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1. 发明授权

US09629378B2 Dispersion of phytosterols 有权
公开(公告)号：US09629378B2
公开(公告)日：2017-04-25
申请号：US13202862
申请日：2010-01-29
申请人： Thomas Francis Harting Glade , Miguel Angel Fuenzalida Diaz , Alejandro Markovits Rojas
发明人： Thomas Francis Harting Glade , Miguel Angel Fuenzalida Diaz , Alejandro Markovits Rojas
IPC分类号： A61K31/575 , A61P3/06 , A23D7/005 , A23C9/13 , A23C9/152 , A23L27/60 , A23L33/11
CPC分类号： A23D7/0056 , A23C9/13 , A23C9/152 , A23C2240/10 , A23D7/0053 , A23L27/60 , A23L33/11
摘要： The invention relates to a method for the production of highly stable aqueous dispersions of phytosterols, phytostanols and derivatives thereof, which allows the use of a wide range of emulsifiers in relatively small concentrations in relation to the phytosterols and which allows the preparation of dispersions with high concentrations of phytosterols. Said dispersions are obtained using a method in which one or more phytosterols, an aqueous medium and one or more emulsifiers are dispersed in a disperser at a temperature of at least 140° C. in order to obtain an emulsion and the resulting emulsion is subsequently cooled in order to obtain a dispersion of sterols in an aqueous medium.

2. 发明授权

US08258330B1 Carrier fluid composition comprising fatty acids ethyl esters and process for reducing the concentration of persistent organic pollutants in fish oil 有权
标题翻译：包含脂肪酸乙酯的载体流体组合物和用于降低鱼油中持久性有机污染物浓度的方法
公开(公告)号：US08258330B1
公开(公告)日：2012-09-04
申请号：US13343348
申请日：2012-01-04
申请人： Thomas Francis Harting Glade , Miguel Angel Fuenzalida Diaz , Alejandro Markovits Rojas
发明人： Thomas Francis Harting Glade , Miguel Angel Fuenzalida Diaz , Alejandro Markovits Rojas
IPC分类号： C11B3/00
CPC分类号： C11B3/006 , C11B3/001 , C11B3/12
摘要： Carrier fluid compositions and their use in processes for reducing the concentration of persistent organic pollutants, such as polychlorodibenzo-p-dioxins (PCDDs), polychlorodibenzo-p-furans (PCDDF), polychlorinated biphenyls (PCBs), polybrominated diphenyl ethers (PBDEs), polycyclic aromatic hydrocarbons (PAHs), and pesticides, such as chlorinated hydrocarbons, chlorinated toxaphenes and camphenes, in fish oil are disclosed. The process includes vacuum distillation of the fish oil in the presence of the carrier fluid compositions to provide a fish oil residue having a reduced concentration of persistent organic pollutants.
摘要翻译：载体流体组合物及其用于降低持久性有机污染物浓度的方法，如多氯二苯并对二恶英（PCDD），多氯二苯并呋喃（PCDDF），多氯联苯（PCBs），多溴二苯醚（PBDEs）公开了多环芳烃（PAHs），以及鱼油中的氯化烃类，氯化硝酸酯类和胡椒类等农药。该方法包括在载体流体组合物存在下对鱼油进行真空蒸馏以提供具有降低的持久性有机污染物浓度的鱼油残余物。

3. 发明授权

US08957231B2 Concentrate of omega 3 有权
标题翻译：浓缩的欧米茄3
公开(公告)号：US08957231B2
公开(公告)日：2015-02-17
申请号：US13994785
申请日：2011-12-25
申请人： Juvenal Antonio Sepulveda Reyes , Miriam Rosa Berrios Cornejo , Miguel Angel Fuenzalida Dias , Alejandro Markovits Rojas , Thomas Francis Harting Glade
发明人： Juvenal Antonio Sepulveda Reyes , Miriam Rosa Berrios Cornejo , Miguel Angel Fuenzalida Dias , Alejandro Markovits Rojas , Thomas Francis Harting Glade
IPC分类号： C07C51/00 , C11B3/00 , A23D9/00 , C11B1/10 , C11C1/10 , C11C3/00 , C11C1/08
CPC分类号： C11B3/001 , A23D9/00 , C11B1/10 , C11C1/08 , C11C1/10 , C11C3/003
摘要： An efficient and simple process to obtain a concentrate that includes over 80% in weight of ethyl esters of ω-3 fatty acids based on a composition of matter that contains esters of ω-3 fatty acids or free ω-3 fatty acids that comprises the stages of: a) contacting the composition of matter with ethanol of at least 96% in weight and a hydroxide of an alkali metal at a temperature between 60 and 200° C. to form a liquid mixture that includes alkaline salts of fatty acids; b) cool the liquid mixture to a temperature between 50 and −20° C. to form a solid phase and a liquid phase and separate the liquid phase from the solid phase; c) contact the separated liquid phase of stage b) with an acid to form an acidified mixture with a water content under 10%, where the mixture consists of a solid phase that includes the alkali metal salt of the acid and a liquid phase that comprises ω-3 fatty acids; d) heat the mixture of stage c) between 50 to 150° C. in the presence of an esterification catalyst to form a mixture that includes ethyl esters of ω-3 fatty acids; e) contact the mixture of stage d) with an alkali to form a neutralized mixture; f) distill the neutralized mixture to obtain a distillate that includes over 80% in weight of ethyl esters of ω-3 fatty acids.
摘要翻译：基于包含ω-3脂肪酸酯或ω-3脂肪酸酯的物质的组成，获得含有超过80重量％的ω-3脂肪酸的乙酯的浓缩物的有效和简单的方法，其包含阶段：a）在60至200℃的温度下使物质组合物与至少96重量％的乙醇和碱金属的氢氧化物接触以形成包含脂肪酸的碱性盐的液体混合物; b）将液体混合物冷却至50至-20℃的温度，以形成固相和液相，并将液相与固相分离; c）将步骤b）的分离的液相与酸接触以形成水含量低于10％的酸化混合物，其中混合物由包含酸的碱金属盐和液相的固相组成，所述液相包含 ω-3脂肪酸; d）在酯化催化剂存在下，将步骤c）的混合物加热至50-150℃以形成包含ω-3脂肪酸的乙酯的混合物; e）将阶段d）的混合物与碱接触以形成中和的混合物; f）蒸馏中和的混合物，得到包含超过80％重量的ω-3脂肪酸乙酯的馏出物。

4. 发明申请

US20130267600A1 Concentrate of Omega 3 有权
标题翻译：浓缩的Omega 3
公开(公告)号：US20130267600A1
公开(公告)日：2013-10-10
申请号：US13994785
申请日：2011-12-25
申请人： Juvenal Antonio Sepulveda Reyes , Miriam Rosa Berrios Cornejo , Miguel Angel Fuenzalida Dias , Alejandro Markovits Rojas , Thomas Francis Harting Glade
发明人： Juvenal Antonio Sepulveda Reyes , Miriam Rosa Berrios Cornejo , Miguel Angel Fuenzalida Dias , Alejandro Markovits Rojas , Thomas Francis Harting Glade
IPC分类号： C11B3/00
CPC分类号： C11B3/001 , A23D9/00 , C11B1/10 , C11C1/08 , C11C1/10 , C11C3/003
摘要： An efficient and simple process to obtain a concentrate that includes over 80% in weight of ethyl esters of ω-3 fatty acids based on a composition of matter that contains esters of ω-3 fatty acids or free ω-3 fatty acids that comprises the stages of: a) contacting the composition of matter with ethanol of at least 96% in weight and a hydroxide of an alkali metal at a temperature between 60 and 200° C. to form a liquid mixture that includes alkaline salts of fatty acids; b) cool the liquid mixture to a temperature between 50 and −20° C. to form a solid phase and a liquid phase and separate the liquid phase from the solid phase; c) contact the separated liquid phase of stage b) with an acid to form an acidified mixture with a water content under 10%, where the mixture consists of a solid phase that includes the alkali metal salt of the acid and a liquid phase that comprises ω-3 fatty acids; d) heat the mixture of stage c) between 50 to 150° C. in the presence of an esterification catalyst to form a mixture that includes ethyl esters of ω-3 fatty acids; e) contact the mixture of stage d) with an alkali to form a neutralized mixture; f) distill the neutralized mixture to obtain a distillate that includes over 80% in weight of ethyl esters of ω-3 fatty acids.
摘要翻译：基于含有ω-3脂肪酸酯或游离ω-3脂肪酸的物质的组成，获得含有超过80重量％的ω-3脂肪酸的乙酯的浓缩物的有效和简单的方法，其包含阶段：a）在60至200℃的温度下使物质组合物与至少96重量％的乙醇和碱金属的氢氧化物接触以形成包含脂肪酸的碱性盐的液体混合物; b）将液体混合物冷却至50至-20℃的温度，以形成固相和液相，并将液相与固相分离; c）将步骤b）的分离的液相与酸接触以形成水含量低于10％的酸化混合物，其中混合物由包含酸的碱金属盐和液相的固相组成，所述液相包含 ω-3脂肪酸; d）在酯化催化剂存在下，将步骤c）的混合物加热至50-150℃以形成包含ω-3脂肪酸的乙酯的混合物; e）将阶段d）的混合物与碱接触以形成中和的混合物; f）蒸馏中和的混合物，得到包含超过80％重量的ω-3脂肪酸乙酯的馏出物。

5. 发明申请

US20120046254A1 DISPERSION OF PHYTOSTEROLS 审中-公开
标题翻译：植物甾醇的分散体
公开(公告)号：US20120046254A1
公开(公告)日：2012-02-23
申请号：US13202862
申请日：2010-01-29
申请人： Thomas Francis Harting Glade , Miguel Fuenzalida Diaz , Alejandro Markovits Rojas
发明人： Thomas Francis Harting Glade , Miguel Fuenzalida Diaz , Alejandro Markovits Rojas
IPC分类号： A61K31/575 , A61P3/06
CPC分类号： A23D7/0056 , A23C9/13 , A23C9/152 , A23C2240/10 , A23D7/0053 , A23L27/60 , A23L33/11
摘要： The invention relates to a method for the production of highly stable aqueous dispersions of phytosterols, phytostanols and derivatives thereof, which allows the use of a wide range of emulsifiers in relatively small concentrations in relation to the phytosterols and which allows the preparation of dispersions with high concentrations of phytosterols. Said dispersions are obtained using a method in which one or more phytosterols, an aqueous medium and one or more emulsifiers are dispersed in a disperser at a temperature of at least 140° C. in order to obtain an emulsion and the resulting emulsion is subsequently cooled in order to obtain a dispersion of sterols in an aqueous medium.
摘要翻译：本发明涉及一种生产植物甾醇，植物甾烷醇及其衍生物的高度稳定的水分散体的方法，其允许使用相对于植物甾醇的相对较小浓度的宽范围的乳化剂，并且其允许制备高分散体植物甾醇的浓度。所述分散体使用其中将一种或多种植物甾醇，水性介质和一种或多种乳化剂在至少140℃的温度下分散在分散器中以获得乳液并随后将所得乳液冷却的方法获得以获得在水性介质中的甾醇分散体。

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