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1. 发明授权

US07385079B2 Process for producing α-substituted acrylic norbornanyyl compounds 有权
标题翻译：制备α-取代的丙烯酸降冰片烷基化合物的方法
公开(公告)号：US07385079B2
公开(公告)日：2008-06-10
申请号：US10995335
申请日：2004-11-24
申请人： Takeo Komata , Shinya Akiba , Satoru Miyazawa , Takahisa Tada , Yusuke Kuramoto , Seiji Murata
发明人： Takeo Komata , Shinya Akiba , Satoru Miyazawa , Takahisa Tada , Yusuke Kuramoto , Seiji Murata
IPC分类号： C07C69/52
CPC分类号： C07C67/08 , C07C2602/42 , C07C69/533 , C07C69/54
摘要： A process for producing an α-substituted acrylic norbornanyl compound represented by the formula [3] includes reacting an α-substituted acrylic acid anhydride represented by the formula [1] with a substituted norbornanyl alcohol represented by the formula [2]. wherein R1 represents a hydrogen atom, methyl group, ethyl group, n-propyl group, isopropyl group, n-butyl group, sec-butyl group, tert-butyl group, fluoromethyl group, difluoromethyl group, trifluoromethyl group, or perfluoroethyl group, and wherein one of R2, R3 and R4 is a CF3C(CF3)(OH)CH2— group, and each of the other two of R2, R3 and R4 is a hydrogen.
摘要翻译：由式[3]表示的α-取代的丙烯酸降冰片烷基化合物的制备方法包括使由式[1]表示的α-取代的丙烯酸酐与由式[2]表示的取代的降冰片烷基酯反应。其中R 1表示氢原子，甲基，乙基，正丙基，异丙基，正丁基，仲丁基，叔丁基，氟甲基，二氟甲基，三氟甲基或全氟乙基，其中R 2，R 3和R 4之一是CF 3 N C（CF 3）（OH）CH 2 - 基团，R 2，R 3，R 3， R 4和R 4是氢。

2. 发明申请

US20050131248A1 Process for producing alpha-substituted acrylic norbornanyyl compounds 有权
标题翻译：制备α-取代的丙烯酸降冰片烷基化合物的方法
公开(公告)号：US20050131248A1
公开(公告)日：2005-06-16
申请号：US10995335
申请日：2004-11-24
申请人： Takeo Komata , Shinya Akiba , Satoru Miyazawa , Takahisa Tada , Yusuke Kuramoto , Seiji Murata
发明人： Takeo Komata , Shinya Akiba , Satoru Miyazawa , Takahisa Tada , Yusuke Kuramoto , Seiji Murata
IPC分类号： C07C67/08 , C07C69/52
CPC分类号： C07C67/08 , C07C2602/42 , C07C69/533 , C07C69/54
摘要： A process for producing an α-substituted acrylic norbornanyl compound represented by the formula [3] includes reacting an α-substituted acrylic acid anhydride represented by the formula [1] with a substituted norbornanyl alcohol represented by the formula [2]. wherein R1 represents a hydrogen atom, methyl group, ethyl group, n-propyl group, isopropyl group, n-butyl group, sec-butyl group, tert-butyl group, fluoromethyl group, difluoromethyl group, trifluoromethyl group, or perfluoroethyl group, and wherein one of R2, R3 and R4 is a CF3C(CF3)(OH)CH2— group, and each of the other two of R2, R3 and R4 is a hydrogen.
摘要翻译：由式[3]表示的α-取代的丙烯酸降冰片烷基化合物的制备方法包括使由式[1]表示的α-取代的丙烯酸酐与由式[2]表示的取代的降冰片烷基酯反应。其中R 1表示氢原子，甲基，乙基，正丙基，异丙基，正丁基，仲丁基，叔丁基，氟甲基，二氟甲基，三氟甲基或全氟乙基，其中R 2，R 3和R 4之一是CF 3 N C（CF 3）（OH）CH 2 - 基团，R 2，R 3，R 3， R 4和R 4是氢。

3. 发明授权

US07199262B2 3-Hydroxypropyl ester of 2-trifluoromethylacrylic acid and process for producing same 有权
标题翻译： 2-三氟甲基丙烯酸3-羟丙酯及其制备方法
公开(公告)号：US07199262B2
公开(公告)日：2007-04-03
申请号：US11152144
申请日：2005-06-15
申请人： Takahisa Tada , Seiji Murata , Akihiro Fukui , Junji Negishi
发明人： Takahisa Tada , Seiji Murata , Akihiro Fukui , Junji Negishi
IPC分类号： C07C69/52 , C07C69/34 , C07C69/63
CPC分类号： C07C69/653
摘要： The invention relates to a novel compound, 3-hydroxypropyl ester of 2-trifluoromethyl acrylic acid, represented by the formula [1]. The invention further relates to a process for producing the compound. This process includes reacting 2-trifluoromethylacrylic halide represented by the formula [2], wherein the halogen atom is F or Cl, with 1,3-propanediol represented by the formula [3], in the presence of a base
摘要翻译：本发明涉及由式[1]表示的2-三氟甲基丙烯酸的新型化合物3-羟丙基酯。本发明还涉及一种生产该化合物的方法。该方法包括使由式[2]表示的2-三氟甲基丙烯酰卤与式[3]表示的1,3-丙二醇反应，其中卤素原子为F或Cl，在碱的存在下

4. 发明申请

US20060009653A1 3-Hydroxypropyl ester of 2-trifluoromethylacrylic acid and process for producing same 有权
标题翻译： 2-三氟甲基丙烯酸3-羟丙酯及其制备方法
公开(公告)号：US20060009653A1
公开(公告)日：2006-01-12
申请号：US11152144
申请日：2005-06-15
申请人： Takahisa Tada , Seiji Murata , Akihiro Fukui , Junji Negishi
发明人： Takahisa Tada , Seiji Murata , Akihiro Fukui , Junji Negishi
IPC分类号： C07C69/653
CPC分类号： C07C69/653
摘要： The invention relates to a novel compound, 3-hydroxypropyl ester of 2-trifluoromethyl acrylic acid, represented by the formula [1]. The invention further relates to a process for producing the compound. This process includes reacting 2-trifluoromethylacrylic halide represented by the formula [2], wherein the halogen atom is F or Cl, with 1,3-propanediol represented by the formula [3], in the presence of a base.
摘要翻译：本发明涉及由式[1]表示的2-三氟甲基丙烯酸的新型化合物3-羟丙基酯。本发明还涉及一种生产该化合物的方法。该方法包括使由式[2]表示的2-三氟甲基丙烯酰卤反应，其中卤素原子为F或Cl，与由式[3]表示的1,3-丙二醇在碱存在下反应。

5. 发明授权

US5070208A Method for crystallization of optically active tryptophan 失效
标题翻译：光学活性色氨酸结晶方法
公开(公告)号：US5070208A
公开(公告)日：1991-12-03
申请号：US670182
申请日：1991-03-15
申请人： Kenichi Yarita , Takahisa Tada , Ryuichiro Kasatani
发明人： Kenichi Yarita , Takahisa Tada , Ryuichiro Kasatani
IPC分类号： C07D209/20
CPC分类号： C07D209/20
摘要： Optically active tryptophan is crystallized by a modification of a method of crystrallization of optically active tryptophan through neutralization by mixing an acidic or alkaline aqueous solution of optically active tryptophan, which is obtained by the removal of impurities from an acidic or alkaline aqueous solution of optically active tryptophan containing impurities which inhibit flocculation and crystallization of optically active tryptophan, with an alkali or an acid, by combining portions of an alkali or acid with portions of an acidic or alkaline aqueous solution of optically active tryptophan, from which the impurities have been removed, thereby neutralizing the aqueous solution containing optically active tryptophan such that the pH of the solution to be crystallized is kept in a range of 3 to 8, and simultaneously crystallizing optically active tryptophan as flocculated crystals.
摘要翻译：通过将光学活性色氨酸的酸性或碱性水溶液通过从光学活性的酸性或碱性水溶液中除去杂质获得的光学活性色氨酸水溶液，通过中和来改变光学活性色氨酸的冷冻方法，使光学活性色氨酸结晶化含有杂质的色氨酸，其通过将碱或酸的一部分与已经除去杂质的酸性或碱性光学活性色氨酸水溶液的部分组合而抑制光学活性色氨酸的絮凝和结晶，用碱或酸，从而中和含有光学活性色氨酸的水溶液，使得待结晶的溶液的pH保持在3至8的范围内，同时使旋光色氨酸作为絮凝晶体结晶。

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