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1. 发明申请

US20150367253A1 PHOTOLUMINESCENT THIN-LAYER CHROMATOGRAPHY PLATE AND METHODS FOR MAKING SAME 审中-公开
标题翻译：光致变色薄层色谱板及其制备方法
公开(公告)号：US20150367253A1
公开(公告)日：2015-12-24
申请号：US14741376
申请日：2015-06-16
申请人： US SYNTHETIC CORPORATION , BRIGHAM YOUNG UNIVERSITY
发明人： Supriya Kanyal , Cody Vic Cushman , Matthew R. Linford , David Scott Jensen
IPC分类号： B01D15/38 , C23C16/455 , C23C16/34 , B01D15/20
CPC分类号： B01D15/3857 , B01D15/206 , C23C16/345 , C23C16/401 , C23C16/407 , C23C16/45525
摘要： In an embodiment, a method for manufacturing a chromatography apparatus such as a thin layer chromatography (“TLC”) plate is disclosed. The method includes forming a layer of elongated nanostructures (e.g., carbon nanotubes), and at least partially coating the oxidized elongated nanostructures with a coating. The coating includes a stationary phase and/or precursor of a stationary phase and at least one photoluminescent material for use in chromatography. Embodiments for TLC plates and related methods are also disclosed.
摘要翻译：在一个实施方式中，公开了薄层色谱（“TLC”）板等色谱装置的制造方法。该方法包括形成细长的纳米结构层（例如，碳纳米管），并且用涂层至少部分地涂覆氧化的细长纳米结构。涂层包括用于色谱法的固定相和/或固定相的前体和至少一种光致发光材料。还公开了TLC板的实施例和相关方法。

2. 发明授权

US09126227B2 Thin layer chromatography plates and related methods of manufacture including priming prior to infiltration with stationary phase and/or precursor thereof 有权
标题翻译：薄层色谱板和相关的制造方法，包括在用固定相和/或其前体渗透之前起泡
公开(公告)号：US09126227B2
公开(公告)日：2015-09-08
申请号：US14186996
申请日：2014-02-21
申请人： US SYNTHETIC CORPORATION , BRIGHAM YOUNG UNIVERSITY
发明人： Matthew R. Linford , David Scott Jensen , Andrew E. Dadson , Robert C. Davis
IPC分类号： B05D5/00 , C23C16/01 , C23C16/02 , C23C16/40 , C23C16/455 , B01J20/32 , G01N30/60 , G01N30/92 , B82Y30/00
CPC分类号： B01D15/10 , B01J20/283 , B01J20/284 , B01J20/3204 , B01J20/3223 , B01J20/3236 , B01J20/324 , B01J20/3259 , B01J20/3289 , B01J20/3297 , B01J2220/82 , B05D5/00 , B82Y30/00 , C23C16/01 , C23C16/0272 , C23C16/402 , C23C16/403 , C23C16/45555 , G01N30/6095 , G01N30/92
摘要： In an embodiment, a method for manufacturing a thin layer chromatography (“TLC”) plate is disclosed. The method includes forming a layer of elongated nanostructures (e.g., carbon nanotubes), priming the elongated nanostructures with one or more adhesion priming layers, and at least partially coating the elongated nanostructures with a coating. The coating includes a stationary phase and/or precursor of a stationary phase for use in chromatography. The stationary phase may be functionalized with hydroxyl groups by exposure to a base or acid. The stationary phase may further be treated with a silane (e.g., an amino silane) to improve the performance of the TLC plate. Embodiments for TLC plates and related methods are also disclosed.
摘要翻译：在一个实施方案中，公开了薄层色谱（“TLC”）板的制造方法。该方法包括形成细长的纳米结构层（例如，碳纳米管），用一个或多个粘合引发层引发细长的纳米结构，并用涂层至少部分地涂覆细长的纳米结构。涂层包括用于色谱法的固定相和/或固定相的前体。固定相可以通过暴露于碱或酸而被羟基官能化。可以用硅烷（例如氨基硅烷）进一步处理固定相，以改善TLC板的性能。还公开了TLC板的实施例和相关方法。

3. 发明申请

US20160038914A1 POROUS COMPOSITE PARTICULATE MATERIALS, METHODS OF MAKING AND USING SAME, AND RELATED APPARATUSES 审中-公开
标题翻译：多孔复合颗粒材料，制备和使用它们的方法和相关装置
公开(公告)号：US20160038914A1
公开(公告)日：2016-02-11
申请号：US14885909
申请日：2015-10-16
申请人： BRIGHAM YOUNG UNIVERSITY , US SYNTHETIC CORPORATION
发明人： Matthew R. Linford , Andrew E. Dadson , Landon A. Wiest , David S. Jensen
IPC分类号： B01J20/285 , B01D15/10 , B01J20/20 , B01J20/28 , B01J20/26
CPC分类号： B01J20/285 , B01D15/10 , B01J13/02 , B01J13/14 , B01J13/22 , B01J20/20 , B01J20/262 , B01J20/28004 , B01J20/28016 , B01J20/28057 , B01J20/282 , B01J20/286 , B01J20/3204 , B01J20/3223 , B01J20/3236 , B01J20/324 , B01J20/3268 , B01J20/3272 , B01J20/3282 , B01J20/3289 , B01J20/3293 , B01J20/3295 , B01J2220/52 , B01J2220/58
摘要： In an embodiment, a porous composite particulate material includes a plurality of composite particles. Each composite particle includes an acid-base-resistant core particle at least partially surrounded by one or more layers of acid-base-resistant shell particles. The shell particles are adhered to the core particle by a polymeric layer. The shell particles and/or core particles may be made from an acid-base-resistant material that is stable in harsh chemical conditions. For example, the shell particles and/or core particles may be made from diamond, graphitic carbon, silicon carbide, boron nitride, tungsten carbide, niobium carbide, zirconia, noble metals, acid-base stable highly cross-linked polymers, acid-base stable at least partially cross-linked polymers, titania, alumina, thoria combinations of the foregoing, or other acid-base-resistant materials. The porous composite particulate materials disclosed herein and related methods and devices may be used in separation technologies, including, but not limited to, chromatography and solid phase extraction.
摘要翻译：在一个实施方案中，多孔复合颗粒材料包括多个复合颗粒。每个复合颗粒包括至少部分地被一层或多层耐酸碱性壳颗粒包围的耐酸碱性芯颗粒。壳颗粒通过聚合物层粘附到芯颗粒。壳颗粒和/或芯颗粒可以由在苛刻的化学条件下稳定的耐酸碱材料制成。例如，壳颗粒和/或芯颗粒可以由金刚石，石墨碳，碳化硅，氮化硼，碳化钨，碳化铌，氧化锆，贵金属，酸碱稳定的高度交联的聚合物，酸碱稳定的至少部分交联的聚合物，二氧化钛，氧化铝，氧化钍组合，或其它耐酸碱材料。本文公开的多孔复合颗粒材料和相关方法和装置可以用于分离技术，包括但不限于色谱和固相萃取。

4. 发明申请

US20160030924A9 POROUS COMPOSITE PARTICULATE MATERIALS, METHODS OF MAKING AND USING SAME, AND RELATED APPARATUSES 审中-公开
标题翻译：多孔复合颗粒材料，制备和使用它们的方法和相关装置
公开(公告)号：US20160030924A9
公开(公告)日：2016-02-04
申请号：US14463525
申请日：2014-08-19
申请人： BRIGHAM YOUNG UNIVERSITY , US SYNTHETIC CORPORATION
发明人： David Scott Jensen , Andrew E. Dadson , Matthew R. Linford
IPC分类号： B01J20/32 , B01J20/281 , B01D15/26
CPC分类号： B01J20/3293 , B01D15/26 , B01J13/14 , B01J13/22 , B01J20/0211 , B01J20/0218 , B01J20/28004 , B01J20/28016 , B01J20/28019 , B01J20/28057 , B01J20/281 , B01J20/286 , B01J20/3204 , B01J20/3223 , B01J20/3234 , B01J20/3236 , B01J20/324 , B01J20/3268 , B01J20/3272 , B01J20/3282 , B01J20/3289 , B01J20/3295 , B01J2220/52 , B01J2220/58 , B01J2220/82
摘要： In an embodiment, a porous composite particulate material includes a plurality of composite particles. Each composite particle includes an acid-base-resistant core particle at least partially surrounded by one or more layers of acid-base-resistant shell particles. The shell particles are adhered to the core particle by a polymeric layer. The shell particles and/or core particles may be made from an acid-base-resistant material that is stable in harsh chemical conditions. For example, the shell particles may be made from diamond, graphitic carbon, silicon carbide, boron nitride, tungsten carbide, niobium carbide, zirconia, noble metals, combinations of the foregoing, or other acid-base-resistant materials and the core particle may include at least one exterior layer of non-diamond carbon. The porous composite particulate materials disclosed herein and related methods and devices may be used in separation technologies, including, but not limited to, chromatography and solid phase extraction.
摘要翻译：在一个实施方案中，多孔复合颗粒材料包括多个复合颗粒。每个复合颗粒包括至少部分地被一层或多层耐酸碱性壳颗粒包围的耐酸碱性芯颗粒。壳颗粒通过聚合物层粘附到芯颗粒。壳颗粒和/或芯颗粒可以由在苛刻的化学条件下稳定的耐酸碱材料制成。例如，壳颗粒可以由金刚石，石墨碳，碳化硅，氮化硼，碳化钨，碳化铌，氧化锆，贵金属，前述的组合或其它耐酸碱材料和芯颗粒制成包括至少一个非金刚石碳外层。本文公开的多孔复合颗粒材料和相关方法和装置可以用于分离技术，包括但不限于色谱和固相萃取。

5. 发明申请

US20150343326A1 THIN LAYER CHROMATOGRAPHY PLATES 审中-公开
标题翻译：薄层色谱板
公开(公告)号：US20150343326A1
公开(公告)日：2015-12-03
申请号：US14825019
申请日：2015-08-12
申请人： US SYNTHETIC CORPORATION , BRIGHAM YOUNG UNIVERSITY
发明人： Matthew R. Linford , David Scott Jensen , Andrew E. Dadson , Robert C. Davis
IPC分类号： B01D15/10 , B01J20/283 , C23C16/40 , C23C16/02 , C23C16/455 , G01N30/92 , B01J20/284
CPC分类号： B01D15/10 , B01J20/283 , B01J20/284 , B01J20/3204 , B01J20/3223 , B01J20/3236 , B01J20/324 , B01J20/3259 , B01J20/3289 , B01J20/3297 , B01J2220/82 , B05D5/00 , B82Y30/00 , C23C16/01 , C23C16/0272 , C23C16/402 , C23C16/403 , C23C16/45555 , G01N30/6095 , G01N30/92
摘要： In an embodiment, a method for manufacturing a thin layer chromatography (“TLC”) plate is disclosed. The method includes forming a layer of elongated nanostructures (e.g., carbon nanotubes), priming the elongated nanostructures with one or more adhesion priming layers, and at least partially coating the elongated nanostructures with a coating. The coating includes a stationary phase and/or precursor of a stationary phase for use in chromatography. The stationary phase may be functionalized with hydroxyl groups by exposure to a base or acid. The stationary phase may further be treated with a silane (e.g., an amino silane) to improve the performance of the TLC plate. Embodiments for TLC plates and related methods are also disclosed.
摘要翻译：在一个实施方案中，公开了薄层色谱（“TLC”）板的制造方法。该方法包括形成细长的纳米结构层（例如，碳纳米管），用一个或多个粘合引发层引发细长的纳米结构，并用涂层至少部分地涂覆细长的纳米结构。涂层包括用于色谱法的固定相和/或固定相的前体。固定相可以通过暴露于碱或酸而被羟基官能化。可以用硅烷（例如氨基硅烷）进一步处理固定相，以改善TLC板的性能。还公开了TLC板的实施例和相关方法。

6. 发明申请

US20140170311A1 THIN LAYER CHROMATOGRAPHY PLATES AND RELATED METHODS OF MANUFACTURE INCLUDING PRIMING PRIOR TO INFILTRATION WITH STATIONARY PHASE AND/OR PRECURSOR THEREOF 审中-公开
标题翻译：薄层色谱板和相关的制造方法，包括在其静置相和/或前驱体浸润之前的预处理
公开(公告)号：US20140170311A1
公开(公告)日：2014-06-19
申请号：US14186996
申请日：2014-02-21
申请人： BRIGHAM YOUNG UNIVERSITY , US SYNTHETIC CORPORATION
发明人： Matthew R. Linford , David Scott Jensen , Andrew E. Dadson , Robert C. Davis
IPC分类号： B05D5/00
CPC分类号： B01D15/10 , B01J20/283 , B01J20/284 , B01J20/3204 , B01J20/3223 , B01J20/3236 , B01J20/324 , B01J20/3259 , B01J20/3289 , B01J20/3297 , B01J2220/82 , B05D5/00 , B82Y30/00 , C23C16/01 , C23C16/0272 , C23C16/402 , C23C16/403 , C23C16/45555 , G01N30/6095 , G01N30/92
摘要： In an embodiment, a method for manufacturing a thin layer chromatography (“TLC”) plate is disclosed. The method includes forming a layer of elongated nanostructures (e.g., carbon nanotubes), priming the elongated nanostructures with one or more adhesion priming layers, and at least partially coating the elongated nanostructures with a coating. The coating includes a stationary phase and/or precursor of a stationary phase for use in chromatography. The stationary phase may be functionalized with hydroxyl groups by exposure to a base or acid. The stationary phase may further be treated with a silane (e.g., an amino silane) to improve the performance of the TLC plate. Embodiments for TLC plates and related methods are also disclosed.
摘要翻译：在一个实施方案中，公开了薄层色谱（“TLC”）板的制造方法。该方法包括形成细长的纳米结构层（例如，碳纳米管），用一个或多个粘合引发层引发细长的纳米结构，并用涂层至少部分地涂覆细长的纳米结构。涂层包括用于色谱法的固定相和/或固定相的前体。固定相可以通过暴露于碱或酸而被羟基官能化。可以用硅烷（例如氨基硅烷）进一步处理固定相，以改善TLC板的性能。还公开了TLC板的实施例和相关方法。

7. 发明申请

US20160158728A1 MODIFIED DIAMOND PARTICLES 审中-公开
公开(公告)号：US20160158728A1
公开(公告)日：2016-06-09
申请号：US15040771
申请日：2016-02-10
申请人： BRIGHAM YOUNG UNIVERSITY
发明人： Matthew R. Linford , Landon A. Wiest , David Jensen
IPC分类号： B01J20/32 , B01J20/286 , B01D15/20 , G01N1/40
CPC分类号： B01J20/3248 , B01D15/206 , B01D15/34 , B01D15/36 , B01D15/361 , B01D15/3804 , B01J20/286 , B01J20/287 , B01J20/3204 , B01J20/3244 , B01J20/3246 , B01J20/3251 , B01J20/3253 , G01N1/405 , Y10T428/2991
摘要： Modified diamond particles for use in chromatography with a desired functional group at the diamond surface, formed from reaction of hydroxyl groups at diamond surfaces with a reactive molecule.

8. 发明申请

US20150160173A1 THIN LAYER CHROMATOGRAPHY PLATES AND RELATED METHODS 审中-公开
标题翻译：薄层色谱板及相关方法
公开(公告)号：US20150160173A1
公开(公告)日：2015-06-11
申请号：US14619670
申请日：2015-02-11
申请人： Brigham Young University
发明人： Matthew R. Linford , Supriya Kanyal
IPC分类号： G01N30/93 , C01B31/02
CPC分类号： G01N30/93 , B01D15/10 , B01D15/26 , B01J20/28007 , B01J20/286 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/162 , C01B32/168 , G01N30/92
摘要： In an embodiment, a method for manufacturing a thin layer chromatography (“TLC”) plate is disclosed. The method includes forming a layer of elongated nanostructures (e.g., carbon nanotubes), and at least partially coating the elongated nanostructures with a coating including silicon nitride. At least a portion of the elongated nanostructures may be removed after being coated. The silicon nitride of the coating may be at least partially oxidized to form silicon dioxide.
摘要翻译：在一个实施方案中，公开了薄层色谱（“TLC”）板的制造方法。该方法包括形成细长的纳米结构层（例如，碳纳米管），并且用包括氮化硅的涂层至少部分地涂覆细长纳米结构。至少一部分细长的纳米结构可以在被涂覆之后被去除。涂层的氮化硅可以至少部分氧化形成二氧化硅。

9. 发明申请

US20140182771A1 SONICATION FOR IMPROVED PARTICLE SIZE DISTRIBUTION OF CORE-SHELL PARTICLES 审中-公开
标题翻译：用于改进核心颗粒粒度分布的通知
公开(公告)号：US20140182771A1
公开(公告)日：2014-07-03
申请号：US14152375
申请日：2014-01-10
申请人： BRIGHAM YOUNG UNIVERSITY
发明人： Matthew R. Linford , Chuan-Hsi Hung
IPC分类号： B32B38/00
CPC分类号： B32B38/0008 , B01J20/28004 , B01J20/286 , B01J20/3282 , B01J20/3289 , B01J20/3293 , B01J20/3295
摘要： In one or more embodiments, a porous composite particulate material includes a plurality of composite particles including an acid-base-resistant core particle at least partially surrounded by one or more layers of acid-base-resistant shell particles. The shell particles are adhered to the core particle by a polymeric material. The shell particles and/or core particles may be made from an acid-base-resistant material that is stable in harsh chemical conditions. During application of the polymeric material/shell particle bilayer, the core particles are sonicated to homogenize the particle size distribution and minimize agglomeration of particles. Multiple bilayers of polymer/shell particles may be applied. In one embodiment, the core particle comprises generally spherical glassy carbon, while the shell particles may comprise nano-sized diamond particles. Other acid-base-resistant materials may be employed. The porous composite particulate materials may be used in separation technologies, including, but not limited to, chromatography and solid phase extraction.
摘要翻译：在一个或多个实施方案中，多孔复合颗粒材料包括多个复合颗粒，其包括至少部分地被一层或多层耐酸碱性壳颗粒包围的耐酸碱性芯颗粒。壳颗粒通过聚合材料粘附到芯颗粒。壳颗粒和/或芯颗粒可以由在苛刻的化学条件下稳定的耐酸碱材料制成。在应用聚合物材料/壳粒子双层的过程中，超声处理核心颗粒以使颗粒尺寸分布均匀化并使颗粒的聚集最小化。可以应用多个双层的聚合物/壳颗粒。在一个实施方案中，芯颗粒包含通常为球形的玻璃碳，而壳颗粒可包含纳米尺寸的金刚石颗粒。可以使用其它耐酸碱的材料。多孔复合颗粒材料可用于分离技术，包括但不限于色谱和固相萃取。

10. 发明授权

US09511575B2 Sonication for improved particle size distribution of core-shell particles 有权
标题翻译：用于改善核 - 壳颗粒的粒度分布的超声处理
公开(公告)号：US09511575B2
公开(公告)日：2016-12-06
申请号：US14152375
申请日：2014-01-10
申请人： BRIGHAM YOUNG UNIVERSITY
发明人： Matthew R. Linford , Chuan-Hsi Hung
IPC分类号： B32B38/00 , B01J20/28 , B01J20/286 , B01J20/32
CPC分类号： B32B38/0008 , B01J20/28004 , B01J20/286 , B01J20/3282 , B01J20/3289 , B01J20/3293 , B01J20/3295
摘要： In one or more embodiments, a porous composite particulate material includes a plurality of composite particles including an acid-base-resistant core particle at least partially surrounded by one or more layers of acid-base-resistant shell particles. The shell particles are adhered to the core particle by a polymeric material. The shell particles and/or core particles may be made from an acid-base-resistant material that is stable in harsh chemical conditions. During application of the polymeric material/shell particle bilayer, the core particles are sonicated to homogenize the particle size distribution and minimize agglomeration of particles. Multiple bilayers of polymer/shell particles may be applied. In one embodiment, the core particle comprises generally spherical glassy carbon, while the shell particles may comprise nano-sized diamond particles. Other acid-base-resistant materials may be employed. The porous composite particulate materials may be used in separation technologies, including, but not limited to, chromatography and solid phase extraction.
摘要翻译：在一个或多个实施方案中，多孔复合颗粒材料包括多个复合颗粒，其包括至少部分地被一层或多层耐酸碱性壳颗粒包围的耐酸碱性芯颗粒。壳颗粒通过聚合材料粘附到芯颗粒。壳颗粒和/或芯颗粒可以由在苛刻的化学条件下稳定的耐酸碱材料制成。在应用聚合物材料/壳粒子双层的过程中，超声处理核心颗粒以使颗粒尺寸分布均匀化并使颗粒的聚集最小化。可以应用多个双层的聚合物/壳颗粒。在一个实施方案中，核心颗粒包含通常为球形的玻璃碳，而壳颗粒可包含纳米尺寸的金刚石颗粒。可以使用其它耐酸碱的材料。多孔复合颗粒材料可用于分离技术，包括但不限于色谱和固相萃取。

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