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1. 发明授权

US5481022A N-aryloxyacyl-n-phenyltetrahydrophthalamic acid derivatives, methods of producing same, and herbicides containing same as effective components 失效
标题翻译： N-芳氧基酰基 - 正苯基四氢酞酸衍生物，其制备方法和含有与有效成分相同的除草剂
公开(公告)号：US5481022A
公开(公告)日：1996-01-02
申请号：US256646
申请日：1994-07-19
申请人： Tetsuo Takematsu , Takashi Kume , Shoji Yamaoka , Takeo Komata , Kiyoshi Suzuki , Yukio Ikeda , Matsue Kawamura , Yumiko Koda , Kaoru Mori
发明人： Tetsuo Takematsu , Takashi Kume , Shoji Yamaoka , Takeo Komata , Kiyoshi Suzuki , Yukio Ikeda , Matsue Kawamura , Yumiko Koda , Kaoru Mori
IPC分类号： A01N37/30 , A01N37/36 , A01N37/38 , C07C231/08 , C07C233/92 , C07C235/68 , C07C235/88 , C07C257/02 , C07C229/38 , A01N37/10
CPC分类号： C07C235/88 , A01N37/36 , A01N37/38 , C07C235/68 , C07C257/02 , C07C2101/16
摘要： The invention provides N-aryloxyacyl-N-phenyltetrahydrophthalamic acid derivatives represented by the general formula [I], a method of producing the same, and a herbicide containing the same as the effective components, ##STR1## wherein X and Y each individually represent hydrogen atoms or halogen atoms, Ar represents a substituted or unsubstituted phenyl group or naphthyl group, R.sup.1 represents a hydrogen atom, a halogen atom, a lower alkyl group, a lower alkoxy group, a lower alkenyloxy group, a lower alkynyloxy group, a lower alkoxyalkoxy group or a lower alkoxycarbonylalkoxy group, R.sup.2 represents a hydrogen atom or a lower alkyl group, R.sup.3 represents a hydroxyl, a lower alkoxy group, a lower alkenyloxy group, a lower alkynyloxy group, a lower alkoxyalkoxy group, a benzyloxy group or a lower alkoxycarbonylalkoxy group, and m is an integer ranging from 0 to 5. This herbicide which is very useful can be widely applied to upland, paddy field, orchard, turf, forest, non-crop land, etc., and is not harmful to crops.
摘要翻译： PCT No.PCT / JP93 / 01756 Sec。 371日期：1994年7月19日 102（e）日期1994年7月19日PCT 1993年12月2日PCT公布。公开号WO94 / 12469 日期：1994年6月9日本发明提供由通式[I]表示的N-芳氧基酰基-N-苯基四氢酞酸衍生物，其制备方法和含有与有效成分相同的除草剂， I]其中X和Y各自独立地表示氢原子或卤原子，Ar表示取代或未取代的苯基或萘基，R1表示氢原子，卤素原子，低级烷基，低级烷氧基，低级烯氧基低级烷氧基，低级烷氧基烷氧基或低级烷氧羰基烷氧基，R2表示氢原子或低级烷基，R3表示羟基，低级烷氧基，低级链烯氧基，低级炔氧基，低级烷氧基烷氧基烷氧基，苄氧基或低级烷氧基羰基烷氧基，m为0〜5的整数。该除草剂非常有用，可广泛应用于高地，水田，果园，草坪，森林， - 耕地等，对作物无害。

2. 发明授权

US5801122A N-phenyltetrahydrophthalamic acid derivatives, methods of producing same, and herbicides containing same as effective components 失效
标题翻译： N-苯基四氢酞酸衍生物，其制造方法，以及含有与有效成分相同的除草剂
公开(公告)号：US5801122A
公开(公告)日：1998-09-01
申请号：US676148
申请日：1996-07-15
申请人： Tetsuo Takematsu , Takeo Komata , Takashi Kume , Yumiko Kohda , Kiyoshi Suzuki , Matsue Kawamura , Yukio Ikeda , Kaoru Mori
发明人： Tetsuo Takematsu , Takeo Komata , Takashi Kume , Yumiko Kohda , Kiyoshi Suzuki , Matsue Kawamura , Yukio Ikeda , Kaoru Mori
IPC分类号： A01N37/26 , A01N39/00 , A01N43/10 , A01N43/40 , C07C323/52 , C07D213/82 , C07D333/38 , A01N43/36 , C07C321/00 , C07D333/22
CPC分类号： C07D213/82 , A01N37/26 , A01N39/00 , A01N43/10 , A01N43/40 , C07C323/52 , C07D333/38 , C07C2101/16
摘要： The invention provides N-phenyltetrahydrophthalamic acid derivatives represented by the general formula �I!, methods of producing the same, herbicides containing the same as the effective components, imidoylchloride derivatives as the intermediate products and methods of producing the same, ##STR1## wherein X and Y each individually represent hydrogen atoms or halogen atoms, R.sup.1 represents a lower alkoxycarbonylalkylthio group, R.sup.2 represents a lower alkyl group, a halogenated lower alkyl group or a substituted or unsubstituted phenyl group, and R.sup.3 represents a lower alkoxy group, a lower alkenyloxy group, a lower alkynyloxy group, or a lower alkoxyalkoxy group. The herbicides of the present invention, which are very useful, can be widely applied to upland, paddy field, orchard, turf, forest, non-crop land, etc., and are not harmful to crops.
摘要翻译： PCT No.PCT / JP95 / 00044 Sec。 371日期：1996年7月15日 102（e）日期1996年7月15日PCT提交1995年1月19日PCT公布。第WO95 / 19962号公报日期1995年7月27日本发明提供由通式[I]表示的N-苯基四氢酞酸衍生物，其制备方法，含有与有效成分相同的除草剂，作为中间产物的亚氨基氯衍生物及其制备方法，表示氢原子或卤素原子，R1表示低级烷氧基羰基烷硫基，R2表示低级烷基，卤代低级烷基或取代或未取代的苯基，R3表示低级烷氧基，低级链烯氧基，低级炔氧基基团或低级烷氧基烷氧基。本发明的除草剂非常有用，可广泛应用于旱地，水田，果园，草坪，森林，非作物地等，对作物无害。

3. 发明授权

US5510317A N-acyl-N-phenylmaleamic acid derivatives, methods of producing same, and herbicides containing same as effective components 失效
标题翻译： N-酰基-N-苯基马来酰胺酸衍生物，其制备方法，以及含有与有效成分相同的除草剂
公开(公告)号：US5510317A
公开(公告)日：1996-04-23
申请号：US256683
申请日：1994-07-20
申请人： Tetsuo Takematsu , Takashi Kume , Takeo Komata , Kiyoshi Suzuki , Yukio Ikeda , Matsue Kawamura , Kaoru Mori
发明人： Tetsuo Takematsu , Takashi Kume , Takeo Komata , Kiyoshi Suzuki , Yukio Ikeda , Matsue Kawamura , Kaoru Mori
IPC分类号： A01N37/30 , C07C231/08 , C07C231/10 , C07C231/12 , C07C233/91 , C07C233/92 , C07C235/88 , A01N27/00 , A01N29/04 , A01N29/10 , C07C229/36
CPC分类号： C07C233/92 , A01N37/30 , C07C233/91
摘要： The invention provides N-acyl-N-phenylmaleamic acid derivatives represented by the general formula I!, a method of producing the same, and a herbicide containing the same as the effective components, ##STR1## wherein X and Y each individually represent hydrogen atoms or halogen atoms, R.sup.1 represents a hydrogen atom, a halogen atom, a lower alkyl group, a lower alkenyl group, a lower alkynyl group, a lower alkoxyalkyl group or a lower alkoxycarbonylalkyl group, R.sup.2 represents a lower alkyl group, a halogenated lower alkyl group or a substituted or unsubstituted phenyl group, R.sup.3 represents a hydrogen atom or a lower alkyl group, and R.sup.4 represents a hydroxyl, a lower alkoxy group, a lower alkenyloxy group, a lower alkynyloxy group, a lower alkoxyalkoxy group, a benzyloxy group or a lower alkoxycarbonylalkoxy group. This herbicide which is very useful can be widely applied to upland, paddy field, orchard, turf, forest, non-crop land, etc., and is not harmful to crops.
摘要翻译： PCT No.PCT / JP93 / 01755 Sec。 371日期：1994年7月20日 102（e）日期1994年7月20日PCT 1993年12月2日PCT公布。 WO94 / 12468 PCT出版物日期：1994年6月9日本发明提供由通式[I]表示的N-酰基-N-苯基马来酰胺酸衍生物，其制备方法和含有与有效成分相同的除草剂， I]其中X和Y各自独立地表示氢原子或卤原子，R1表示氢原子，卤素原子，低级烷基，低级烯基，低级炔基，低级烷氧基烷基或低级烷氧基羰基烷基， R2表示低级烷基，卤代低级烷基或取代或未取代的苯基，R3表示氢原子或低级烷基，R4表示羟基，低级烷氧基，低级链烯氧基，低级炔氧基低级烷氧基烷氧基，苄氧基或低级烷氧羰基烷氧基。这种非常有用的除草剂可广泛应用于旱地，水田，果园，草坪，森林，非作物地等，对作物无害。

4. 发明授权

US06337417B1 N-phenyltetrahydrophthalamic acid derivatives, methods of producing same, and herbicides containing same as effective components 失效
标题翻译： N-苯基四氢酞酸衍生物，其制造方法，以及含有与有效成分相同的除草剂
公开(公告)号：US06337417B1
公开(公告)日：2002-01-08
申请号：US09097010
申请日：1998-06-15
申请人： Tetsuo Takematsu , Takeo Komata , Takashi Kume , Yumiko Kohda , Kiyoshi Suzuki , Matsue Kawamura , Yukio Ikeda , Kaoru Mori
发明人： Tetsuo Takematsu , Takeo Komata , Takashi Kume , Yumiko Kohda , Kiyoshi Suzuki , Matsue Kawamura , Yukio Ikeda , Kaoru Mori
IPC分类号： A01N4310
CPC分类号： C07D213/82 , A01N37/26 , A01N39/00 , A01N43/10 , A01N43/40 , C07C323/52 , C07C2601/16 , C07D333/38
摘要： The invention provides N-phenyltetrahydrophthalamic acid derivatives represented by the general formula [I], methods of producing the same, herbicides containing the same as the effective components, imidoylchloride derivatives as the intermediate products and methods of producing the same, wherein X and Y each individually represent hydrogen atoms or halogen atoms, R1 represents a lower alkoxycarbonylalkylthio group, R2 represents a lower alkyl group, a halogenated lower alkyl group or a substituted or unsubstituted phenyl group, and R3 represents a lower alkoxy group, a lower alkenyloxy group, a lower alkynyloxy group, or a lower alkoxyalkoxy group. The herbicides of the present invention, which are very useful, can be widely applied to upland, paddy field, orchard, turf, forest, non-crop land, etc., and are not harmful to crops.
摘要翻译：本发明提供由通式[I]表示的N-苯基四氢酞酸衍生物，其制备方法，含有与有效成分相同的除草剂，作为中间产物的亚氨基氯衍生物及其制备方法，其中X和Y各自分别表示氢原子或卤素原子，R1表示低级烷氧基羰基烷硫基，R2表示低级烷基，卤代低级烷基或取代或未取代的苯基，R3表示低级烷氧基，低级链烯氧基，低级烷氧基炔氧基或低级烷氧基烷氧基。本发明的除草剂非常有用，可广泛应用于旱地，水田，果园，草坪，森林，非作物地等，对作物无害。

5. 发明授权

US5468719A N-acyl-n-phenyltetrahydrophthalamic acid derivatives, methods of producing same, and herbicides containing same as effective components 失效
标题翻译： N-酰基-N-苯基四氢酞酸衍生物，其制造方法，以及含有与有效成分相同的除草剂
公开(公告)号：US5468719A
公开(公告)日：1995-11-21
申请号：US133200
申请日：1993-10-22
申请人： Tetsu Takematsu , Takeo Komata , Takashi Kume , Kiyoshi Suzuki , Matsue Kawamura , Yumiko Shirakawa , Kaoru Mori
发明人： Tetsu Takematsu , Takeo Komata , Takashi Kume , Kiyoshi Suzuki , Matsue Kawamura , Yumiko Shirakawa , Kaoru Mori
IPC分类号： A01N43/84 , C07D265/36 , A01N43/04
CPC分类号： C07D265/36 , A01N43/84
摘要： The invention provides N-acyl-N-phenyltetrahydrophthalamic acid derivatives represented by the general formula [I], methods of producing the same, herbicides containing the same as the effective components, imidoylchloride derivatives as the intermediate products and methods of producing the same, ##STR1## wherein R.sup.1 represents an alkyl group, an alkenyl group, an alkynyl group, an alkoxyalkyl group, a haloalkyl group, a haloalkenyl group, a haloalkynyl group or a cyanoalkyl group, R.sup.2 represents a lower alkyl group or a halogenated lower alkyl group, and R.sup.3 represents a lower alkoxy group, a lower alkenyloxy group, a lower alkynyloxy group, a lower alkoxyalkoxy group, a substituted or unsubstituted benzyloxy group, a lower haloalkyloxy group or a lower alkoxycarbonylalkoxy group. The herbicides of the present invention, which are very useful, can be widely applied to upland, paddy field, orchard, turf, forest, non-crop land, etc., and are not harmful to crops.
摘要翻译： PCT No.PCT / JP93 / 00245 Sec。 371日期：1993年10月22日 102（e）日期1993年10月22日PCT 1993年2月26日PCT公布。公开号WO93 / 日本特开1993年2月9日。本发明提供了通式[I]表示的N-酰基-N-苯基四氢酞酸衍生物，其制备方法，含有与有效成分相同的除草剂，作为中间产物的亚氨基氯衍生物，制备其的方法，其中R1表示烷基，烯基，炔基，烷氧基烷基，卤代烷基，卤代烯基，卤代炔基或氰基烷基，其中R1表示低级烷基或卤代低级烷基，R3表示低级烷氧基，低级烯氧基，低级炔氧基，低级烷氧基烷氧基，取代或未取代的苄氧基，低级卤代烷氧基或低级烷氧基羰基烷氧基。本发明的除草剂非常有用，可广泛应用于旱地，水田，果园，草坪，森林，非作物地等，对作物无害。

6. 发明授权

US06653488B2 Process for producing benzopyran carboxamide 失效
标题翻译：苯并吡喃甲酰胺的制备方法
公开(公告)号：US06653488B2
公开(公告)日：2003-11-25
申请号：US10214397
申请日：2002-08-08
申请人： Takeo Komata , Matsue Kawamura , Nariaki Ii
发明人： Takeo Komata , Matsue Kawamura , Nariaki Ii
IPC分类号： C07D31158
CPC分类号： C07D311/58
摘要： A first process for producing a benzopyran carboxamide represented by the general formula [1] includes reacting 3-aminopropionitrile.½ sulfate, N≡CCH2CH2NH2.½(H2SO4), with a benzopyran carboxylic halide represented by the general formula [2], in the presence of a base. A second process for producing the benzopyran carboxamide includes the steps of (a) reacting 3-aminopropionitrile.½ sulfate with a base, thereby forming 3-aminopropionitrile; and (b) reacting the 3-aminopropionitrile with the benzopyran carboxylic halide [2], thereby producing the benzopyran carboxamide. A process for stabilizing 3-aminopropionitrile includes turning the 3-aminopropionitrile into a sulfate of the 3-aminopropionitrile. where R is a straight-chain or non-straight-chain perfluoroalkyl group represented by CnF2n+1 where n is an integer of 1-10; and X is fluorine, chlorine, bromine or iodine.
摘要翻译：用于制备由通式[1]表示的苯并吡喃甲酰胺的第一种方法包括使3-氨基丙腈1/2硫酸盐，N = CCH 2 CH 2 NH 2 1/2（H 2 SO 4）与由通式[2]表示的苯并吡喃羧酸卤化物反应存在基地制备苯并吡喃甲酰胺的第二种方法包括以下步骤：（a）使3-氨基丙腈1/2硫酸酯与碱反应，从而形成3-氨基丙腈; 和（b）使3-氨基丙腈与苯并吡喃羧酸卤化物[2]反应，从而产生苯并吡喃甲酰胺。稳定3-氨基丙腈的方法包括将3-氨基丙腈转化为3-氨基丙腈的硫酸盐。其中R是由C n F 2n + 1表示的直链或非直链全氟烷基，其中n是1- 10; X是氟，氯，溴或碘。

7. 发明授权

US07230142B1 Process for purifying fluoromethyl 1,1,1,3,3,3-hexafluoroisopropyl ether 有权
标题翻译：氟甲基1,1,1,3,3,3-六氟异丙醚的纯化方法
公开(公告)号：US07230142B1
公开(公告)日：2007-06-12
申请号：US09381372
申请日：1999-03-03
申请人： Toshikazu Kawai , Matsue Kawamura
发明人： Toshikazu Kawai , Matsue Kawamura
IPC分类号： C07C43/12 , C07C41/38
CPC分类号： C07C41/38 , C07C41/44 , C07C43/123
摘要： A process for purifying fluoromethyl 1,1,1,3,3,3-hexafluoroisopropyl ether containing at least 1,1,1,3,3,3-hexafluoroisopropyl alcohol. The purifying process comprises the treatment of causing fluoromethyl 1,1,1,3,3,3-hexafluoroisopropyl ether containing at least 1,1,1,3,3,3-hexafluoroisopropyl alcohol, to contact with a basic aqueous solution. The basic aqueous solution contains a basic substance in an amount providing a chemical equivalent ratio of the basic substance to 1,1,1,3,3,3-hexafluoroisopropyl alcohol being within a range of not less than 1.
摘要翻译：一种含有至少1,1,1,3,3,3-六氟异丙醇的氟甲基1,1,1,3,3,3-六氟异丙醚的纯化方法。净化方法包括使含有至少1,1,1,3,3,3-六氟异丙醇的氟甲基1,1,1,3,3,3-六氟异丙醚与碱性水溶液接触的处理。碱性水溶液含有碱性物质与1,1,1,3,3,3-六氟异丙醇的化学当量比在不小于1的范围内的碱性物质。

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