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1. 发明授权

US08529682B2 Process for preparing an indicator composition and indicator compositions 有权
标题翻译：制备指示剂组合物和指示剂组合物的方法
公开(公告)号：US08529682B2
公开(公告)日：2013-09-10
申请号：US13248254
申请日：2011-09-29
申请人： Thaddeus Prusik , Dawn E. Smith , Ray H. Baughman
发明人： Thaddeus Prusik , Dawn E. Smith , Ray H. Baughman
IPC分类号： C09D11/00 , G01N31/00 , G01K1/02 , G01K3/00 , G04F1/00
CPC分类号： C09D11/50
摘要： Indicator inks, indicators formed by printing or otherwise utilizing the inks and host products utilizing the indicators are disclosed. Reactivity-enhancing adjuvants stimulate enhanced thermal reactivity of diacetylenic or other indicator agents capable of responding to ambient thermal conditions with a visual change signaling an end point. The diacetylenic or other agents may be sensitive or relatively insensitive to ambient temperatures. Use of a reactivity-enhancing adjuvant provides a useful means for adapting the reactivities of indicator agents to the response characteristics of prospective host products, for example perishables such as vaccines or fresh fish and maturables such as fruit, cheese and wine. Some exemplary adjuvants include low-temperature polymerization initiators, for example methyl ethyl ketone peroxide and polymerization accelerators, for example cobalt compounds. Such initiators and accelerators can also be used in combination.
摘要翻译：公开了指示剂油墨，通过使用指示剂印刷或以其它方式利用油墨和主体产品形成的指示剂。反应性增强佐剂刺激能够响应于环境热条件的二乙炔或其他指示剂的增强的热反应性，其中以指示终点的视觉改变。二乙炔或其它试剂可能对环境温度敏感或相对不敏感。使用反应性增强佐剂提供了一种有用的方法，用于使指示剂的反应性适应于预期宿主产物的反应特性，例如易腐食物例如疫苗或鲜鱼以及可食用如水果，奶酪和葡萄酒。一些示例性的助剂包括低温聚合引发剂，例如甲基乙基酮过氧化物和聚合促进剂，例如钴化合物。这样的引发剂和促进剂也可以组合使用。

2. 发明授权

US08642807B2 Crystallized diacetylenic indicator compounds and methods of preparing the compounds 有权
标题翻译：结晶二乙炔指示剂化合物及其制备方法
公开(公告)号：US08642807B2
公开(公告)日：2014-02-04
申请号：US13529605
申请日：2012-06-21
申请人： Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik
发明人： Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik
IPC分类号： C07C275/20 , G01K11/12 , G01D21/00
CPC分类号： G01K11/12 , C07C273/02 , C07C275/20 , C09B69/10 , G01K3/04 , G01N21/78 , G01N31/22 , G01N31/229
摘要： Crystallized diacetylenic compounds having certain crystallographic and other characteristics; diacetylenic compounds and mixtures crystallized from diacetylenic solutions; methods of preparing and identifying solvent systems for dissolving diacetylenic compounds; diacetylenic solutions; methods of recrystallizing diacetylenic compounds; crystals of 2,4-hexadiyn-1,6-bis(alkylurea) compounds; and ambient condition indicators and time-temperature condition indicators comprising crystallized diacetylenic compounds.
摘要翻译：具有某些晶体学特性的结晶二炔化合物; 二乙炔化合物和从二乙炔溶液中结晶的混合物; 制备和鉴定溶解二乙炔化合物的溶剂体系的方法; 二乙酰溶液; 二乙炔化合物重结晶方法; 2,4-己二炔-1,6-双（烷基脲）化合物的晶体; 环境条件指标和包含结晶二乙炔化合物的时间 - 温度条件指标。

3. 发明授权

US08354486B2 Co-crystallizable diacetylenic monomer compositions, crystal phases and mixtures, and related methods 有权
标题翻译：可共结构的二炔单体组合物，结晶相和混合物及相关方法
公开(公告)号：US08354486B2
公开(公告)日：2013-01-15
申请号：US12730835
申请日：2010-03-24
申请人： Elizabeth Castillo Martinez , Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik , Carl M. Lentz
发明人： Elizabeth Castillo Martinez , Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik , Carl M. Lentz
IPC分类号： C08F238/00 , G01D21/00 , C07C275/20 , C08F2/36
CPC分类号： C07C275/20 , C08F238/02 , G01N31/229
摘要： Solid polymerizable diacetylenic monomer compositions, including compositions co-crystallized from a diversity of solvent systems under diverse cooling conditions, can exhibit diffraction patterns associated with the color development reactivities of the compositions. High reactivity compositions are disclosed and high reactivity and low reactivity phases can be identified. A low angle powder X-ray diffraction peak can indicate the presence of one or more crystal phases in a composition. A fingerprint region can exhibit fingerprint patterns of diffraction peaks associated with different reactivities. Information about polymerization of the diacetylenic monomers is disclosed using 13C nuclear magnetic resonance (“NMR”) characterization. Diacetylenic monomer compositions useful in ambient condition indicators, for example time-temperature indicators are disclosed.
摘要翻译：固体可聚合二炔单体组合物，包括在不同冷却条件下从各种溶剂体系共结晶的组合物可以显示与组合物的显色反应性相关的衍射图。公开了高反应性组合物，并且可以鉴定出高反应性和低反应性相。低角度粉末X射线衍射峰可以指示组合物中存在一个或多个结晶相。指纹区域可以显示与不同反应性相关的衍射峰的指纹图谱。使用13C核磁共振（NMR）表征公开了关于二乙炔单体的聚合的信息。公开了用于环境条件指示剂的二乙炔单体组合物，例如时间 - 温度指示剂。

4. 发明授权

US07891310B2 Freeze indicators, flexible freeze indicators, combination indicators and manufacturing methods 有权
标题翻译：冻结指标，灵活冻结指标，组合指标和制造方法
公开(公告)号：US07891310B2
公开(公告)日：2011-02-22
申请号：US12500799
申请日：2009-07-10
申请人： Dene H. Taylor , Thaddeus Prusik , Dawn E. Smith , Ray H. Baughman
发明人： Dene H. Taylor , Thaddeus Prusik , Dawn E. Smith , Ray H. Baughman
IPC分类号： G01K11/12 , G01K3/00
CPC分类号： G01K3/005 , G01K3/04 , G01K11/06 , Y10S252/962
摘要： Freeze indicators providing a visual indication of exposure of the freeze indicator to a freezing or near-freezing temperature and their manufacture are disclosed. The freeze indicators employ colloidal dispersions as active elements and include flexible freeze indicators, freeze indicators protected against drying out and freeze indicators employing core shell composites, for example gold coated pigments as active indicator elements. Also disclosed are: a combination freeze indicator and threshold temperature indicator; a combination threshold indicator and cumulative temperature indicator; and three-way combination indicators that can provide indications of cumulative past temperature exposure, exposure to freezing temperatures and exposure to a temperature above a threshold.
摘要翻译：公开了冻结指示器，其提供了将冷冻指示剂暴露于冷冻或接近冻结温度的视觉指示及其制造。冻结指示剂使用胶体分散体作为活性元素，并且包括灵活的冷冻指示剂，防止干燥的冷冻指示剂和使用核心壳复合材料的冷冻指示剂，例如镀金颜料作为活性指示剂元素。还公开了：组合冻结指示器和阈值温度指示器; 组合阈值指标和累积温度指标; 和三路组合指示器，可以提供累积过去的温度暴露，暴露于冷冻温度和暴露于高于阈值的温度的指示。

5. 发明授权

US07571695B2 Freeze indicators, flexible freeze indicators and manufacturing methods 有权
标题翻译：冻结指标，灵活冻结指标和制造方法
公开(公告)号：US07571695B2
公开(公告)日：2009-08-11
申请号：US11750054
申请日：2007-05-17
申请人： Dene H. Taylor , Thaddeus Prusik , Dawn E. Smith , Ray H. Baughman
发明人： Dene H. Taylor , Thaddeus Prusik , Dawn E. Smith , Ray H. Baughman
IPC分类号： G01K11/12
CPC分类号： G01K3/005 , G01K3/04 , G01K11/06 , Y10S252/962
摘要： Freeze indicators providing a visual indication of exposure of the freeze indicator to a freezing or near-freezing temperature and their manufacture are disclosed. The freeze indicators employ colloidal dispersions as active elements and include flexible freeze indicators, freeze indicators protected against drying out and freeze indicators employing core shell composites, for example gold coated pigments as active indicator elements. Also disclosed are: a combination freeze indicator and threshold temperature indicator; a combination threshold indicator and cumulative temperature indicator; and three-way combination indicators that can provide indications of cumulative past temperature exposure, exposure to freezing temperatures and exposure to a temperature above a threshold.
摘要翻译：公开了冻结指示器，其提供了将冷冻指示剂暴露于冷冻或接近冻结温度的视觉指示及其制造。冻结指示剂使用胶体分散体作为活性元素，并且包括灵活的冷冻指示剂，防止干燥的冷冻指示剂和使用核心壳复合材料的冷冻指示剂，例如镀金颜料作为活性指示剂元素。还公开了：组合冻结指示器和阈值温度指示器; 组合阈值指标和累积温度指标; 和三路组合指示器，可以提供累积过去的温度暴露，暴露于冷冻温度和暴露于高于阈值的温度的指示。

6. 发明申请

US20100024714A1 FREEZE INDICATORS, FLEXIBLE FREEZE INDICATORS, COMBINATION INDICATORS AND MANUFACTURING METHODS 有权
标题翻译：冷冻指示器，灵活冻结指示器，组合指示器和制造方法
公开(公告)号：US20100024714A1
公开(公告)日：2010-02-04
申请号：US12500799
申请日：2009-07-10
申请人： Dene H. TAYLOR , Thaddeus Prusik , Dawn E. Smith , Ray H. Baughman
发明人： Dene H. TAYLOR , Thaddeus Prusik , Dawn E. Smith , Ray H. Baughman
IPC分类号： G01K1/02 , G01D21/00
CPC分类号： G01K3/005 , G01K3/04 , G01K11/06 , Y10S252/962
摘要： Freeze indicators providing a visual indication of exposure of the freeze indicator to a freezing or near-freezing temperature and their manufacture are disclosed. The freeze indicators employ colloidal dispersions as active elements and include flexible freeze indicators, freeze indicators protected against drying out and freeze indicators employing core shell composites, for example gold coated pigments as active indicator elements. Also disclosed are: a combination freeze indicator and threshold temperature indicator; a combination threshold indicator and cumulative temperature indicator; and three-way combination indicators that can provide indications of cumulative past temperature exposure, exposure to freezing temperatures and exposure to a temperature above a threshold.
摘要翻译：公开了冻结指示器，其提供了将冷冻指示剂暴露于冷冻或接近冻结温度的视觉指示及其制造。冻结指示剂使用胶体分散体作为活性元素，并且包括灵活的冷冻指示剂，防止干燥的冷冻指示剂和使用核心壳复合材料的冷冻指示剂，例如镀金颜料作为活性指示剂元素。还公开了：组合冻结指示器和阈值温度指示器; 组合阈值指标和累积温度指标; 和三路组合指示器，可以提供累积过去的温度暴露，暴露于冷冻温度和暴露于高于阈值的温度的指示。

7. 发明授权

US08269042B2 Crystallized diacetylenic indicator compounds and methods of preparing the compounds 有权
标题翻译：结晶二乙炔指示剂化合物及其制备方法
公开(公告)号：US08269042B2
公开(公告)日：2012-09-18
申请号：US12261887
申请日：2008-10-30
申请人： Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik
发明人： Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik
IPC分类号： C07C275/04
CPC分类号： G01K11/12 , C07C273/02 , C07C275/20 , C09B69/10 , G01K3/04 , G01N21/78 , G01N31/22 , G01N31/229
摘要： Crystallized diacetylenic compounds having certain crystallographic and other characteristics; diacetylenic compounds and mixtures crystallized from diacetylenic solutions; methods of preparing and identifying solvent systems for dissolving diacetylenic compounds; diacetylenic solutions; methods of recrystallizing diacetylenic compounds; crystals of 2,4-hexadiyn-1,6-bis(alkylurea) compounds; and ambient condition indicators and time-temperature condition indicators comprising crystallized diacetylenic compounds.
摘要翻译：具有某些晶体学特性的结晶二炔化合物; 二乙炔化合物和从二乙炔溶液中结晶的混合物; 制备和鉴定溶解二乙炔化合物的溶剂体系的方法; 二乙酰溶液; 二乙炔化合物重结晶方法; 2,4-己二炔-1,6-双（烷基脲）化合物的晶体; 环境条件指标和包含结晶二乙炔化合物的时间 - 温度条件指标。

8. 发明申请

US20110086995A1 CO-CRYSTALLIZABLE DIACETYLENIC MONOMER COMPOSITIONS, CRYSTAL PHASES AND MIXTURES, AND RELATED METHODS 有权
标题翻译：可结晶的二乙烯单体组合物，晶体相和混合物及相关方法
公开(公告)号：US20110086995A1
公开(公告)日：2011-04-14
申请号：US12730835
申请日：2010-03-24
申请人： Elizabeth CASTILLO MARTINEZ , Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik , Carl M. Lentz
发明人： Elizabeth CASTILLO MARTINEZ , Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik , Carl M. Lentz
IPC分类号： C08F238/00
CPC分类号： C07C275/20 , C08F238/02 , G01N31/229
摘要： Solid polymerizable diacetylenic monomer compositions, including compositions co-crystallized from a diversity of solvent systems under diverse cooling conditions, can exhibit diffraction patterns associated with the color development reactivities of the compositions. High reactivity compositions are disclosed and high reactivity and low reactivity phases can be identified. A low angle powder X-ray diffraction peak can indicate the presence of one or more crystal phases in a composition. A fingerprint region can exhibit fingerprint patterns of diffraction peaks associated with different reactivities. Information about polymerization of the diacetylenic monomers is disclosed using 13C nuclear magnetic resonance (“NMR”) characterization. Diacetylenic monomer compositions useful in ambient condition indicators, for example time-temperature indicators are disclosed.
摘要翻译：固体可聚合二炔单体组合物，包括在不同冷却条件下从多种溶剂体系共结晶的组合物可以显示与组合物的显色反应性相关的衍射图。公开了高反应性组合物，并且可以鉴定出高反应性和低反应性相。低角度粉末X射线衍射峰可以指示组合物中存在一个或多个结晶相。指纹区域可以显示与不同反应性相关的衍射峰的指纹图谱。使用13C核磁共振（“NMR”）表征公开了关于二乙炔单体的聚合的信息。公开了用于环境条件指示剂的二乙炔单体组合物，例如时间 - 温度指示剂。

9. 发明申请

US20090131718A1 CRYSTALLIZED DIACETYLENIC INDICATOR COMPOUNDS AND METHODS OF PREPARING THE COMPOUNDS 有权
标题翻译：结晶二乙酸指示剂化合物及其制备方法
公开(公告)号：US20090131718A1
公开(公告)日：2009-05-21
申请号：US12261887
申请日：2008-10-30
申请人： Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik
发明人： Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik
IPC分类号： C07C273/02 , C07C275/20 , G01K3/00
CPC分类号： G01K11/12 , C07C273/02 , C07C275/20 , C09B69/10 , G01K3/04 , G01N21/78 , G01N31/22 , G01N31/229
摘要： Crystallized diacetylenic compounds having certain crystallographic and other characteristics; diacetylenic compounds and mixtures crystallized from diacetylenic solutions; methods of preparing and identifying solvent systems for dissolving diacetylenic compounds; diacetylenic solutions; methods of recrystallizing diacetylenic compounds; crystals of 2,4-hexadiyn-1,6-bis(alkylurea) compounds; and ambient condition indicators and time-temperature condition indicators comprising crystallized diacetylenic compounds.
摘要翻译：具有某些晶体学特性的结晶二炔化合物; 二乙炔化合物和从二乙炔溶液中结晶的混合物; 制备和鉴定溶解二乙炔化合物的溶剂体系的方法; 二乙酰溶液; 二乙炔化合物重结晶方法; 2,4-己二炔-1,6-双（烷基脲）化合物的晶体; 环境条件指标和包含结晶二乙炔化合物的时间 - 温度条件指标。

10. 发明授权

US4892677A Defrost indicator 失效
标题翻译：除霜指示器
公开(公告)号：US4892677A
公开(公告)日：1990-01-09
申请号：US683443
申请日：1984-12-19
申请人： Anthony F. Preziosi , Thaddeus Prusik , Ray H. Baughman
发明人： Anthony F. Preziosi , Thaddeus Prusik , Ray H. Baughman
IPC分类号： G01N31/22 , G07C1/00
CPC分类号： G07C1/00 , G01N31/229 , Y10S252/962 , Y10S428/913
摘要： A new process is described which is useful for producing novel articles of manufacture useful for monitoring the time-temperature history of perishable items. The process initially involves forming a solution comprised of a diacetylenic monomer and a solvent. The solution is frozen, and the frozen solution having crystalline diacetylenic monomer therein is irradiated to partially polymerize the diacetylenic monomer. Partial polymerization of the crystalline diacetylenic monomer admixed with frozen solvent results in the production of a novel article of manufacture having color. The novel article of manufacture is comprised of frozen solvent, diacetylenic monomer, and colored polydiacetylene. Due to the intensity of the color of the polydiacetylene, the entire article of manufacture appears to be colored.The colored article of manufacture may be attached to various perishables to monitor the shelf life of the perishables. upon exposure to temperatures above a critical temperature, the frozen solvent melts and extracts unreached monomer from the colored polymer, thereby causing a sharp color transition which indicates that the perishable should possibly be discarded.
摘要翻译：描述了一种新方法，其可用于生产可用于监测易腐物品的时间 - 温度历史的新型制品。该方法最初涉及形成由二乙炔单体和溶剂组成的溶液。将溶液冷冻，照射其中具有结晶二炔单体的冷冻溶液以部分聚合二乙炔单体。与冷冻溶剂混合的结晶二乙炔单体的部分聚合导致生产具有颜色的新型制品。新型制品由冷冻溶剂，二乙炔单体和着色聚二乙炔组成。由于聚二乙炔颜色的强度，整个制品似乎是有色的。有色制品可以附着在各种易腐食品上，以监测易腐品的保质期。在暴露于高于临界温度的温度下，冷冻的溶剂熔融并从着色聚合物中提取未接触的单体，从而引起明显的颜色转变，这表明易腐物质可能被丢弃。

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