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    • 5. 发明授权
    • Process for the epoxidation of olefins
    • 烯烃环氧化方法
    • US06720436B2
    • 2004-04-13
    • US10384217
    • 2003-03-07
    • Willi HofenGeorg ThieleThomas HaasWolfgang WöllPercy KampeisBärbel Kolbe
    • Willi HofenGeorg ThieleThomas HaasWolfgang WöllPercy KampeisBärbel Kolbe
    • C07D30112
    • C07D301/12
    • A process for the catalytic epoxidation of olefins in at least one reaction stage comprising: (a) reacting the olefin with hydrogen peroxide in an organic, water-miscible solvent in the presence of a titanium silicalite catalyst in a reactor while continuously feeding an inert gas stream into the reactor, (b) continuously removing an exit gas stream containing olefin oxide, unreacted olefin, oxygen and inert gas from the reactor, (c) bringing the exit gas stream into contact in an absorption unit with the same solvent as used in the reaction stage, (d) removing a solvent stream loaded with olefin and olefin oxide from the absorption unit and (e) discharging an gas stream containing oxygen and the inert gas from the absorption unit.
    • 一种用于在至少一个反应阶段中对烯烃进行催化环氧化的方法,包括:(a)在反应器中在钛硅沸石催化剂存在下,使烯烃与有机的水混溶性溶剂中的过氧化氢反应,同时连续进料惰性气体 (b)从反应器中连续除去含有烯烃氧化物,未反应的烯烃,氧和惰性气体的出口气流,(c)使出口气流与吸收单元中的相同溶剂接触, 反应阶段,(d)从吸收单元除去负载有烯烃和烯烃氧化物的溶剂流,和(e)从吸收单元排出含有氧和惰性气体的气流。
    • 9. 发明授权
    • Process for the recovery of combustible components of a gas stream
    • 用于回收气流的可燃组分的方法
    • US06749668B2
    • 2004-06-15
    • US10174549
    • 2002-06-18
    • Willi HofenGeorg ThieleWolfgang Wöll
    • Willi HofenGeorg ThieleWolfgang Wöll
    • B01D5314
    • B01D53/14
    • A process for the recovery of combustible components of a gas stream containing the combustible components and oxygen by selective absorption of the combustible components in a solvent, whereby during the absorption the gas phase is dispersed in a continuous liquid phase of the solvent. In a preferred embodiment the process is applied to give a process for the epoxidation of propene with hydrogen peroxide in the alcoholic solvent in presence of a catalyst, wherein a gas stream including unreacted propene, propene oxide and oxygen from the decomposition of the hydrogen peroxide is separated from the epoxidation reaction mixture and the combustible components in said gas stream are recovered using the process as described above.
    • 通过在溶剂中选择性吸收可燃组分来回收含有可燃组分和氧的气流的可燃组分的方法,由此在吸收期间气相分散在溶剂的连续液相中。 在优选的实施方案中,应用该方法以在催化剂存在下,在醇溶剂中用过氧化氢环氧化丙烯的方法,其中包含未反应的丙烯,氧化丙烯和来自过氧化氢分解的氧的气流是 与环氧化反应混合物分离,并使用上述方法回收所述气流中的可燃组分。