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1. 发明授权

US07666962B2 Polymerization with living characteristics 有权
标题翻译：具有生活特性的聚合
公开(公告)号：US07666962B2
公开(公告)日：2010-02-23
申请号：US11805949
申请日：2007-05-25
申请人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
发明人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
IPC分类号： C08F2/00
CPC分类号： C08K5/38 , C07C327/36 , C07C329/00 , C07F9/4065 , C08F2/38 , C08F12/08 , C08F293/00 , C08F293/005 , C08L25/06
摘要： This invention concerns a free radical polymerization process, selected chain transfer agents employed in the process and polymers made thereby, in which the process comprises preparing polymer of general Formula (A) and Formula (B) comprising contacting: (i) a monomer selected from the group consisting of vinyl monomers (of structure CH2=CUV), maleic anhydride, N-alkylmaleimide, N-arylmaleimide, dialkyl fumarate and cyclopolymerizable monomers; (ii) a thiocarbonylthio compound selected from Formula (C) and Formula (D) having a chain transfer constant greater than about 0.1; and (iii) free radicals produced from a free radical source; the polymer of Formula (A) being made by contacting (i), (ii) C and (iii) and that of Formula (B) by contacting (i), (ii) D, and (iii); and (iv) controlling the polydispersity of the polymer being formed by varying the ratio of the number of molecules of (ii) to the number of molecules of (iii); wherein Q, R, U, V, Z, Z′, m, p and q am as defined in the text.
摘要翻译：本发明涉及自由基聚合方法，该方法中使用的选择的链转移剂和由此制备的聚合物，其中该方法包括制备通式（A）和式（B）的聚合物，其包括：（i）选自由乙烯基单体（结构CH 2 = CUV），马来酸酐，N-烷基马来酰亚胺，N-芳基马来酰亚胺，富马酸二烷基酯和可环化聚合的单体组成的组; （ii）选自式（C）和式（D）的硫代羰基硫代化合物，其链转移常数大于约0.1; 和（iii）自由基产生的自由基; 式（A）的聚合物通过使（i），（ii）D和（iii）接触而使（i），（ii）C和（iii）与式（B）和（iv）通过改变（ii）的分子数与（iii）的分子数之比来控制形成的聚合物的多分散性; 其中如文中所定义的Q，R，U，V，Z，Z'，m，p和q am。

2. 发明授权

US07662986B2 Polymerization with living characteristics 失效
标题翻译：具有生活特性的聚合
公开(公告)号：US07662986B2
公开(公告)日：2010-02-16
申请号：US11805929
申请日：2007-05-25
申请人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
发明人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
IPC分类号： C07C327/00 , C07C255/00
CPC分类号： C08K5/38 , C07C327/36 , C07C329/00 , C07F9/4065 , C08F2/38 , C08F12/08 , C08F293/00 , C08F293/005 , C08L25/06
摘要： This invention concerns a free radical polymerization process, selected chain transfer agents employed in the process and polymers made thereby, in which the process comprises preparing polymer of general Formula (A) and Formula (B) comprising contacting: (i) a monomer selected from the group consisting of vinyl monomers (of structure CH2═CUV), maleic anhydride, N-alkylmaleimide, N-arylmaleimide, dialkyl fumarate and cyclopolymerizable monomers; (ii) a thiocarbonylthio compound selected from Formula (C) and Formula (D) having a chain transfer constant greater than about 0.1; and (iii) free radicals produced from a free radical source; the polymer of Formula (A) being made by contacting (i), (ii) C and (iii) and that of Formula (B) by contacting (i), (ii) D, and (iii); and (iv) controlling the polydispersity of the polymer being formed by varying the ratio of the number of molecules of (ii) to the number of molecules of (iii); wherein Q, R, U, V, Z, Z′, m, p and q are as defined in the text.
摘要翻译：本发明涉及自由基聚合方法，该方法中使用的选择的链转移剂和由此制备的聚合物，其中该方法包括制备通式（A）和式（B）的聚合物，其包括：（i）选自由乙烯基单体（结构为CH2-CUV），马来酸酐，N-烷基马来酰亚胺，N-芳基马来酰亚胺，富马酸二烷基酯和可环化聚合的单体组成的组; （ii）选自式（C）和式（D）的硫代羰基硫代化合物，其链转移常数大于约0.1; 和（iii）自由基产生的自由基; 式（A）的聚合物通过使（i），（ii）D和（iii）接触而使（i），（ii）C和（iii）与式（B）和（iv）通过改变（ii）的分子数与（iii）的分子数之比来控制形成的聚合物的多分散性; 其中Q，R，U，V，Z，Z'，m，p和q如文中所定义。

3. 发明授权

US07714075B1 Polymerization with living characteristics 失效
标题翻译：具有生活特性的聚合
公开(公告)号：US07714075B1
公开(公告)日：2010-05-11
申请号：US09762833
申请日：1997-07-03
申请人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
发明人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
IPC分类号： C08L23/04
CPC分类号： C08K5/38 , C07C327/36 , C07C329/00 , C07F9/4065 , C08F2/38 , C08F12/08 , C08F293/00 , C08F293/005 , C08L25/06
摘要： This invention concerns a free radical polymerization process, selected chain transfer agents employed in the process and polymers made thereby, in which the process comprises preparing polymer of general Formula (A) and Formula (B) comprising contacting: (i) a monomer selected from the group consisting of vinyl monomers (of structure CH2═CUV), maleic anhydride, N-alkylmaleimide, N-arylmaleimide, dialkyl fumarate and cyclopolymerizable monomers; (ii) a thiocarbonylthio compound selected from Formula (C) and Formula (D) having a chain transfer constant greater than about 0.1; and (iii) free radicals produced from a free radical source; the polymer of Formula (A) being made by contacting (i), (ii) C and (iii) and that of Formula (B) by contacting (i), (ii) D, and (iii); and (iv) controlling the polydispersity of the polymer being formed by varying the ratio of the number of molecules of (ii) to the number of molecules of (iii); wherein Q, R, U, V, Z, Z′, m, p and q are as defined in the text.
摘要翻译：本发明涉及自由基聚合方法，该方法中使用的选择的链转移剂和由此制备的聚合物，其中该方法包括制备通式（A）和式（B）的聚合物，其包括使（i）选自由乙烯基单体（结构为CH 2 = CUV），马来酸酐，N-烷基马来酰亚胺，N-芳基马来酰亚胺，富马酸二烷基酯和可环化聚合的单体组成的组; （ii）选自式（C）和式（D）的硫代羰基硫代化合物，其链转移常数大于约0.1; 和（iii）自由基产生的自由基; 式（A）的聚合物通过使（i），（ii）D和（iii）接触而使（i），（ii）C和（iii）与式（B）和（iv）通过改变（ii）的分子数与（iii）的分子数之比来控制形成的聚合物的多分散性; 其中Q，R，U，V，Z，Z'，m，p和q如文中所定义。

4. 发明申请

US20080139836A1 Polymerization with living characteristics 失效
标题翻译：具有生活特性的聚合
公开(公告)号：US20080139836A1
公开(公告)日：2008-06-12
申请号：US11805929
申请日：2007-05-25
申请人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
发明人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
IPC分类号： C07C327/36
CPC分类号： C08K5/38 , C07C327/36 , C07C329/00 , C07F9/4065 , C08F2/38 , C08F12/08 , C08F293/00 , C08F293/005 , C08L25/06
摘要： This invention concerns a free radical polymerization process, selected chain transfer agents employed in the process and polymers made thereby, in which the process comprises preparing polymer of general Formula (A) and Formula (B) comprising contacting: (i) a monomer selected from the group consisting of vinyl monomers (of structure CH2═CUV), maleic anhydride, N-alkylmaleimide, N-arylmaleimide, dialkyl fumarate and cyclopolymerizable monomers; (ii) a thiocarbonylthio compound selected from Formula (C) and Formula (D) having a chain transfer constant greater than about 0.1; and (iii) free radicals produced from a free radical source; the polymer of Formula (A) being made by contacting (i), (ii) C and (iii) and that of Formula (B) by contacting (i), (ii) D, and (iii); and (iv) controlling the polydispersity of the polymer being formed by varying the ratio of the number of molecules of (ii) to the number of molecules of (iii); wherein Q, R, U, V, Z, Z′, m, p and q are as defined in the text.
摘要翻译：本发明涉及自由基聚合方法，该方法中使用的选择的链转移剂和由此制备的聚合物，其中该方法包括制备通式（A）和式（B）的聚合物，其包括：（i）选自由乙烯基单体（结构CH 2 CO 2），马来酸酐，N-烷基马来酰亚胺，N-芳基马来酰亚胺，富马酸二烷基酯和可环化聚合的单体组成的组; （ii）选自式（C）和式（D）的硫代羰基硫代化合物，其链转移常数大于约0.1; 和（iii）自由基产生的自由基; 式（A）的聚合物通过使（i），（ii）D和（iii）接触而使（i），（ii）C和（iii）与式（B）和（iv）通过改变（ii）的分子数与（iii）的分子数之比来控制形成的聚合物的多分散性; 其中Q，R，U，V，Z，Z'，m，p和q如文中所定义。

5. 发明申请

US20080139764A1 Polymerization with living characteristics 有权
标题翻译：具有生活特性的聚合
公开(公告)号：US20080139764A1
公开(公告)日：2008-06-12
申请号：US11805949
申请日：2007-05-25
申请人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
发明人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
IPC分类号： C08F4/00
CPC分类号： C08K5/38 , C07C327/36 , C07C329/00 , C07F9/4065 , C08F2/38 , C08F12/08 , C08F293/00 , C08F293/005 , C08L25/06
摘要： This invention concerns a free radical polymerization process, selected chain transfer agents employed in the process and polymers made thereby, in which the process comprises preparing polymer of general Formula (A) and Formula (B) comprising contacting: (i) a monomer selected from the group consisting of vinyl monomers (of structure CH2=CUV), maleic anhydride, N-alkylmaleimide, N-arylmaleimide, dialkyl fumarate and cyclopolymerizable monomers; (ii) a thiocarbonylthio compound selected from Formula (C) and Formula (D) having a chain transfer constant greater than about 0.1; and (iii) free radicals produced from a free radical source; the polymer of Formula (A) being made by contacting (i), (ii) C and (iii) and that of Formula (B) by contacting (i), (ii) D, and (iii); and (iv) controlling the polydispersity of the polymer being formed by varying the ratio of the number of molecules of (ii) to the number of molecules of (iii); wherein Q, R, U, V, Z, Z′, m, p and q am as defined in the text.
摘要翻译：本发明涉及自由基聚合方法，该方法中使用的选择的链转移剂和由此制备的聚合物，其中该方法包括制备通式（A）和式（B）的聚合物，其包括：（i）选自由乙烯基单体（结构CH 2/2 = CUV），马来酸酐，N-烷基马来酰亚胺，N-芳基马来酰亚胺，富马酸二烷基酯和可环化聚合的单体组成的组; （ii）选自式（C）和式（D）的硫代羰基硫代化合物，其链转移常数大于约0.1; 和（iii）自由基产生的自由基; 式（A）的聚合物通过使（i），（ii）D和（iii）接触而使（i），（ii）C和（iii）与式（B）和（iv）通过改变（ii）的分子数与（iii）的分子数之比来控制形成的聚合物的多分散性; 其中如文中所定义的Q，R，U，V，Z，Z'，m，p和q am。

6. 发明授权

US07250479B2 Polymerization with living characteristics 有权
标题翻译：具有生活特性的聚合
公开(公告)号：US07250479B2
公开(公告)日：2007-07-31
申请号：US10784425
申请日：2004-02-23
申请人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
发明人： Tam Phuong Le , Graeme Moad , Ezio Rizzardo , San Hoa Thang
IPC分类号： C08F2/00
CPC分类号： C08K5/38 , C07C327/36 , C07C329/00 , C07F9/4065 , C08F2/38 , C08F12/08 , C08F293/00 , C08F293/005 , C08L25/06
摘要： This invention concerns a free radical polymerization process, selected chain transfer agents employed in the process and polymers made thereby, in which the process comprises preparing polymer of general Formula (A) and Formula (B) comprising contacting: (i) a monomer selected from the group consisting of vinyl monomers (of structure CH2═CUV), maleic anhydride, N-alkylmaleimide, N-arylmaleimide, dialkyl fumarate and cyclopolymerizable monomers; (ii) a thiocarbonylthio compound selected from Formula (C) and Formula (D) having a chain transfer constant greater than about 0.1; and (iii) free radicals produced from a free radical source; the polymer of Formula (A) being made by contacting (i), (ii) C and (iii) and that of Formula (B) by contacting (i), (ii) D, and (iii); and (iv) controlling the polydispersity of the polymer being formed by varying the ratio of the number of molecules of (ii) to the number of molecules of (iii); wherein Q, R, U, V, Z, Z′, m, p and q are as defined in the text
摘要翻译：本发明涉及自由基聚合方法，该方法中使用的选择的链转移剂和由此制备的聚合物，其中该方法包括制备通式（A）和式（B）的聚合物，其包括：（i）选自由乙烯基单体（结构CH 2 CO 2），马来酸酐，N-烷基马来酰亚胺，N-芳基马来酰亚胺，富马酸二烷基酯和可环化聚合的单体组成的组; （ii）选自式（C）和式（D）的硫代羰基硫代化合物，其链转移常数大于约0.1; 和（iii）自由基产生的自由基; 式（A）的聚合物通过使（i），（ii）D和（iii）接触而使（i），（ii）C和（iii）与式（B）和（iv）通过改变（ii）的分子数与（iii）的分子数之比来控制形成的聚合物的多分散性; 其中Q，R，U，V，Z，Z'，m，p和q如文中所定义

7. 发明申请

US20100137548A1 PROCESS FOR TRANSFORMING THE END GROUPS OF POLYMERS 有权
标题翻译：改造聚合物末端组的方法
公开(公告)号：US20100137548A1
公开(公告)日：2010-06-03
申请号：US12528249
申请日：2007-02-23
申请人： Graeme Moad , San Hoa Thang , Ezio Rizzardo
发明人： Graeme Moad , San Hoa Thang , Ezio Rizzardo
IPC分类号： C08G18/10 , C08G75/28
CPC分类号： C08F8/00 , C08F2/38 , C08F8/04 , C08F8/12 , C08F112/08 , C08F2438/03 , C08F2810/40 , C08G18/6287 , C08G65/3322 , C08G65/33337 , C08G65/33368 , C08G65/334 , C08G65/3344 , C08G65/3348 , C08L25/06 , C08L71/02 , C08L2205/05 , C08L2666/04 , C08F120/18
摘要： The present invention is directed to a process for the cleavage of one or more starting polymers having thiocarbonylthio groups of the formula (I) into derived polymers in which the —S—(C═S)— group is transformed. The process includes contacting the starting polymer containing groups Yb with one or more reagents containing groups Xa to produce the derived polymer and a byproduct containing the groups Yb, wherein the groups Xa is one or more reactive groups and the groups Yb is an extracting group and a byproduct, which is then separated from the derived polymer by conventional separation processes. The derived polymer is free from odor or color that is sometimes associated with the starting polymer and it can be used in making optical lenses, such as high refractive index spectacle lenses.
摘要翻译：本发明涉及将具有式（I）的硫代羰基硫基的一种或多种起始聚合物切割成其中-S-（C = S） - 基团被转化的衍生聚合物的方法。该方法包括使含有基团Yb的起始聚合物与含有基团Xa的一种或多种试剂接触以制备衍生的聚合物和含有基团Yb的副产物，其中基团Xa是一个或多个反应性基团，基团Yb是提取基团，副产物，然后通过常规分离方法与衍生的聚合物分离。衍生的聚合物没有有时与起始聚合物相关的气味或颜色，并且可以用于制造光学透镜，例如高折射率眼镜镜片。

8. 发明授权

US06653407B2 Process for preparing star shaped microgels from macromonomers with terminal ethylenic unsaturation 有权
标题翻译：从具有末端烯属不饱和键的大分子单体制备星形微凝胶的方法
公开(公告)号：US06653407B2
公开(公告)日：2003-11-25
申请号：US09969672
申请日：2001-10-03
申请人： Charles T. Berge , Michael Fryd , Jeffrey W. Johnson , Graeme Moad , Ezio Rizzardo , Christopher Scopazzi , San Hoa Thang
发明人： Charles T. Berge , Michael Fryd , Jeffrey W. Johnson , Graeme Moad , Ezio Rizzardo , Christopher Scopazzi , San Hoa Thang
IPC分类号： C08F238
CPC分类号： C08F265/04 , C08F290/04 , C08F290/061 , C08F293/00 , C08F293/005 , Y10S514/944
摘要： The present invention is directed to a process for forming star shaped microgels which include a core of crosslinked polymer and multiplicity of substantially linear polymeric arms of macromonomers attached to the core. The process includes polymerizing monoethylenically unsaturated monomers in the presence of a chain transfer agent to form macromonomers each having a terminal polymerizable ethylenically unsaturated group and then polymerizing, in presence of the macromonomers, the monoethylenically unsaturated monomers and multi-olefinic crosslinking monomers. The microgels of the present invention can be used as rheology control agents in waterborne and solvent-borne coatings and in adhesives and cosmetics.
摘要翻译：本发明涉及一种形成星形微凝胶的方法，其包括交联聚合物的核心和连接到核心的大分子单体的基本上线性的多个聚合物臂的多个。该方法包括在链转移剂的存在下聚合单烯属不饱和单体以形成各自具有末端可聚合烯属不饱和基团的大分子单体，然后在大分子单体存在下，单烯属不饱和单体和多烯属交联单体聚合。本发明的微凝胶可用作水性和溶剂型涂料以及粘合剂和化妆品中的流变控制剂。

9. 发明授权

US5977278A Polymers formed from allylic chain transfer agents 失效
标题翻译：由烯丙基链转移剂形成的聚合物
公开(公告)号：US5977278A
公开(公告)日：1999-11-02
申请号：US74438
申请日：1998-05-07
申请人： Ezio Rizzardo , San Hoa Thang , Graeme Moad , Charles T. Berge
发明人： Ezio Rizzardo , San Hoa Thang , Graeme Moad , Charles T. Berge
IPC分类号： C07C69/593 , C07C69/604 , C07C69/618 , C08F2/38
CPC分类号： C07C69/618 , C07C69/593 , C07C69/604 , C08F2/38
摘要： The present invention relates to polymers having the formula: ##STR1## wherein: M, Q, X, Y, Z, R.sup.3 and R.sup.4 are as defined in the text.
摘要翻译：本发明涉及具有下式的聚合物：其中：M，Q，X，Y，Z，R 3和R 4如本文所定义。

10. 发明授权

US5571850A Aqueous dispersions containing cyclopolymer dispersants 失效
标题翻译：含有环聚合物分散剂的水分散体
公开(公告)号：US5571850A
公开(公告)日：1996-11-05
申请号：US586852
申请日：1996-01-25
申请人： Sheau-Hwa Ma , San Hoa Thang , Ezio Rizzardo , Graeme Moad
发明人： Sheau-Hwa Ma , San Hoa Thang , Ezio Rizzardo , Graeme Moad
IPC分类号： C07C69/604 , C07C69/618 , C07C69/65 , C07D239/62 , C07D319/06 , C07F9/40 , C08F36/20 , C09D11/00 , C09D11/02 , C08L9/00
CPC分类号： C07D239/62 , C07C69/604 , C07C69/618 , C07C69/65 , C07D319/06 , C07F9/4015 , C08F36/20 , C09D11/326
摘要： Aqueous dispersions which are particularly well suited for use as aqueous jet ink compositions having an aqueous carrier medium which comprises water or a mixture of water and at least one organic solvent, a particulate solid, preferably a pigment, and a cyclopolymer dispersant.
摘要翻译： PCT No.PCT / US94 / 08645 Sec。 371日期：1996年1月25日 102（e）日期1996年1月25日PCT提交1994年7月29日PCT公布。公开号WO95 / 04109 日期1995年2月9日特别适合用作具有水性载体介质的水性分散体的水分散体，其包含水或水与至少一种有机溶剂的混合物，颗粒状固体，优选颜料和环聚合物分散剂。

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