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1. 发明授权

US07408085B2 Rapid cost effective method for the synthesis of TPD-type arylamines 有权
标题翻译：用于合成TPD型芳基胺的快速成本有效的方法
公开(公告)号：US07408085B2
公开(公告)日：2008-08-05
申请号：US11563937
申请日：2006-11-28
申请人： Timothy P. Bender , Jennifer A. Coggan , Gregory McGuire , Leanne Dawn Murphy , Alan Edward John Toth
发明人： Timothy P. Bender , Jennifer A. Coggan , Gregory McGuire , Leanne Dawn Murphy , Alan Edward John Toth
IPC分类号： C07C209/18 , C07C211/33
CPC分类号： C07C209/10 , C07C211/55
摘要： A process for forming a tetra(aryl)-biphenyldiamine compound, including reacting a dibromobiphenyl compound and a diarylamine compound in the presence of a palladium ligated catalyst and a base.
摘要翻译：一种形成四（芳基） - 联苯二胺化合物的方法，包括在钯连接的催化剂和碱的存在下使二溴联苯化合物和二芳基胺化合物反应。

2. 发明授权

US07803959B2 Synthesis of aromatic silicon-containing compounds 有权
标题翻译：芳香族含硅化合物的合成
公开(公告)号：US07803959B2
公开(公告)日：2010-09-28
申请号：US11278769
申请日：2006-04-05
申请人： Jennifer A. Coggan , Timothy P. Bender , Alan Edward John Toth
发明人： Jennifer A. Coggan , Timothy P. Bender , Alan Edward John Toth
IPC分类号： C07F7/18
CPC分类号： G03G5/14708 , G03G5/0578 , G03G5/0605 , G03G5/0614 , G03G5/062 , G03G5/078 , G03G5/14773 , G03G15/75
摘要： Methods are provided for preparing aromatic silicon-containing compounds. The methods include providing an aromatic starting material; reacting the aromatic starting material with a base to form an aromatic salt; and reacting the aromatic salt with a halo-alkylene-silane to form an aromatic silicon-containing compound. Compositions prepared by these methods, protective layers that include hydrolysis and condensation products of such compositions, electrophotographic photoreceptors that include such protective layers, and image forming apparatuses that include such electrophotographic photoreceptors are also provided. In addition, method for preparing electrophotographic photoreceptors that include protective layers including hydrolysis and condensation products of aromatic silicon-containing compounds prepared by the methods for preparing aromatic silicon-containing compounds are provided.
摘要翻译：提供制备芳香族含硅化合物的方法。所述方法包括提供芳族起始原料; 使芳族起始原料与碱反应形成芳族盐; 并使芳族盐与卤代 - 亚烷基 - 硅烷反应，形成芳香族含硅化合物。还提供了通过这些方法制备的组合物，包括这些组合物的水解和缩合产物，包括这种保护层的电子照相感光体的保护层和包括这种电子照相感光体的图像形成装置。此外，提供了制备包含通过制备芳香族含硅化合物的方法制备的芳香族含硅化合物的水解和缩合产物的保护层的电子照相感光体的制备方法。

3. 发明授权

US07321021B2 Removing impurities from polythiophene 有权
标题翻译：从聚噻吩中除去杂质
公开(公告)号：US07321021B2
公开(公告)日：2008-01-22
申请号：US11085215
申请日：2005-03-22
申请人： Alan Edward John Toth , Tamara Perez-Cruz
发明人： Alan Edward John Toth , Tamara Perez-Cruz
IPC分类号： C08G75/00
CPC分类号： C08G61/126
摘要： Impurities are removed from polythiophene by mixing a composition comprising polythiophene, water and an organic liquid at a temperature at which the organic liquid dissolves the polythiophene; allowing an aqueous phase to separate from an organic phase and recovering organic phase; adding water to recovered organic phase and mixing the resulting composition at a temperature at which the organic liquid dissolves the polythiophene; allowing an aqueous phase to separate from an organic phase and recovering organic phase; and allowing polythiophene solid to precipitate from recovered organic phase.
摘要翻译：通过在有机液体溶解聚噻吩的温度下混合包含聚噻吩，水和有机液体的组合物，从聚噻吩除去杂质; 允许水相与有机相分离并回收有机相; 在回收的有机相中加水并在有机液体溶解聚噻吩的温度下混合所得组合物; 允许水相与有机相分离并回收有机相; 并使聚噻吩固体从回收的有机相中沉淀出来。

4. 发明申请

US20120049163A1 Continuous Process For Preparing Nanodispersions Using An Ultrasonic Flow-Through Heat Exchanger 有权
标题翻译：使用超声波流通换热器制备纳米分散体的连续工艺
公开(公告)号：US20120049163A1
公开(公告)日：2012-03-01
申请号：US12872240
申请日：2010-08-31
申请人： Alan Edward John Toth , Santiago Faucher , Yiliang Wu , Marko Saban
发明人： Alan Edward John Toth , Santiago Faucher , Yiliang Wu , Marko Saban
IPC分类号： H01L51/10 , B06B1/00 , H01L51/40 , H01B1/12
CPC分类号： C08J3/09 , C08G2261/3223 , C08J2365/00 , C08J2400/00 , C08L65/00 , C09D11/30 , C09D11/52 , H01L51/0003 , H01L51/0007 , H01L51/0036 , H01L51/0545 , H01L51/0558
摘要： Described is a continuous process for preparing nanodispersions including providing a composition comprising a liquid and a solute; heating the composition to dissolution of the solute to form a solution comprising the solute dissolved in the liquid; directing the heated solution through a continuous tube wherein the continuous tube has a first end for receiving the solution, a continuous flow-through passageway disposed in an ultrasonic heat exchanger, and a second end for discharging a product stream; treating the heated solution as the solution passes through the continuous flow-through passageway disposed in the ultrasonic heat exchanger to form the product stream comprising nanometer size particles in the liquid; optionally, collecting the product stream in a product receiving vessel; and optionally, filtering the product stream.
摘要翻译：描述了制备纳米分散体的连续方法，包括提供包含液体和溶质的组合物; 将组合物加热以溶解溶质以形成溶解在液体中的溶质; 将加热的溶液引导通过连续管，其中连续管具有用于接收溶液的第一端，设置在超声波热交换器中的连续流通通道和用于排出产物流的第二端; 当溶液通过设置在超声波热交换器中的连续流通通道时处理加热的溶液，以形成在液体中包含纳米尺寸颗粒的产物流; 任选地，将产物流收集在产品接收容器中; 并且可选地，过滤产品流。

5. 发明授权

US08759421B2 Continuous process for preparing nanodispersions using an ultrasonic flow-through heat exchanger 有权
标题翻译：使用超声波流通热交换器制备纳米分散体的连续方法
公开(公告)号：US08759421B2
公开(公告)日：2014-06-24
申请号：US12872240
申请日：2010-08-31
申请人： Alan Edward John Toth , Santiago Faucher , Yiliang Wu , Marko Saban
发明人： Alan Edward John Toth , Santiago Faucher , Yiliang Wu , Marko Saban
IPC分类号： C08G59/42
CPC分类号： C08J3/09 , C08G2261/3223 , C08J2365/00 , C08J2400/00 , C08L65/00 , C09D11/30 , C09D11/52 , H01L51/0003 , H01L51/0007 , H01L51/0036 , H01L51/0545 , H01L51/0558
摘要： Described is a continuous process for preparing nanodispersions including providing a composition comprising a liquid and a solute; heating the composition to dissolution of the solute to form a solution comprising the solute dissolved in the liquid; directing the heated solution through a continuous tube wherein the continuous tube has a first end for receiving the solution, a continuous flow-through passageway disposed in an ultrasonic heat exchanger, and a second end for discharging a product stream; treating the heated solution as the solution passes through the continuous flow-through passageway disposed in the ultrasonic heat exchanger to form the product stream comprising nanometer size particles in the liquid; optionally, collecting the product stream in a product receiving vessel; and optionally, filtering the product stream.
摘要翻译：描述了制备纳米分散体的连续方法，包括提供包含液体和溶质的组合物; 将组合物加热以溶解溶质以形成溶解在液体中的溶质; 将加热的溶液引导通过连续管，其中连续管具有用于接收溶液的第一端，设置在超声波热交换器中的连续流通通道和用于排出产物流的第二端; 当溶液通过设置在超声波热交换器中的连续流通通道时处理加热的溶液，以形成在液体中包含纳米尺寸颗粒的产物流; 任选地，将产物流收集在产品接收容器中; 并且可选地，过滤产品流。

6. 发明授权

US07314908B2 Polythiophene processes 有权
标题翻译：聚噻吩工艺
公开(公告)号：US07314908B2
公开(公告)日：2008-01-01
申请号：US11281514
申请日：2005-11-18
申请人： Alan Edward John Toth , Tamara Perez-Cruz
发明人： Alan Edward John Toth , Tamara Perez-Cruz
IPC分类号： C08F6/00
CPC分类号： C08G61/126
摘要： Polythiophene may be processed using a method including providing a composition including the polythiophene and a liquid including at least one hydrocarbon having at least 6 carbon atoms; heating the composition to a temperature of at least about 50° C.; and separating solid polythiophene from the heated composition. Alternatively, the method may include providing a composition including polythiophene and an organic liquid; heating the composition to dissolve a portion of the polythiophene in the organic liquid; and separating solid polythiophene from the heated composition.
摘要翻译：聚噻吩可以使用包括提供包含聚噻吩的组合物和包含至少一种具有至少6个碳原子的烃的液体的方法进行处理; 将组合物加热至至少约50℃的温度; 并从加热的组合物中分离固体聚噻吩。或者，该方法可以包括提供包含聚噻吩和有机液体的组合物; 加热组合物以溶解有机液体中的一部分聚噻吩; 并从加热的组合物中分离固体聚噻吩。

7. 发明授权

US07816469B2 Process for producing polymer nanodispersions 有权
标题翻译：生产聚合物纳米分散体的方法
公开(公告)号：US07816469B2
公开(公告)日：2010-10-19
申请号：US11609651
申请日：2006-12-12
申请人： Alan Edward John Toth
发明人： Alan Edward John Toth
IPC分类号： C08F34/04 , C08L81/00
CPC分类号： C08J3/14 , C08J3/09 , C08J2365/00 , C08L65/00
摘要： This disclosure is generally directed to a batch process of producing semi-conductive polymer nanodispersions in which a composition comprising a liquid and a polymer is at least partially dissolved in the liquid, resulting in dissolved polymer molecules in the composition, wherein the dissolution occurs in a dissolution vessel. The solubility of the dissolved polymer molecules in the composition is then increased to increase the concentration of dissolved polymer in the composition to a range from about 0.1% to about 30% based on a total weight of the polymer and the liquid, wherein increasing the solubility of the dissolved polymer in the composition occurs in a dissolution vessel. The dissolved polymer in the composition is then diluted with a diluent, wherein the dissolution of the dissolved polymer in the composition occurs by addition of the composition to the diluent in a precipitation vessel.
摘要翻译：本公开一般涉及制备半导体聚合物纳米分散体的分批方法，其中包含液体和聚合物的组合物至少部分地溶解在液体中，导致组合物中溶解的聚合物分子，其中溶解发生在溶解容器然后增加溶解的聚合物分子在组合物中的溶解度，从而将组合物中溶解的聚合物的浓度增加到基于聚合物和液体的总重量的约0.1％至约30％的范围，其中增加溶解度的溶解聚合物在溶解容器中发生。然后将组合物中溶解的聚合物用稀释剂稀释，其中溶解的聚合物在组合物中的溶解是通过在沉淀容器中向稀释剂中加入组合物而发生的。

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