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1. 发明授权

US06956132B2 Process for producing 2-phenylacetophenone derivatives and precursors therefor 失效
标题翻译：制备2-苯基苯乙酮衍生物及其前体的方法
公开(公告)号：US06956132B2
公开(公告)日：2005-10-18
申请号：US10485615
申请日：2002-07-15
申请人： Takeshi Ohshima , Shigeyuki Nishimura , Takayoshi Ando
发明人： Takeshi Ohshima , Shigeyuki Nishimura , Takayoshi Ando
IPC分类号： C07C45/42 , C07C45/51 , C07C49/813 , C07C49/76 , C07C211/00
CPC分类号： C07C49/813 , C07C45/42 , C07C45/516
摘要： A process for producing 2-phenylacetophenone derivatives represented by the formula (I): (wherein X is an alkyl group or a haloalkyl group, and Y is a hydrogen atom, a halogen atom or an alkyl group which may be substituted), which comprises reacting a compound represented by the formula (II): (wherein X and Y are as defined above, and R is a hydrogen atom or an alkyl group) with an acid.
摘要翻译：一种制备由式（I）表示的2-苯基苯乙酮衍生物的方法：（其中X是烷基或卤代烷基，Y是氢原子，卤原子或可被取代的烷基），其包括与式（II）表示的化合物（其中X和Y如上定义，R是氢原子或烷基）与酸反应。

2. 发明申请

US20110021774A1 METHOD FOR PRODUCING PYRIMIDINE COMPOUND 有权
标题翻译：生产吡啶化合物的方法
公开(公告)号：US20110021774A1
公开(公告)日：2011-01-27
申请号：US12933980
申请日：2009-04-16
申请人： Shigeo Murai , Ryoji Koto , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takao Awazu , Hisayoshi Jonishi , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
发明人： Shigeo Murai , Ryoji Koto , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takao Awazu , Hisayoshi Jonishi , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
IPC分类号： C07D401/12 , C07D239/42
CPC分类号： C07D239/42 , C07D239/52 , C07D401/12
摘要： To provide a method for producing pyrimidine compound useful as an intermediate for agricultural chemicals or pharmaceuticals, which is simple in operation, presents high yield and produces only a small amount of by-products.The method comprises reacting a compound represented by the formula (I) with a compound represented by the formula (II) in the presence of a pyridine compound to produce a compound represented by the formula (III), a compound represented by the formula (IV) or their mixture.
摘要翻译：提供一种制造用作农药或药物中间体的嘧啶化合物的方法，其操作简单，产率高，仅产生少量副产物。该方法包括使式（I）表示的化合物与式（II）表示的化合物在吡啶化合物的存在下反应，制得由式（III）表示的化合物，式（IV）表示的化合物）或它们的混合物。

3. 发明授权

US08440824B2 Method for producing pyrimidine compound 有权
标题翻译：制备嘧啶化合物的方法
公开(公告)号：US08440824B2
公开(公告)日：2013-05-14
申请号：US12933980
申请日：2009-04-16
申请人： Shigeo Murai , Ryoji Koto , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takao Awazu , Hisayoshi Jonishi , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
发明人： Shigeo Murai , Ryoji Koto , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takao Awazu , Hisayoshi Jonishi , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
IPC分类号： C07D239/02
CPC分类号： C07D239/42 , C07D239/52 , C07D401/12
摘要： To provide a method for producing pyrimidine compound useful as an intermediate for agricultural chemicals or pharmaceuticals, which is simple in operation, presents high yield and produces only a small amount of by-products.The method comprises reacting a compound represented by the formula (I) with a compound represented by the formula (II) in the presence of a pyridine compound to produce a compound represented by the formula (III), a compound represented by the formula (IV) or their mixture.
摘要翻译：提供一种制造用作农药或药物中间体的嘧啶化合物的方法，其操作简单，产率高，仅产生少量副产物。该方法包括使式（I）表示的化合物与式（II）表示的化合物在吡啶化合物的存在下反应，制得由式（III）表示的化合物，式（IV）表示的化合物）或它们的混合物。

4. 发明授权

US08338612B2 Process for producing toluidine compound 有权
标题翻译：甲苯胺化合物的制备方法
公开(公告)号：US08338612B2
公开(公告)日：2012-12-25
申请号：US12671050
申请日：2008-07-29
申请人： Shigeo Murai , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
发明人： Shigeo Murai , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
IPC分类号： C07D213/74
CPC分类号： C07D213/72
摘要： Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component, a solvent selected from the group consisting of ketones, nitriles, ethers and esters and a sufficient amount of water to substantially dissolve the alkali component, (2) a step of neutralizing or acidifying the reaction mixture with an acid and (3) a step of removing the solvent by distillation from the mixture containing fluazinam as the reaction product and the reaction solvent to precipitate crystals the product.
摘要翻译：由于氟啶胺作为农药的有效成分是优异的，而且是非常有用的，因此希望能以低成本的环境友好的方式以简单的操作以适当的形式有效地生产。通过使用工业上有利的反应体系，通过使用包括（1）在碱组分，选自酮，腈的溶剂存在下使ACTF和DCDNBTF反应的步骤，以简单的操作获得所需产物，醚和酯和足够量的水以基本上溶解碱组分，（2）用酸中和或酸化反应混合物的步骤和（3）通过蒸馏从包含氟啶胺的混合物中除去溶剂的步骤为反应产物和反应溶剂使产物析出晶体。

5. 发明申请

US20100197930A1 PROCESS FOR PRODUCING TOLUIDINE COMPOUND 有权
标题翻译：生产托洛芬化合物的方法
公开(公告)号：US20100197930A1
公开(公告)日：2010-08-05
申请号：US12671050
申请日：2008-07-29
申请人： Shigeo Murai , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
发明人： Shigeo Murai , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
IPC分类号： C07D213/36
CPC分类号： C07D213/72
摘要： Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component, a solvent selected from the group consisting of ketones, nitriles, ethers and esters and a sufficient amount of water to substantially dissolve the alkali component, (2) a step of neutralizing or acidifying the reaction mixture with an acid and (3) a step of removing the solvent by distillation from the mixture containing fluazinam as the reaction product and the reaction solvent to precipitate crystals the product.
摘要翻译：由于氟啶胺作为农药的有效成分是优异的，而且是非常有用的，因此希望能以低成本的环境友好的方式以简单的操作以适当的形式有效地生产。通过使用工业上有利的反应体系，通过使用包括（1）在碱组分，选自酮，腈的溶剂存在下使ACTF和DCDNBTF反应的步骤，以简单的操作获得所需产物，醚和酯和足够量的水以基本上溶解碱组分，（2）用酸中和或酸化反应混合物的步骤和（3）通过蒸馏从包含氟啶胺的混合物中除去溶剂的步骤为反应产物和反应溶剂使产物析出晶体。

6. 发明授权

US09027865B2 Webbing winding device 有权
标题翻译：卷绕装置
公开(公告)号：US09027865B2
公开(公告)日：2015-05-12
申请号：US13525921
申请日：2012-06-18
申请人： Masaru Ukita , Wataru Yanagawa , Yoshiaki Maekubo , Takayoshi Ando
发明人： Masaru Ukita , Wataru Yanagawa , Yoshiaki Maekubo , Takayoshi Ando
IPC分类号： B65H75/48 , B60R22/34
CPC分类号： B60R22/3413
摘要： In a webbing winding device, even when a piston moves toward the other side in a movement direction due to a reaction when the piston moves to a maximum movement position, an engagement surface of a hook portion comes into contact with a subject engagement surface of a subject engagement portion, so that the movement of the piston toward the other side in the movement direction is restricted. Accordingly, the piston is prevented from returning to a standby position, and a pawl is prevented from returning to a lock position. For this reason, a state where a rotation of a locking ring in the pull-out direction is maintained. Accordingly, after the piston moves from the standby position to the maximum movement position, the piston is prevented from returning to the standby position, and the force limiter load is prevented from being changed.
摘要翻译：在一种织带缠绕装置中，即使当活塞在活塞移动到最大移动位置时由于反应而在活塞方向上朝向另一侧移动时，钩部的接合表面与主体接合表面接触使得活塞向运动方向的另一侧的运动受到限制。因此，防止活塞返回到待机位置，并且防止棘爪返回到锁定位置。因此，保持锁定环在拉出方向上的旋转的状态。因此，在活塞从待机位置移动到最大移动位置之后，防止活塞返回待机位置，防止力限制器的负载变化。

7. 发明授权

US5571918A Method for producing 2-methylspiro(1,3-oxathiolane-5,3')quinuclidine 失效
标题翻译： 2-甲基螺（1,3-氧硫杂环戊烷-5,3'）奎宁环的制备方法
公开(公告)号：US5571918A
公开(公告)日：1996-11-05
申请号：US439576
申请日：1995-05-11
申请人： Koji Hayashi , Sho Tokumoto , Hiroshi Yoshizawa , Tatsuo Isogai , Masaru Kimura , Masahiko Sawaki , Takayoshi Ando , Isamu Katsuyama , Hayato Ariyoshi , Tadashi Nakamura
发明人： Koji Hayashi , Sho Tokumoto , Hiroshi Yoshizawa , Tatsuo Isogai , Masaru Kimura , Masahiko Sawaki , Takayoshi Ando , Isamu Katsuyama , Hayato Ariyoshi , Tadashi Nakamura
IPC分类号： C07D453/00 , A61K31/435 , A61P25/00 , A61P43/00 , B01J27/135 , B01J27/16 , B01J31/02 , C07B61/00 , C07D453/02 , C07D497/20
CPC分类号： C07D497/20
摘要： A method for producing 2-methylspiro(1,3-oxathiolane-5,3')quinuclidine, which comprises reacting 3-hydroxy-3-mercaptomethylquinuclidine or a salt thereof and a carbonyl compound in the presence of a catalyst made of at least one member selected from the group consisting of tin halides, oxyacids of phosphorus, phosphorus oxyhalides and organic sulfonic acids, to produce cis-form 2-methylspiro(1,3-oxathiolane-5,3')quinuclidine or a salt thereof.
摘要翻译：一种2-甲基螺（1,3-氧硫杂环戊烷-5,3'）奎宁环的制备方法，其包括使3-羟基-3-巯基乙基奎宁环或其盐与羰基化合物在催化剂存在下反应，所述催化剂由至少一种选自锡卤化物，磷酸的氧酸，磷酰卤和有机磺酸的组分，以制备顺式2-甲基螺（1,3-氧硫杂环戊烷-5,3'）奎宁环或其盐。

8. 发明授权

US08350057B2 Method for producing 3-methyl-2-thiophenecarboxylic acid 有权
标题翻译： 3-甲基-2-噻吩羧酸的制备方法
公开(公告)号：US08350057B2
公开(公告)日：2013-01-08
申请号：US13000937
申请日：2009-06-25
申请人： Takayoshi Ando , Norio Adachi , Akihiro Isogai
发明人： Takayoshi Ando , Norio Adachi , Akihiro Isogai
IPC分类号： C07D333/40
CPC分类号： C07D333/40
摘要： A method for producing 3-methyl-2-thiophenecarboxylic acid is provided.A method for producing 3-methyl-2-thiophenecarboxylic acid, which comprises reacting a compound represented by the formula (I): (wherein X is a chlorine atom or a bromine atom) with magnesium in the presence of an alkyl halide to give a Grignard reagent represented by the formula (II): (wherein X is the same as defined above), reacting the Grignard reagent of the formula (II) with carbon dioxide, and acidifying the reaction product.
摘要翻译：提供了3-甲基-2-噻吩羧酸的制备方法。一种3-甲基-2-噻吩羧酸的制备方法，其包括在烷基卤存在下使式（I）表示的化合物（其中X为氯原子或溴原子）与镁反应，得到由式（II）表示的格利雅试剂（其中X与上述定义相同），使式（II）的格氏试剂与二氧化碳反应，并使反应产物酸化。

9. 发明申请

US20110112311A1 METHOD FOR PRODUCING 3-METHYL-2-THIOPHENECARBOXYLIC ACID 有权
标题翻译： 3-甲基-2-噻吩羧酸的制备方法
公开(公告)号：US20110112311A1
公开(公告)日：2011-05-12
申请号：US13000937
申请日：2009-06-25
申请人： Takayoshi Ando , Norio Adachi , Akihiro Isogai
发明人： Takayoshi Ando , Norio Adachi , Akihiro Isogai
IPC分类号： C07D333/40
CPC分类号： C07D333/40
摘要： A method for producing 3-methyl-2-thiophenecarboxylic acid is provided.A method for producing 3-methyl-2-thiophenecarboxylic acid, which comprises reacting a compound represented by the formula (I): (wherein X is a chlorine atom or a bromine atom) with magnesium in the presence of an alkyl halide to give a Grignard reagent represented by the formula (II): (wherein X is the same as defined above), reacting the Grignard reagent of the formula (II) with carbon dioxide, and acidifying the reaction product.
摘要翻译：提供了3-甲基-2-噻吩羧酸的制备方法。一种3-甲基-2-噻吩羧酸的制备方法，其包括在烷基卤存在下使式（I）表示的化合物（其中X为氯原子或溴原子）与镁反应，得到由式（II）表示的格利雅试剂（其中X与上述定义相同），使式（II）的格氏试剂与二氧化碳反应，并使反应产物酸化。

10. 发明授权

US08376258B2 Webbing take-up device 有权
标题翻译：织带收卷装置
公开(公告)号：US08376258B2
公开(公告)日：2013-02-19
申请号：US12904955
申请日：2010-10-14
申请人： Takayoshi Ando , Teruhiko Koide , Masafumi Tsujimoto
发明人： Takayoshi Ando , Teruhiko Koide , Masafumi Tsujimoto
IPC分类号： B65H75/48
CPC分类号： B60R22/46 , B60R2022/468
摘要： A webbing take-up device enabling a reduction in size of an overload release mechanism and easy adjustment of an operation torque of the overload release mechanism is provided. In the overload release mechanism of this webbing take-up device, rotary force of a large diameter gear is transmitted to a small diameter gear via plural annular friction springs. The friction springs are disposed between an inner periphery face of a main body portion of the large diameter gear and a tubular portion of the small diameter gear, side by side along an axial direction of the two gears. Consequently, a radial direction enlargement of the large diameter gear and small diameter gear due to space for disposing the friction springs may be restrained. Moreover, the operation torque of the overload release mechanism may be adjusted stepwise by changing the number of the friction springs to be used, in accordance with requirements.
摘要翻译：提供一种能够减小过载释放机构的尺寸并且容易调节过载释放机构的操作扭矩的织带卷取装置。在这种织带卷取装置的过载释放机构中，大直径齿轮的旋转力通过多个环形摩擦弹簧传递到小直径齿轮。摩擦弹簧沿着两个齿轮的轴向并排设置在大直径齿轮的主体部分的内周面和小直径齿轮的管状部分之间。因此，可以抑制由于设置摩擦弹簧的空间而引起的大直径齿轮和小直径齿轮的径向扩大。此外，可以根据要求通过改变要使用的摩擦弹簧的数量来逐步地调节过载释放机构的操作扭矩。

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