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1. 发明授权

US4414111A Shaped composite adsorbent and a process for preparing the same 失效
标题翻译：成型复合吸附剂及其制备方法
公开(公告)号：US4414111A
公开(公告)日：1983-11-08
申请号：US385410
申请日：1982-05-17
申请人： Toshiyuki Iwaisako , Akio Inoue
发明人： Toshiyuki Iwaisako , Akio Inoue
IPC分类号： B01J39/08 , B01J20/26 , B01J20/28 , B01J20/32 , B01J41/08 , B01J47/00 , B05D3/10 , B05D5/00
CPC分类号： B01J47/007 , B01J20/321 , B01J20/3236 , B01J20/3238 , B01J20/3265 , Y10T428/24355 , Y10T428/249986 , Y10T428/265 , Y10T428/268
摘要： A shaped composite adsorbent made of a shaped porous material of a skin-core structure comprising a powdery ion-exchange type adsorbent and an ionic group-containing acrylonitrile polymer and wherein said shaped porous material has a semi-permeable skin layer of 0.01 to 1.mu. in thickness and a void volume rate of 50 to 90%, which is capable of adsorbing solutes present at low concentration with high selectivity and high yield. The shaped composite adsorbent of the present invention can be obtained by a process comprising dissolving an ionic group-containing acrylonitrile polymer in and dispersing a powdery ion exchange type adsorbent in an inorganic solvent for said acrylonitrile polymer, extruding the resultant into a coagulating liquid bath to effect coagulation-shaping thereof. The adsorption capacity and mechanical strength of the shaped composite adsorbent of the present invention can be further improved by subjecting the above-obtained coagulation-shaped material to heat treatment in a wet state, without drying.
摘要翻译： PCT No.PCT / JP81 / 00379 Sec。 371日期1982年5月17日 102（e）日期1982年5月17日PCT提交1981年12月15日PCT公布。公开号WO82 / 02006 日本1982年6月24日。一种由包含粉末状离子交换型吸附剂和含离子性基团的丙烯腈聚合物的皮肤芯结构的成形多孔材料制成的成形复合吸附剂，其中所述成形多孔材料具有半渗透性表皮层的厚度为0.01〜1μm，空隙体积率为50〜90％，能够以高选择性和高收率吸附低浓度的溶质。本发明的成形复合吸附剂可以通过以下方法获得，该方法包括将含离子基团的丙烯腈聚合物溶解并分散在用于所述丙烯腈聚合物的无机溶剂中并将粉末状离子交换型吸附剂分散，将所得物挤出到凝固液浴中其凝固成型。本发明的成型复合吸附剂的吸附能力和机械强度可以通过对上述得到的凝固形状的材料进行湿润处理而不干燥而进一步改善。

2. 发明授权

US4003752A Magnesia cement composition, process of its manufacture, and composite comprising same 失效
标题翻译：氧化镁水泥组合物，其制造方法和包含其的复合材料
公开(公告)号：US4003752A
公开(公告)日：1977-01-18
申请号：US579068
申请日：1975-05-20
申请人： Susumu Isohata , Kazutaka Watabe , Morio Shimoshimizu , Toshiyuki Iwaisako
发明人： Susumu Isohata , Kazutaka Watabe , Morio Shimoshimizu , Toshiyuki Iwaisako
IPC分类号： B32B13/04 , C04B28/30 , E04C2/04 , C04B9/04
CPC分类号： E04C2/044 , B32B13/04 , C04B28/30
摘要： A magnesia cement composition comprising active magnesia, magnesium sulfate, and pulp or a mixture of pulp and fibrous glass. When hardened, this composition yields a crack-free low-shrinkage material. Valuable composite boards are obtained by lamination from the hardened composition and core materials such as cellular concrete, plywood, plastic foam, gypsum plaster board, and cemented excelsior board.
摘要翻译：包含活性氧化镁，硫酸镁和纸浆或纸浆和纤维状玻璃的混合物的氧化镁水泥组合物。当硬化时，该组合物产生无裂纹的低收缩材料。通过从硬化组合物和多孔混凝土，胶合板，塑料泡沫，石膏板和胶合板等芯材层压得到有价值的复合板。

3. 发明授权

US4381397A Method for synthesizing trioxane 失效
公开(公告)号：US4381397A
公开(公告)日：1983-04-26
申请号：US233414
申请日：1981-02-11
申请人： Koichi Yoshida , Toshiyuki Iwaisako , Junzo Masamoto , Katsuhiko Hamanaka , Hajime Komaki
发明人： Koichi Yoshida , Toshiyuki Iwaisako , Junzo Masamoto , Katsuhiko Hamanaka , Hajime Komaki
IPC分类号： B01J23/00 , B01J23/22 , B01J23/28 , B01J23/30 , B01J27/00 , B01J27/18 , C07B61/00 , C07D323/06
CPC分类号： C07D323/06
摘要： A method for synthesizing trioxane by heating and reacting an aqueous formaldehyde solution in the presence of a heteropolyacid. As the heteropolyacid, there is preferably used one that contains, as a coordinating element or coordinating elements, W, Mo, V or Nb alone or two or more of them.

4. 发明授权

US4120943A Process for producing pseudo-boehmite 失效
标题翻译：制造假勃姆石的方法
公开(公告)号：US4120943A
公开(公告)日：1978-10-17
申请号：US751683
申请日：1976-12-17
申请人： Toshiyuki Iwaisako , Naomi Yamaguchi , Hisao Yomogida , Yoshinobu Ito
发明人： Toshiyuki Iwaisako , Naomi Yamaguchi , Hisao Yomogida , Yoshinobu Ito
IPC分类号： C01F7/14 , B01J20/08 , B01J35/10 , B01J37/22 , C01F7/34 , C01F7/02
CPC分类号： C01F7/34 , B01J20/08 , B01J35/002 , B01J35/0026 , B01J35/023 , B01J35/1047 , B01J35/1076 , B01J37/22 , B01J35/1019
摘要： Pseudo-boehmite having a bulk density of about 0.05 to 0.2 g/cc, an oil absorption of about 2.5 to 6.0 cc/g, a pore volume of about 2.0 to 7.0 cc/g over a pore diameter range of 176.mu. to 0.0035.mu. and a specific surface area of about 200 to 500 m.sup.2 /g, and a process for producing the same; useful as a filler, an absorbent, a catalyst, a filtering agent and a base material for composites; prepared by mixing alkali aluminate and halohydrin together at a low temperature, heating for reaction the resulting mixture, cooling the reacting solution, separating the resulting precipitate by filtration and, if desired subjecting the precipitate to washing with an organic solvent followed by drying.
摘要翻译：堆积密度为约0.05〜0.2g / cc，油吸收量为约2.5〜6.0cc / g，孔径为176〜0.0035μm的孔体积为约2.0〜7.0cc / g的假勃姆石比表面积为约200〜500m 2 / g，及其制造方法。用作填料，吸收剂，催化剂，过滤剂和用于复合材料的基材; 通过在低温下将碱金属铝酸盐和卤代醇混合在一起制备，加热以使所得混合物反应，冷却反应溶液，通过过滤分离所得沉淀物，如果需要，用有机溶剂洗涤沉淀物，然后干燥。

5. 发明授权

US4563536A Method for synthesizing trioxane 失效
标题翻译：三恶烷合成方法
公开(公告)号：US4563536A
公开(公告)日：1986-01-07
申请号：US425040
申请日：1982-09-27
申请人： Koichi Yoshida , Toshiyuki Iwaisako , Junzo Masamoto , Katsuhiko Hamanaka , Hajime Komaki
发明人： Koichi Yoshida , Toshiyuki Iwaisako , Junzo Masamoto , Katsuhiko Hamanaka , Hajime Komaki
IPC分类号： B01J23/00 , B01J23/22 , B01J23/28 , B01J23/30 , B01J27/00 , B01J27/18 , C07B61/00 , C07D323/06
CPC分类号： C07D323/06
摘要： A method for synthesizing trioxane by heating and reacting an aqueous formaldehyde solution in the presence of a heteropolyacid. As the heteropolyacid, there is preferably used one that contains, as a coordinating element or coordinating elements, W, Mo, V or Nb alone or two or more of them.
摘要翻译：一种通过在杂多酸存在下加热和使甲醛水溶液反应来合成三恶烷的方法。作为杂多酸，优选使用含有作为配位元素或配位元素的单独的W，Mo，V或Nb或它们中的两种或更多种的那些。

6. 发明授权

US4493752A Process for recovering trioxane by plural distillation 失效
标题翻译：通过多次蒸馏回收三恶烷的方法
公开(公告)号：US4493752A
公开(公告)日：1985-01-15
申请号：US371461
申请日：1982-04-23
申请人： Takeshi Naito , Junzo Masamoto , Toshiyuki Iwaisako , Kazuhiko Matsuzaki
发明人： Takeshi Naito , Junzo Masamoto , Toshiyuki Iwaisako , Kazuhiko Matsuzaki
IPC分类号： C07D323/06 , C08G2/28 , B01D3/14
CPC分类号： C07D323/06 , C08G2/28
摘要： A process for recovering trioxane from an aqueous solution containing trioxane and triethylamine by the distillation separation process which comprises feeding an aqueous solution containing trioxane and triethylamine to the first distillation column, distilling out triethylamine, trioxane and water from the column top of the first distillation column, withdrawing an aqueous solution containing the major part of the trioxane present in the fed solution from the column bottom of the first distillation column, feeding the withdrawn solution to the second distillation column and taking out the substantially whole quantity of the trioxane fed to the second distillation column from the column top of the second distillation column.
摘要翻译：一种通过蒸馏分离方法从含有三恶烷和三乙胺的水溶液中回收三恶烷的方法，该方法包括将含有三恶烷和三乙胺的水溶液加入到第一蒸馏塔中，从第一蒸馏塔的塔顶馏出三乙胺，三恶烷和水从第一蒸馏塔的塔底排出含有进料溶液中存在的主要部分三恶烷的水溶液，将排出的溶液送入第二蒸馏塔，并取出大量全部量的三恶烷，蒸馏塔从第二蒸馏塔的塔顶。

7. 发明授权

US4436900A Process for deactivating polymerization catalyst 失效
标题翻译：聚合催化剂失活的方法
公开(公告)号：US4436900A
公开(公告)日：1984-03-13
申请号：US479385
申请日：1983-03-28
申请人： Kazuhiko Matsuzaki , Toshiyuki Iwaisako , Junzo Masamoto
发明人： Kazuhiko Matsuzaki , Toshiyuki Iwaisako , Junzo Masamoto
IPC分类号： C08G2/00 , C08G2/18 , C08G2/28
CPC分类号： C08G2/28
摘要： An oxymethylene copolymer produced from trioxane, a cyclic ether and/or a cyclic formal in the presence of a cationic polymerization catalyst is contacted with a deactivating agent for the catalyst in the state of gas phase at a temperature of 160.degree. C. or lower to deactivate the cationic polymerization catalyst rapidly and completely without causing degradation of the copolymer produced.
摘要翻译：在阳离子聚合催化剂存在下，由三恶烷，环醚和/或环状缩甲醛制备的甲醛共聚物在气相状态下与催化剂的钝化剂在160℃或更低至快速且完全地使阳离子聚合催化剂失活而不会引起共聚物的降解。

8. 发明授权

US4332644A Process for separating trioxane 失效
标题翻译：三恶烷分离方法
公开(公告)号：US4332644A
公开(公告)日：1982-06-01
申请号：US271250
申请日：1981-06-08
申请人： Katsuhiko Hamanaka , Toshiyuki Iwaisako , Junzo Masamoto , Koichi Yoshida
发明人： Katsuhiko Hamanaka , Toshiyuki Iwaisako , Junzo Masamoto , Koichi Yoshida
IPC分类号： B01D3/34 , C07D323/06 , B01D11/04
CPC分类号： C07D323/06 , B01D3/34
摘要： In a process for separating trioxane by a continuous distillation which comprises extracting, with benzene, the trioxane-containing distillate obtainable by heating an aqueous solution of formaldehyde, feeding the trioxane-containing benzene solution into a distillation column as a starting material, distilling out the benzene from the column top and withdrawing the trioxane from the column bottom, a process for separating trioxane which comprises retaining the concentration of trioxane X in the liquid composition at the starting material feeding plate of the distillation column (% by weight of trioxane based on the total liquid composition at the feeding plate) in the range satisfying the following relationship: ##EQU1## wherein R is reflux ratio, and .gamma. is a parameter defined by the following equation: ##EQU2## wherein q is the proportion of liquid part in the fed starting material as expressed in terms of ratio by weight and C (%) is the concentration of trioxane in the fed starting material.
摘要翻译：在通过连续蒸馏分离三恶烷的方法中，其包括用苯提取可通过加热甲醛水溶液获得的含三烷烃的馏出物，将含三恶烷的苯溶液作为起始原料进料到蒸馏塔中，蒸馏出苯，从塔底抽出三恶烷，分离三恶烷的方法，该方法包括在蒸馏塔的起始原料进料板中保持液体组合物中三恶烷X的浓度（基于三恶烷的重量％（1）其中R是回流比，γ是由下式定义的参数：其中q 是供料起始原料中液体部分的比例，以重量比表示，C（％）是三恶烷的浓度饲料原料。

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