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1. 发明授权

US06552114B2 Process for preparing a high barrier amorphous polyamide-clay nanocomposite 失效
标题翻译：制备高阻隔无定形聚酰胺 - 粘土纳米复合材料的方法
公开(公告)号：US06552114B2
公开(公告)日：2003-04-22
申请号：US10144427
申请日：2002-05-13
申请人： Sam Richard Turner , Gary Wayne Connell , John Walker Gilmer , Vasiliki Psihogios , James Christopher Matayabas, Jr. , Tie Lan , Shriram Bagrodia
发明人： Sam Richard Turner , Gary Wayne Connell , John Walker Gilmer , Vasiliki Psihogios , James Christopher Matayabas, Jr. , Tie Lan , Shriram Bagrodia
IPC分类号： C08K334
CPC分类号： C08K9/04 , C08K3/346 , C08K7/00 , Y10S977/778 , Y10S977/788 , Y10S977/895 , Y10S977/902 , C08L77/00
摘要： This invention relates to a process for preparing an amorphous polyamide-clay nanocomposite comprising the steps of: a. melt mixing a layered clay material with an oligomeric polyamide resin to form an oligomeric polyamide resin-clay composite, and b. mixing the oligomeric resin-clay composite with a high molecular weight amorphous matrix polyamide comprising (i) a residue of at least two dicarboxylic acid components and (ii) a residue of at least one diamine component, wherein the layered clay material has been cation exchanged with an onium cation of the formula:
摘要翻译：本发明涉及一种制备无定形聚酰胺 - 粘土纳米复合材料的方法，包括以下步骤：a。将层状粘土材料与低聚聚酰胺树脂熔融混合以形成低聚聚酰胺树脂 - 粘土复合材料，和b。将低聚树脂 - 粘土复合材料与高分子量无定形基质聚酰胺混合，其中包括（i）至少两种二羧酸组分的残余物和（ii）至少一种二胺组分的残余物，其中层状粘土材料已经被阳离子交换具有下式的鎓阳离子：

2. 发明授权

US06417262B1 High barrier amorphous polyamide-clay nanocomposite and a process for preparing same 失效
标题翻译：高阻隔无定形聚酰胺 - 粘土纳米复合材料及其制备方法
公开(公告)号：US06417262B1
公开(公告)日：2002-07-09
申请号：US09452826
申请日：1999-12-01
申请人： Sam Richard Turner , Gary Wayne Connell , John Walker Gilmer , Vasiliki Psihogios , James Christopher Matayabas, Jr. , Tie Lan , Shriram Bagrodia
发明人： Sam Richard Turner , Gary Wayne Connell , John Walker Gilmer , Vasiliki Psihogios , James Christopher Matayabas, Jr. , Tie Lan , Shriram Bagrodia
IPC分类号： C08K334
CPC分类号： C08J3/226 , B82Y30/00 , C08J5/005 , C08J2367/02 , C08J2377/06 , C08K3/346 , C08K7/00 , C08K9/04 , C08L101/00 , C08L2666/02 , C08L77/00
摘要： This invention is directed to a polyamide-clay nanocomposite, products produced from the nanocomposite, and a process for preparing a polyamide-clay nanocomposite. The polyamide-clay nanocomposite comprises (a) an amorphous matrix polyamide comprising (i) a residue of a dicarboxylic acid component comprising at least two diacids and (ii) a residue of a diamine component, and (b) a layered clay material, wherein the layered clay material is dispersed in the matrix polyamide.
摘要翻译：本发明涉及聚酰胺 - 粘土纳米复合材料，由纳米复合材料制备的产品，以及制备聚酰胺 - 粘土纳米复合材料的方法。聚酰胺 - 粘土纳米复合材料包含（a）无定形基质聚酰胺，其包含（i）包含至少两种二酸的二羧酸组分的残基和（ii）二胺组分的残余物，和（b）层状粘土材料，其中层状粘土材料分散在基质聚酰胺中。

3. 发明授权

US06552113B2 Polymer-clay nanocomposite comprising an amorphous oligomer 失效
公开(公告)号：US06552113B2
公开(公告)日：2003-04-22
申请号：US09728954
申请日：2000-12-01
申请人： Shriram Bagrodia , Linda Gail Bernard , Gary Wayne Connell , John Walker Gilmer , Tie Lan , James Christopher Matayabas, Jr. , Jeffrey Todd Owens , Vasiliki Psihogios , Emerson Eston Sharpe, Jr. , Sam Richard Turner
发明人： Shriram Bagrodia , Linda Gail Bernard , Gary Wayne Connell , John Walker Gilmer , Tie Lan , James Christopher Matayabas, Jr. , Jeffrey Todd Owens , Vasiliki Psihogios , Emerson Eston Sharpe, Jr. , Sam Richard Turner
IPC分类号： B32B1706
CPC分类号： B82Y30/00 , C08J5/005 , C08K7/00 , C08K9/04 , Y10T428/1352
摘要： This invention is directed to a polymer-clay nanocomposite, products produced from the nanocomposite, and a process for preparing a polymer-clay nanocomposite. The polymer-clay nanocomposite comprises (a) a matrix polymer, (b) an amorphous oligomer, and (c) a layered clay material.

4. 发明授权

US06376591B1 High barrier amorphous polyamide-clay intercalates, exfoliates, and nanocomposite and a process for preparing same 有权
标题翻译：高阻隔无定形聚酰胺 - 粘土插层剂，去角质剂和纳米复合材料及其制备方法
公开(公告)号：US06376591B1
公开(公告)日：2002-04-23
申请号：US09452511
申请日：1999-12-01
申请人： Tie Lan , Vasiliki Psihogios , Sam Richard Turner , Gary Wayne Connell , James Christopher Matayabas, Jr. , John Walker Gilmer
发明人： Tie Lan , Vasiliki Psihogios , Sam Richard Turner , Gary Wayne Connell , James Christopher Matayabas, Jr. , John Walker Gilmer
IPC分类号： C08K334
CPC分类号： C08K3/346 , C08K7/00 , C08K9/08 , C08L77/00
摘要： This invention is directed to a polyamide-clay nanocomposite, products produced from the nanocomposite, and a process for preparing a polyamide-clay nanocomposite. The polyamide-clay nanocomposite comprises (a) an amorphous matrix polyamide comprising (i) a residue of a dicarboxylic acid component comprising at least two diacids and (ii) a residue of a diamine component, and (b) a layered clay material, wherein the layered clay material is dispersed in the matrix polyamide.
摘要翻译：本发明涉及聚酰胺 - 粘土纳米复合材料，由纳米复合材料制备的产品，以及制备聚酰胺 - 粘土纳米复合材料的方法。聚酰胺 - 粘土纳米复合材料包含（a）无定形基质聚酰胺，其包含（i）包含至少两种二酸的二羧酸组分的残基和（ii）二胺组分的残余物，和（b）层状粘土材料，其中层状粘土材料分散在基质聚酰胺中。

5. 发明授权

US06486252B1 Nanocomposites for high barrier applications 失效
标题翻译：用于高屏障应用的纳米复合材料
公开(公告)号：US06486252B1
公开(公告)日：2002-11-26
申请号：US09338222
申请日：1999-06-22
申请人： Robert Boyd Barbee , James Christopher Matayabas, Jr. , Jack Wesley Trexler, Jr. , Rodney Layne Piner , John Walker Gilmer , Gary Wayne Connell , Jeffrey Todd Owens , Sam Richard Turner
发明人： Robert Boyd Barbee , James Christopher Matayabas, Jr. , Jack Wesley Trexler, Jr. , Rodney Layne Piner , John Walker Gilmer , Gary Wayne Connell , Jeffrey Todd Owens , Sam Richard Turner
IPC分类号： C08J510
CPC分类号： C01B33/44 , C08K9/04
摘要： The present invention relates to a composition comprising (i) a layered clay material that has been cation-exchanged with an organic cation salt represented by Formula (I): wherein M is nitrogen or phosphorous, X− is a halide, hydroxide, or acetate anion, R1 is a straight or branched alkyl group having at least 8 carbon atoms, and R2, R3, and R4 are independently hydrogen or a straight or branched alkyl group having 1 to 22 carbon atoms; and (ii) at least one expanding agent, wherein the cation-exchanged clay material contains platelet particles and the expanding agent separates the platelet particles. The present invention also relates to a composite comprising a polymer having dispersed therein a composition of this invention. Preferred polymers for use in the composite include polyesters. The composite of the present invention shows vastly improved platelet separation as evidenced by higher than previously reported basal spacing.
摘要翻译：本发明涉及一种组合物，其包含（i）与式（I）表示的有机阳离子盐进行阳离子交换的层状粘土材料：其中M为氮或磷，X-为卤化物，氢氧化物或乙酸盐阴离子，R1是具有至少8个碳原子的直链或支链烷基，R2，R3和R4独立地是氢或具有1至22个碳原子的直链或支链烷基; 和（ii）至少一种发泡剂，其中所述阳离子交换的粘土材料含有血小板颗粒，所述发泡剂分离所述血小板颗粒。本发明还涉及包含其中分散有本发明组合物的聚合物的复合材料。用于复合材料的优选聚合物包括聚酯。本发明的复合物显示出大大改善的血小板分离，这通过高于先前报道的基础间距来证明。

6. 发明授权

US06713547B2 Process for preparing high barrier nanocomposites 失效
标题翻译：制备高阻隔纳米复合材料的方法
公开(公告)号：US06713547B2
公开(公告)日：2004-03-30
申请号：US10092128
申请日：2002-03-06
申请人： Robert Boyd Barbee , James Christopher Matayabas, Jr. , Jack Wesley Trexler, Jr. , Rodney Layne Piner , John Walker Gilmer , Gary Wayne Connell , Jeffrey Todd Owens , Sam Richard Turner
发明人： Robert Boyd Barbee , James Christopher Matayabas, Jr. , Jack Wesley Trexler, Jr. , Rodney Layne Piner , John Walker Gilmer , Gary Wayne Connell , Jeffrey Todd Owens , Sam Richard Turner
IPC分类号： C08J510
CPC分类号： C01B33/44 , C08K9/04
摘要： The present invention relates to processes for preparing a nanocomposite comprising: a. preparing an organoclay material by reacting a swellable layered clay with an onium ion represented by Formula (I): wherein i) M is nitrogen or phosphorus, ii) R1 is a straight or branched alkyl group having at least 8 carbon atoms, iii) R2, R3, and R4 are independently selected from organic or oligomeric ligands or hydrogen, and iv) at least one of R2, R3, and R4 comprises an alkylene oxide group having from 2 to 6 carbon atoms or a polyalkylene oxide group, and b. melt mixing the organoclay material with an expanding agent, and c. melt extruding the expanded organoclay and a polymer to provide a nanocomposite.
摘要翻译：本发明涉及制备纳米复合材料的方法，包括：a。通过使可溶胀的层状粘土与由式（I）表示的鎓离子反应来制备有机粘土材料：其中i）M是氮或磷，ii）R 1是具有至少8个碳原子的直链或支链烷基，iii）R 2， R 3和R 4独立地选自有机或低聚配体或氢，并且其中R 2，R 3和R 4中的至少一个包含具有2至6个碳原子的环氧烷基或聚环氧烷基，和b。将有机粘土材料与发泡剂熔融混合，和c。熔融挤出膨胀的有机粘土和聚合物以提供纳米复合材料。

7. 发明授权

US6084019A High I.V. polyester compositions containing platelet particles 失效
标题翻译：高I.V. 含有血小板颗粒的聚酯组合物
公开(公告)号：US6084019A
公开(公告)日：2000-07-04
申请号：US996063
申请日：1997-12-22
申请人： James Christopher Matayabas, Jr. , Sam Richard Turner , Bobby Jones Sublett , Gary Wayne Connell , John Walker Gilmer , Robert Boyd Barbee
发明人： James Christopher Matayabas, Jr. , Sam Richard Turner , Bobby Jones Sublett , Gary Wayne Connell , John Walker Gilmer , Robert Boyd Barbee
IPC分类号： C08L67/02 , C08K7/00 , C08K3/34
CPC分类号： C08K7/00 , Y10T428/1397 , Y10T428/261 , Y10T428/268 , Y10T428/269
摘要： The present invention relates to polyester-platelet particle composite compositions comprising about 0.01 to about 25 weight percent platelet particles dispersed in at least one polyester wherein said composition has an I.V. of greater than about 0.55 dl/g, low shear melt viscosity greater than about 30,000 poise and a gas permeability which is at least 10% lower than that of unmodified polyester and processes for producing same.
摘要翻译：本发明涉及包含分散在至少一种聚酯中的约0.01至约25重量％的血小板颗粒的聚酯 - 血小板颗粒复合组合物，其中所述组合物具有I.V. 大于约0.55dl / g，低剪切熔体粘度大于约30,000泊，气体渗透性比未改性聚酯低至少10％及其制备方法。

8. 发明授权

US07230065B2 Blends of polycarbonate and sulfone copolyesters 失效
公开(公告)号：US07230065B2
公开(公告)日：2007-06-12
申请号：US11179406
申请日：2005-07-12
申请人： Wesley Raymond Hale , Sam Richard Turner , Gary Wayne Connell
发明人： Wesley Raymond Hale , Sam Richard Turner , Gary Wayne Connell
IPC分类号： C08G63/00
CPC分类号： C08L67/02 , C08K5/49 , C08L69/00 , C08L2666/18
摘要： The present invention relates to miscible blends of the polycarbonate of bisphenol A and polyesters from aromatic dicarboxylic acids, 1,4-cyclohexanedimethanol, ethylene glycol, and 2,2′-(sulfonylbis(4,1-phenyleneoxy)-bis(ethanol).

9. 发明授权

US07025925B2 Extrusion blow molded articles 失效
标题翻译：挤出吹塑制品
公开(公告)号：US07025925B2
公开(公告)日：2006-04-11
申请号：US10812203
申请日：2004-03-29
申请人： Thomas Joseph Pecorini , Sam Richard Turner , Gary Wayne Connell
发明人： Thomas Joseph Pecorini , Sam Richard Turner , Gary Wayne Connell
IPC分类号： B29C49/04 , B65D1/00
CPC分类号： B29C49/0005 , B29C49/04 , B29K2067/00 , B29L2031/7126 , C08G63/199 , Y10T428/1352
摘要： Disclosed is a process for the manufacture of shaped articles by extrusion blow molding comprising the steps of (1) extruding a copolyester through a die to form a tube of molten copolyester; (2) positioning a mold having the desired finished shape around the tube of molten copolyester; and (3) introducing a gas into the tube of molten copolyester, causing the extrudate to stretch and expand to fill the mold; wherein the copolyester is a linear, copolyester having an inherent viscosity (IV) of at least about 0.7 dL/g measured at a temperature of 25° C. at 0.5 g/dL concentration in a solvent mixture of symmetric tetrachloroethane and phenol having a weight ratio of symmetric tetrachloroethane to phenol of 2:3 and comprising: (1) a diacid component consisting essentially of 90 to 100 mole percent terephthalic acid residues and 0 to about 10 mole percent isophthalic acid residues, naphthalenedicarboxylic acid residues, biphenyldicarboxylic acid residues or a combination of 2 or more of isophthalic, naphthalenedicarboxylic or bipheyldicarboxylic acid residues; and (2) a diol component consisting essentially of about 70 to 90 mole percent 1,4-cyclohexanedimethanol residues and about 30 to 10 mole percent neopentyl glycol residues; wherein the copolyester comprises 100 mole percent diacid component and 100 mole percent diol component. The process is particularly useful for the manufacture of bottles or carboys having and interior volume of about 2 to 50 liters.
摘要翻译：公开了一种通过挤出吹塑成型制造成形制品的方法，包括以下步骤：（1）通过模具挤出共聚酯以形成熔融共聚聚酯管; （2）将具有所需成品形状的模具定位在熔融共聚聚酯管上; 和（3）将气体引入熔融共聚酯的管中，使挤出物拉伸膨胀以填充模具; 其中所述共聚酯是具有至少约0.7dL / g的特性粘度（IV）为至少约0.7dL / g的线性共聚酯，其在25℃的温度下以0.5g / dL的浓度在对称四氯乙烷和具有重量的酚的溶剂混合物中测量对称四氯乙烷与苯酚的比例为2:3，包括：（1）基本上由90至100摩尔％对苯二甲酸残基和0至约10摩尔％间苯二甲酸残基组成的二酸组分，萘二甲酸残基，联苯二羧酸残基或 2个或更多个间苯二甲酸，萘二羧酸或二硫代二羧酸残基的组合; 和（2）基本上由约70至90摩尔％的1,4-环己烷二甲醇残基和约30至10摩尔％的新戊二醇残基组成的二醇组分; 其中所述共聚酯包含100摩尔％的二酸组分和100摩尔％的二醇组分。该方法对于制造具有约2至50升的内部容积的瓶子或者碳罐特别有用。

10. 发明授权

US06444283B1 Polyester-polyamide blends with reduced gas permeability and low haze 有权
标题翻译：聚酯 - 聚酰胺共混物具有降低的透气性和低雾度
公开(公告)号：US06444283B1
公开(公告)日：2002-09-03
申请号：US09628623
申请日：2000-07-31
申请人： Sam Richard Turner , Gary Wayne Connell , Steven Lee Stafford , John David Hewa
发明人： Sam Richard Turner , Gary Wayne Connell , Steven Lee Stafford , John David Hewa
IPC分类号： C08L7700
CPC分类号： C08L67/02 , Y10T428/1352 , C08L77/00
摘要： The invention relates to polyester/polyamide blend compositions for forming an article having low haze and reduced gas permeability compared to the polyester alone. More specifically, the invention relates to blends of semi-crystalline polyesters such as PET with low molecular weight polyamides and to the containers and packages for food, beverages, cosmetics, pharmaceuticals and personal care products that can be fabricated from these blends.
摘要翻译：本发明涉及用于形成与单独的聚酯相比具有低雾度和降低的透气性的制品的聚酯/聚酰胺共混物组合物。更具体地，本发明涉及半结晶聚酯如PET与低分子量聚酰胺的共混物，以及可以由这些共混物制造的用于食品，饮料，化妆品，药物和个人护理产品的容器和包装。

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