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1. 发明授权

US4604435A Thermosetting epoxy resin compositions 失效
标题翻译：热固性环氧树脂组合物
公开(公告)号：US4604435A
公开(公告)日：1986-08-05
申请号：US672052
申请日：1984-11-16
申请人： Taro Koshii , Yoshitsugu Morita , Hideo Shinmi , Tsuneo Hanada
发明人： Taro Koshii , Yoshitsugu Morita , Hideo Shinmi , Tsuneo Hanada
IPC分类号： C09D5/03 , C08G59/00 , C08G59/40 , C08G59/42 , C08L63/00 , C09D163/00 , C09J163/00 , H01B3/40 , H01L23/29 , H01L23/31 , C09J3/16
CPC分类号： C08G59/4223 , C08L63/00
摘要： What is disclosed are thermosetting epoxy resin compositions containing block siloxane copolymers which are used to induce low internal stress in the cured compositions and to provide coefficients of thermal expansion more closely aligned with the coefficients of thermal expansion of the substrates being molded therewith.
摘要翻译：所公开的是含有嵌段硅氧烷共聚物的热固性环氧树脂组合物，其用于在固化的组合物中诱导低内应力，并提供与其模塑的基材的热膨胀系数更紧密地对准的热膨胀系数。

2. 发明授权

US4293479A Heat curable molding composition 失效
标题翻译：热固性成型组合物
公开(公告)号：US4293479A
公开(公告)日：1981-10-06
申请号：US101324
申请日：1979-12-06
申请人： Tsuneo Hanada , Taro Koshii , Hideo Shinmi
发明人： Tsuneo Hanada , Taro Koshii , Hideo Shinmi
IPC分类号： C08L83/00 , C08G59/00 , C08K7/16 , C08K7/18 , C08K7/20 , C08L63/00 , C08L67/00 , C08L83/04
CPC分类号： C08K7/18 , C08K7/20
摘要： What is disclosed is an improved heat curable molding composition which has increased flowability in the mold. The improvement is gained by the use of a fine, spherical noncrystalline filler along with the normal molding compound fillers.
摘要翻译：所公开的是改进的可热固化的模塑组合物，其在模具中具有增加的流动性。通过使用细小的球形非晶态填料以及普通模塑料填料获得改进。

3. 再颁专利

USRE32958E Thermosetting epoxy resin compositions 失效
标题翻译：热固性环氧树脂组合物
公开(公告)号：USRE32958E
公开(公告)日：1989-06-20
申请号：US95970
申请日：1987-09-14
申请人： Taro Koshii , Yoshitsugu Morita , Hideo Shinmi , Tsuneo Hanada
发明人： Taro Koshii , Yoshitsugu Morita , Hideo Shinmi , Tsuneo Hanada
IPC分类号： C08L63/00
CPC分类号： C08L63/00
摘要： What is disclosed are thermosetting epoxy resin compositions containing block siloxane copolymers which are used to induce low internal stress in the cured compositions and to provide coefficients of thermal expansion more closely aligned with the coefficients of thermal expansion of the substrates being molded therewith.

4. 发明授权

US4144222A Thermosetting silicone resin molding composition 失效
标题翻译：热固性硅树脂成型组合物
公开(公告)号：US4144222A
公开(公告)日：1979-03-13
申请号：US820024
申请日：1977-07-28
申请人： Hideo Shinmi , Tsuneo Hanada
发明人： Hideo Shinmi , Tsuneo Hanada
IPC分类号： C08L83/00 , C08L83/04
CPC分类号： C08K5/57 , C08K3/0016 , C08G77/12 , C08G77/16 , C08G77/70
摘要： An improved thermosetting silicone resin molding composition characterized by consisting essentially of 100 parts by weight of organopolysiloxane resin having organic radical: Si ratio of 1.0:1 to 1.7:1 and containing at least 0.2% by weight of silicon-bonded hydroxyl groups, organohydrogenpolysiloxane containing at least one silicon bonded hydrogen atom in each molecule thereof, said organohydrogenpolysiloxane being in such an amount that the number of the hydrogen atoms per hydroxyl group in said organopolysiloxane is between 0.001 and 0.30, 0.01 to 15 parts by weight of organotin oxide, and 50 to 700 parts by weight of an inorganic filler.
摘要翻译：一种改进的热固性硅树脂模塑组合物，其特征在于基本上由100重量份的有机基团硅比率为1.0:1至1.7:1的有机聚硅氧烷树脂组成，并含有至少0.2重量％的与硅键合的羟基，含有有机基聚硅氧烷的有机氢聚硅氧烷含有每个分子中至少有一个硅键合的氢原子，所述有机氢聚硅氧烷的量使得所述有机聚硅氧烷中每个羟基的氢原子数为0.001至0.30,0.01至15重量份的有机锡氧化物，和50 至700重量份的无机填料。

5. 发明申请

US20090074990A1 Method for manufacturing optically anisotropic material 审中-公开
标题翻译：光学各向异性材料的制造方法
公开(公告)号：US20090074990A1
公开(公告)日：2009-03-19
申请号：US11918731
申请日：2005-05-26
申请人： Zemin Shi , Tadashi Akamatsu , Michio Sato , Tsuneo Hanada
发明人： Zemin Shi , Tadashi Akamatsu , Michio Sato , Tsuneo Hanada
IPC分类号： C09K19/00 , B05D5/06
CPC分类号： C09D4/00 , C08F220/42 , G02B5/3016 , G02B5/3083 , G02F1/13363 , Y10T428/10
摘要： When an optically anisotropic material is manufactured, an optically anisotropic liquid crystal layer with good adhesion properties and without irregular alignment is formed on a substrate. The optically anisotropic material having the optically anisotropic liquid crystal layer formed on the substrate can be manufactured by subjecting the surface of the substrate to rubbing treatment, subjecting the rubbing-treated surface to surface treatment with the hydrolysate of an alkoxysilane compound, applying a polymerizable nematic liquid crystal composition to the surface-treated surface, subjecting the applied polymerizable liquid crystal composition to alignment treatment, and subjecting the polymerizable liquid crystal composition to curing treatment while the alignment state thereof is maintained, whereby the optically anisotropic liquid crystal layer is formed.
摘要翻译：当制造光学各向异性材料时，在基板上形成具有良好粘附性且不规则排列的光学各向异性液晶层。具有形成在基板上的光学各向异性液晶层的光学各向异性材料可以通过对基板的表面进行摩擦处理，对经摩擦处理的表面进行表面处理，用烷氧基硅烷化合物的水解物进行表面处理，将液晶组合物涂布到表面处理表面，对涂布的聚合性液晶组合物进行取向处理，并且在保持取向状态的同时使聚合性液晶组合物进行固化处理，由此形成光学各向异性液晶层。

6. 发明授权

US07427363B2 Composition for forming liquid crystal film, optically anisotropic film, and production method thereof 有权
标题翻译：用于形成液晶膜的组合物，光学各向异性膜及其制备方法
公开(公告)号：US07427363B2
公开(公告)日：2008-09-23
申请号：US10581747
申请日：2004-08-31
申请人： Zemin Shi , Tadashi Akamatsu , Michio Sato , Tsuneo Hanada
发明人： Zemin Shi , Tadashi Akamatsu , Michio Sato , Tsuneo Hanada
IPC分类号： C09K19/00 , C09K19/52
CPC分类号： C09K19/3852 , C09K19/406 , C09K19/408 , C09K2019/328 , C09K2219/03 , Y10T428/10
摘要： A simple technique for introducing a hybrid alignment or a homeotropic (vertical) alignment into liquid crystal films, which, by their nature, tend to have a horizontal alignment of liquid crystal molecules. The technique does not require special alignment films.A liquid crystal composition for forming a liquid crystal film contains a polymerizable liquid crystal compound and a hydrolysate of an alkoxysilane compound. The hydrolysate of the alkoxysilane compound contains a siloxane oligomer of which degree of polymerization is from 2 to 25. Furthermore, the alkoxysilane compound is a trialkoxysilane compound having a functional group. This liquid crystal film composition can be produced by hydrolyzing an alkoxysilane compound to obtain a hydrolysate and then uniformly mixing the hydrolysate with a polymerizable liquid crystal compound. Alternatively, it can be obtained by uniformly mixing the alkoxysilane compound with the polymerizable liquid crystal compound and subsequently hydrolyzing the alkoxysilane compound in the mixture. One mole of the alkoxysilane compound is preferably hydrolyzed with 0.1 d to 2.0 d mol of water, given that the number of alkoxyl groups in a molecule of the alkoxysilane compound is d. An optically anisotropic film can be obtained by applying the liquid crystal film composition to a base film, causing the liquid crystal molecules in the composition to alignment in a nematic alignment, and curing the composition. The alignment of the liquid crystal molecules in the film is preferably a nematic hybrid or nematic hemeotropic (vertical) alignment.
摘要翻译：用于将混合取向或垂直（垂直）取向引入液晶膜的简单技术，其本质上倾向于具有液晶分子的水平取向。该技术不需要特殊的取向膜。用于形成液晶膜的液晶组合物含有可聚合液晶化合物和烷氧基硅烷化合物的水解产物。烷氧基硅烷化合物的水解物含有聚合度为2〜25的硅氧烷低聚物。此外，烷氧基硅烷化合物为具有官能团的三烷氧基硅烷化合物。该液晶膜组合物可以通过水解烷氧基硅烷化合物得到水解产物，然后将水解产物与可聚合液晶化合物均匀混合来制备。或者，可以通过将烷氧基硅烷化合物与可聚合液晶化合物均匀混合，然后水解该混合物中的烷氧基硅烷化合物而获得。考虑到烷氧基硅烷化合物分子中的烷氧基数为d，1摩尔烷氧基硅烷化合物优选用0.1d至2.0dmol的水进行水解。可以通过将液晶膜组合物施加到基膜上，使组合物中的液晶分子以向列取向取向并固化该组合物，从而获得光学各向异性膜。膜中的液晶分子的取向优选为向列混合或向列型共蒸发（垂直）取向。

7. 发明授权

US4517238A Method of making integral molded silicone products with different phases and the molded products prepared therefrom 失效
标题翻译：制备具有不同相的一体成型硅酮产品的方法和由其制备的模制产品
公开(公告)号：US4517238A
公开(公告)日：1985-05-14
申请号：US477206
申请日：1983-03-21
申请人： Katsutoshi Mine , Toshio Suzuki , Tsuneo Hanada
发明人： Katsutoshi Mine , Toshio Suzuki , Tsuneo Hanada
IPC分类号： C09K3/00 , B32B25/20 , B32B27/00 , C08J3/24 , C08L83/04 , C09D183/04 , H01B3/46 , H01L21/31 , H01L21/312 , B05D3/02 , B32B7/02
CPC分类号： C08J3/245 , C08L83/04 , C09D183/04 , C08G77/12 , C08G77/20 , C08G77/70 , C08J2383/04 , Y10T428/24942 , Y10T428/31536 , Y10T428/31612 , Y10T428/31663
摘要： Integral silicone molded products comprising a unitary structure of a substrate with different phases is made by coating a substrate with a mixture of an alkenyl containing polyorganosiloxane, a polyorganohydrogensiloxane, and an addition-reaction catalyst where at least one component is applied to the substrate and then additional components are applied and diffuse to result in a coating with a polyorganosiloxane phase whose degree of crosslinking is low and a polyorganosiloxane phase whose degree of crosslinking is high and the phase having the low degree of crosslinking is next to the substrate. Such molded products are coated hybrid IC transistors, solar battery modules, and optical fibers.
摘要翻译：通过用含有聚有机硅氧烷，聚有机氢硅氧烷和加成反应催化剂的混合物涂覆基材，制成包含具有不同相的基板的整体结构的整体硅酮模制产品，其中至少一种组分施加到基材上，然后另外的组分被施加和扩散以导致其交联度低的聚有机硅氧烷相的涂层和交联度高的交联度低的交联的相关的聚有机硅氧烷相与基板相邻。这种模制产品是涂覆的混合IC晶体管，太阳能电池模块和光纤。

8. 发明申请

US20070114491A1 Composition for forming liquid crystal film, optically anisotropic film, and production method thereof 有权
标题翻译：用于形成液晶膜的组合物，光学各向异性膜及其制备方法
公开(公告)号：US20070114491A1
公开(公告)日：2007-05-24
申请号：US10581747
申请日：2004-08-31
申请人： Zemin Shi , Tadashi Akamatsu , Michio Sato , Tsuneo Hanada
发明人： Zemin Shi , Tadashi Akamatsu , Michio Sato , Tsuneo Hanada
IPC分类号： C09K19/52 , C09K19/54 , C09K19/38
CPC分类号： C09K19/3852 , C09K19/406 , C09K19/408 , C09K2019/328 , C09K2219/03 , Y10T428/10
摘要： A simple technique for introducing a hybrid alignment or a homeotropic (vertical) alignment into liquid crystal films, which, by their nature, tend to have a horizontal alignment of liquid crystal molecules. The technique does not require special alignment films. A liquid crystal composition for forming a liquid crystal film contains a polymerizable liquid crystal compound and a hydrolysate of an alkoxysilane compound. The hydrolysate of the alkoxysilane compound contains a siloxane oligomer of which degree of polymerization is from 2 to 25. Furthermore, the alkoxysilane compound is a trialkoxysilane compound having a functional group. This liquid crystal film composition can be produced by hydrolyzing an alkoxysilane compound to obtain a hydrolysate and then uniformly mixing the hydrolysate with a polymerizable liquid crystal compound. Alternatively, it can be obtained by uniformly mixing the alkoxysilane compound with the polymerizable liquid crystal compound and subsequently hydrolyzing the alkoxysilane compound in the mixture. One mole of the alkoxysilane compound is preferably hydrolyzed with 0.1d to 2.0d mol of water, given that the number of alkoxyl groups in a molecule of the alkoxysilane compound is d. An optically anisotropic film can be obtained by applying the liquid crystal film composition to a base film, causing the liquid crystal molecules in the composition to align in a nematic alignment, and curing the composition. The alignment of the liquid crystal molecules in the film is preferably a nematic hybrid or nematic homeotropic (vertical) alignment.
摘要翻译：用于将混合取向或垂直（垂直）取向引入液晶膜的简单技术，其本质上倾向于具有液晶分子的水平取向。该技术不需要特殊的取向膜。用于形成液晶膜的液晶组合物含有可聚合液晶化合物和烷氧基硅烷化合物的水解产物。烷氧基硅烷化合物的水解物含有聚合度为2〜25的硅氧烷低聚物。此外，烷氧基硅烷化合物为具有官能团的三烷氧基硅烷化合物。该液晶膜组合物可以通过水解烷氧基硅烷化合物得到水解产物，然后将水解产物与可聚合液晶化合物均匀混合来制备。或者，可以通过将烷氧基硅烷化合物与可聚合液晶化合物均匀混合，然后水解该混合物中的烷氧基硅烷化合物而获得。考虑到烷氧基硅烷化合物的分子中的烷氧基数为d，一摩尔烷氧基硅烷化合物优选用0.1d至2.0dmol的水进行水解。可以通过将液晶膜组合物施加到基膜上，使组合物中的液晶分子以向列取向取向并固化该组合物来获得光学各向异性膜。膜中液晶分子的取向优选为向列混合或向列垂面（垂直）取向。

9. 发明授权

US4594134A Method for preparing a spherical cured polymer or a composition thereof containing linear organopolysiloxane blocks 失效
标题翻译：制备球形固化聚合物的方法或其包含线性有机聚硅氧烷嵌段的组合物
公开(公告)号：US4594134A
公开(公告)日：1986-06-10
申请号：US670369
申请日：1984-11-09
申请人： Tsuneo Hanada , Yoshitsugu Morita
发明人： Tsuneo Hanada , Yoshitsugu Morita
IPC分类号： C08J3/12 , C08L63/00 , C08L83/04 , C08L83/10 , C08F2/46
CPC分类号： C08J3/12 , C08L63/00 , C08L83/04 , C08L83/10 , C08G77/42 , C08G77/70 , C08J2383/00 , Y10S528/901
摘要： Provided is a method for preparing a spherical cured product having a diameter of 5 mm or less of a polymer or a polymer composition containing at least 10 wt % of the linear organopolysiloxane blocks represented by the following general formula (1), characterized by curing in an atomized state a curable polymer or a curable polymer composition containing at least 10 wt % of the linear organopolysiloxane blocks represented by the following general formula (1):--R.sub.2 SiO].sub.n (1)wherein R's are the same or different monovalent hydrocarbon groups and n is an integer of 5 or more.
摘要翻译：提供一种制备直径为5mm以下的聚合物或含有至少10重量％的由以下通式（1）表示的直链有机聚硅氧烷嵌段的聚合物组合物的球形固化产品的方法，其特征在于固化在雾化状态，包含至少10重量％的由以下通式（1）表示的直链有机聚硅氧烷嵌段的可固化聚合物或可固化聚合物组合物：-R2SiO] n（1）其中R是相同或不同的一价烃基和 n为5以上的整数。

10. 发明授权

US4267297A Room temperature curable silicone resins 失效
标题翻译：室温固化硅树脂
公开(公告)号：US4267297A
公开(公告)日：1981-05-12
申请号：US86559
申请日：1979-10-19
申请人： Tsuneo Hanada , Ryuzo Mikami
发明人： Tsuneo Hanada , Ryuzo Mikami
IPC分类号： C08L83/04 , C09D183/04 , C08L83/06 , C08G77/16 , C08G77/18
CPC分类号： C08L83/04 , C09D183/04 , C08G77/16 , C08G77/18
摘要： What is disclosed are room temperature curable silicone resins which have solvent, heat and weather resistance, mold release properties and water repellency in their cured state. Silicone resins are treated with alkoxylated siloxanes, alkoxysilanes and aminoalkoxysilanes to give these properties.
摘要翻译：所公开的是在其固化状态下具有溶剂，耐热和耐候性，脱模性和拒水性的室温可固化有机硅树脂。硅氧烷树脂用烷氧基化硅氧烷，烷氧基硅烷和氨基烷氧基硅烷处理，得到这些性质。

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