystallographically to the MWW type.
摘要翻译：制备环氧丙烷的方法，其至少包括步骤（i）和（ii）：（i）提供包含至少一种多孔氧化物质的催化剂; （ii）使丙烯与至少一种腈作为溶剂中的氢过氧化物反应或在包含至少一种腈的溶剂混合物中，在（i）的催化剂存在下反应，其中所述至少一种多孔氧化物质是被分配的沸石 X射线晶体学到MWW型。

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