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1. 发明授权

US07405315B2 Mesoporous silica and process for producing the same 失效
标题翻译：介孔二氧化硅及其制备方法
公开(公告)号：US07405315B2
公开(公告)日：2008-07-29
申请号：US10716427
申请日：2003-11-20
申请人： Takashi Tatsumi , Hideaki Yoshitake , Toshiyuki Yokoi , Shunai Che , Kazutami Sakamoto
发明人： Takashi Tatsumi , Hideaki Yoshitake , Toshiyuki Yokoi , Shunai Che , Kazutami Sakamoto
IPC分类号： C07F7/04
CPC分类号： C01B37/02 , C07B2200/11 , C07F7/1804
摘要： (A) An anionic surfactant, (B) a silicate monomer and (C) a basic silane are mixed in water or a mixed solvent of a water-miscible organic solvent and water to obtain a mesoporous silica complex having mesopores with a uniform size, the anionic surfactant Component (A) is removed by washing the resultant mesoporous silica complex with an acidic aqueous solution, a water-miscible organic solvent or an aqueous solution thereof to obtain a mesoporous silica outer shell utilizing the structure of the mesoporous silica complex as a template, and the mesoporous silica complex or the mesoporous silica outer shell is calcined to obtain a mesoporous silica. The mesoporous silica can be synthesized in this manner utilizing the anionic surfactant micelle with a remarkably low affinity to the silicate monomer.
摘要翻译：（A）阴离子表面活性剂，（B）硅酸盐单体和（C）碱性硅烷在水或水混溶性有机溶剂与水的混合溶剂中混合，得到具有均匀尺寸的介孔的介孔二氧化硅配合物，通过用酸性水溶液，水溶性有机溶剂或其水溶液洗涤所得介孔二氧化硅配合物来除去阴离子表面活性剂组分（A），以获得使用介孔二氧化硅络合物的结构的介孔二氧化硅外壳作为模板和介孔二氧化硅配合物或介孔二氧化硅外壳进行煅烧，得到介孔二氧化硅。可以以这种方式利用对硅酸盐单体的亲和力非常低的阴离子表面活性剂胶束来合成介孔二氧化硅。

2. 发明授权

US08063114B2 Inorganic mesoporous material having chiral twisted structure and process for producing the same 失效
标题翻译：具有手性扭转结构的无机介孔材料及其制造方法
公开(公告)号：US08063114B2
公开(公告)日：2011-11-22
申请号：US11579203
申请日：2005-04-28
申请人： Takashi Tatsumi , Shunai Che , Kazutami Sakamoto
发明人： Takashi Tatsumi , Shunai Che , Kazutami Sakamoto
IPC分类号： C08G77/00 , C08G63/44
CPC分类号： C01B37/02 , B01D15/3833 , B01J20/103 , B01J20/28007 , B01J20/28083 , B01J20/283 , B01J20/29 , B01J20/3057 , B22F1/0025 , B82Y30/00 , C30B29/16 , C30B29/605
摘要： A chiral inorganic mesoporous material characterized by having a chiral twisted structure and being mesoporous; a process for producing the material; and a method of using the material. The process for inorganic mesoporous material production is a method in which one or more polymerizable inorganic monomers selected from the group consisting of polymerizable inorganic monomers and polymerizable inorganic monomers having a functional group capable of having a charge are polymerized in the presence of a solvent using as a template a self-assembly of a chiral surfactant such as an N-(higher alkanoyl)amino acid salt. Examples of the use of the inorganic mesoporous material include the separation of racemates and reaction fields for asymmetric syntheses.
摘要翻译：一种手性无机介孔材料，其特征在于具有手性扭曲结构并且具有介孔性; 一种生产该材料的方法; 以及使用该材料的方法。无机介孔材料生产方法是一种或多种选自可聚合无机单体和具有可带电荷的官能团的可聚合无机单体的可聚合无机单体在溶剂存在下使用如下方法聚合的方法：模板是手性表面活性剂如N-（高级烷酰基）氨基酸盐的自组装。使用无机介孔材料的实例包括外消旋体的分离和不对称合成的反应场。

3. 发明申请

US20090043003A1 INORGANIC MESOPOROUS MATERIAL HAVING CHIRAL TWISTED STRUCTURE AND PROCESS FOR PRODUCING THE SAME 失效
标题翻译：无纺织物材料，具有双向结构及其制造方法
公开(公告)号：US20090043003A1
公开(公告)日：2009-02-12
申请号：US11579203
申请日：2005-04-28
申请人： Takashi Tatsumi , Shunai Che , Kazutami Sakamoto
发明人： Takashi Tatsumi , Shunai Che , Kazutami Sakamoto
IPC分类号： C08L79/00 , C08J9/00 , C23C16/44
CPC分类号： C01B37/02 , B01D15/3833 , B01J20/103 , B01J20/28007 , B01J20/28083 , B01J20/283 , B01J20/29 , B01J20/3057 , B22F1/0025 , B82Y30/00 , C30B29/16 , C30B29/605
摘要： A chiral inorganic mesoporous material characterized by having a chiral twisted structure and being mesoporous; a process for producing the material; and a method of using the material. The process for inorganic mesoporous material production is a method in which one or more polymerizable inorganic monomers selected from the group consisting of polymerizable inorganic monomers and polymerizable inorganic monomers having a functional group capable of having a charge are polymerized in the presence of a solvent using as a template a self-assembly of a chiral surfactant such as an N-(higher alkanoyl)amino acid salt. Examples of the use of the inorganic mesoporous material include the separation of racemates and reaction fields for asymmetric syntheses.
摘要翻译：一种手性无机介孔材料，其特征在于具有手性扭曲结构并且具有介孔性; 一种生产该材料的方法; 以及使用该材料的方法。无机介孔材料生产方法是一种或多种选自可聚合无机单体和具有可带电荷的官能团的可聚合无机单体的可聚合无机单体在溶剂存在下使用如下方法聚合的方法：模板是手性表面活性剂如N-（高级烷酰基）氨基酸盐的自组装。使用无机介孔材料的实例包括外消旋体的分离和不对称合成的反应场。

4. 发明申请

US20120016045A1 Process For The Preparation Of Layered Silicates 审中-公开
标题翻译：层状硅酸盐的制备方法
公开(公告)号：US20120016045A1
公开(公告)日：2012-01-19
申请号：US13254022
申请日：2010-03-03
申请人： Bilge Yilmaz , Ulrich Müller , Meike Pfaff , Hermann Gies , Feng-Shou Xiao , Takashi Tatsumi , Dirk de Vos , Xinhe Bao , Weiping Zhang
发明人： Bilge Yilmaz , Ulrich Müller , Meike Pfaff , Hermann Gies , Feng-Shou Xiao , Takashi Tatsumi , Dirk de Vos , Xinhe Bao , Weiping Zhang
IPC分类号： C08J9/00 , C01B33/20
CPC分类号： C01B33/20 , B01J20/10 , B01J20/30 , B01J21/16 , B01J29/049 , C01B33/38 , C01B37/00 , C01B37/02 , C01B39/02 , C01B39/04
摘要： The present invention relates to a process for the preparation of a layered silicate containing at least silicon and oxygen, comprising (1) providing a mixture containing silica and/or at least one silica precursor, water, at least one tetraalkylammonium compound selected from the group consisting of diethyldimethylammonium compound, a triethylmethylammonium compound, and a mixture of a diethyldimethylammonium and a triethylmethylammonium compound, and at least one base, and optionally at least one suitable seeding material; and (2) heating of the mixture obtained according to (1) under autogenous pressure (hydrothermal conditions) to a temperature in the range of from to 120 to 160° C. for a period in the range of from 5 to 10 days to give a suspension containing the layered silicate.
摘要翻译：本发明涉及一种制备至少含硅和氧的层状硅酸盐的方法，其包括（1）提供含有二氧化硅和/或至少一种二氧化硅前体的混合物，水，至少一种选自以下的四烷基铵化合物由二乙基二甲基铵化合物，三乙基甲基铵化合物和二乙基二甲基铵和三乙基甲基铵化合物的混合物组成，以及至少一种碱和任选的至少一种合适的接种材料; 和（2）根据（1）获得的混合物在自生压力（水热条件）下加热至120至160℃的温度范围为5至10天，得到含有层状硅酸盐的悬浮液。

5. 发明申请

US20120004332A1 Metal-Bridged Pillared Silicate Compounds And Process For Their Production 有权
标题翻译：金属桥接的硅酸盐化合物及其生产工艺
公开(公告)号：US20120004332A1
公开(公告)日：2012-01-05
申请号：US13175125
申请日：2011-07-01
申请人： Bilge Yilmaz , Ulrich Müller , Trees De Baerdemaeker , Hermann Gies , Feng-Shou Xiao , Takashi Tatsumi , Xinhe Bao , Weiping Zhang , Dirk de Vos
发明人： Bilge Yilmaz , Ulrich Müller , Trees De Baerdemaeker , Hermann Gies , Feng-Shou Xiao , Takashi Tatsumi , Xinhe Bao , Weiping Zhang , Dirk de Vos
IPC分类号： C08J9/00 , B01J29/04 , C07C2/00 , C01B39/00
CPC分类号： B01J29/049 , C01B33/20 , C01B37/005 , C01B39/026 , C01B39/48 , C07C2/84 , C07C2523/28 , C07C2523/72 , C07C2523/755 , C07C2523/883 , C07C2523/885
摘要： The present invention relates to a pillared silicate compound comprising a layered silicate structure, and bridging metal atoms located between adjacent silicate layers of the silicate structure, wherein said bridging metal atoms form at least one covalent bond to each of the adjacent silicate layers, as well as a process for the preparation of a pillared silicate compound, and further includes a pillared silicate compound obtainable and or obtained according to said process, as well as a method of catalyzing a chemical reaction comprising the step of contacting one or more chemical compounds with the any of the aforementioned pillared silicate compounds.
摘要翻译：本发明涉及包含层状硅酸盐结构的柱状硅酸盐化合物和位于硅酸盐结构的相邻硅酸盐层之间的桥连金属原子，其中所述桥连金属原子与每个相邻的硅酸盐层形成至少一个共价键作为制备柱状硅酸盐化合物的方法，还包括根据所述方法可获得和/或获得的柱状硅酸盐化合物，以及催化化学反应的方法，包括使一种或多种化学化合物与任何上述柱状硅酸盐化合物。

6. 发明授权

US4910607A Image processing device of multifunctional type 失效
标题翻译：多功能型图像处理装置
公开(公告)号：US4910607A
公开(公告)日：1990-03-20
申请号：US102606
申请日：1987-09-30
申请人： Toshiro Kita , Susumu Genba , Masato Takemoto , Takashi Tatsumi , Toshiyuki Itoga , Yutaka Iizuka , Satoshi Tominaga , Mikio Higashiyama , Akira Tanimoto , Shinji Okamoto , Toshihiko Yoshida
发明人： Toshiro Kita , Susumu Genba , Masato Takemoto , Takashi Tatsumi , Toshiyuki Itoga , Yutaka Iizuka , Satoshi Tominaga , Mikio Higashiyama , Akira Tanimoto , Shinji Okamoto , Toshihiko Yoshida
IPC分类号： H04M11/00 , G06F3/00 , G06T1/00 , H04N1/00 , H04N1/32
CPC分类号： H04N1/00238 , G06F3/002 , H04N1/00206 , H04N1/00236 , H04N1/00241 , H04N1/32496 , H04N1/32502 , H04N1/32512 , H04N1/32529 , H04N1/00204 , H04N2201/0074 , H04N2201/0081 , H04N2201/0082 , H04N2201/0086
摘要： An image processing device for controlling data transfer includes an image scanner, an image printer, a facsimile control unit, bus lines for data transfer, a bidirectional parallel interface unit, and a main CPU in a housing. The device is connected to an external data processing device through the parallel interface unit. In addition to the functions which are obtained independent from the external data processing device, the image processing device realizes various kinds of functions by controlling the image scanner, the image printer facsimile control unit and the interface unit by the main CPU in response to commands from the data processing device. As a result, various kinds of image processing functions are carried out.
摘要翻译：用于控制数据传送的图像处理装置包括图像扫描器，图像打印机，传真控制单元，用于数据传送的总线，双向并行接口单元和壳体中的主CPU。该设备通过并行接口单元连接到外部数据处理设备。除了独立于外部数据处理装置获得的功能之外，图像处理装置通过主CPU响应于来自主CPU的命令来控制图像扫描器，图像打印机传真控制单元和接口单元来实现各种功能数据处理设备。结果，执行各种图像处理功能。

7. 发明授权

US4876134A Laminated panel having a stainless steel foil core and a process for producing the panel 失效
标题翻译：具有不锈钢箔芯的层压板及其制造方法
公开(公告)号：US4876134A
公开(公告)日：1989-10-24
申请号：US105071
申请日：1987-10-05
申请人： Yoshiro Saitoh , Takashi Tatsumi
发明人： Yoshiro Saitoh , Takashi Tatsumi
IPC分类号： B32B3/12
CPC分类号： B32B3/12 , Y10T156/1003 , Y10T156/1051 , Y10T156/1085 , Y10T428/1234 , Y10T428/12417 , Y10T428/236 , Y10T428/24149 , Y10T428/24165 , Y10T428/24694
摘要： A process for producing a laminated panel core made of stainless steel includes the step of preparing a core of the laminated panel by subjecting stainless steel foils to repeated outward and inward foldings in a constant mode in one direction to make a plurality of multi-layered folded sheets of stainless steel. An adhesive is applied to a portion of the surfaces of the folded sheets and a desired number of the multi-layered sheets are laminated. The adhesive causes the sheets to adhere to one another in the areas of application of the adhesive. The laminate is sliced in a plane perpendicular to the plane generally defined by each of the multi-layered sheets into an appropriate small thickness and is extended and deformed in a plane parallel to the plane in which the laminate is sliced and in the direction of lamination of the sheets. A multi-layered sheet for use in a process for forming laminated panels and a stainless steel foil core for use in a laminated panel are also disclosed.
摘要翻译：制造由不锈钢制成的层压板芯的方法包括通过使不锈钢箔沿一个方向以恒定模式重复向外和向内折叠来制备层压板的芯的步骤，以制造多个多层折叠不锈钢板。将粘合剂施加到折叠片材的一部分表面，并且层叠所需数量的多层片材。粘合剂使得片材在施加粘合剂的区域中彼此粘合。层叠体在垂直于通常由多层板的每一层限定的平面的平面中切片成适当的小厚度，并且在平行于层压板切割的平面的平面和层叠方向上延伸和变形的床单。还公开了一种用于形成层压板的方法的多层片和用于层压板的不锈钢箔芯。

8. 发明授权

US09260313B2 Process for the preparation of pillared silicates 有权
标题翻译：柱状硅酸盐的制备方法
公开(公告)号：US09260313B2
公开(公告)日：2016-02-16
申请号：US13254032
申请日：2010-03-03
申请人： Bilge Yilmaz , Ulrich Müller , Feng-Shou Xiao , Hermann Gies , Takashi Tatsumi , Dirk de Vos , Xinhe Bao , Weiping Zhang
发明人： Bilge Yilmaz , Ulrich Müller , Feng-Shou Xiao , Hermann Gies , Takashi Tatsumi , Dirk de Vos , Xinhe Bao , Weiping Zhang
IPC分类号： B01J29/04 , C01B39/00 , C04B35/622 , C01B37/00 , C01B31/02 , C01B37/02 , C01B39/02 , C01B39/46 , C01B39/48 , C04B35/16
CPC分类号： C01B37/005 , C01B32/05 , C01B37/02 , C01B39/026 , C01B39/46 , C01B39/48 , C04B35/16 , C04B2235/3201 , C04B2235/3222 , C04B2235/3427 , C04B2235/5409
摘要： The present invention relates to a process for the preparation of a silicate compound, comprising (1) providing at least one layered silicate; and (2) mixing said layered silicate with water and at least one silicon containing compound according to formula R4-mSi[—(SiR2)n—R]m wherein at least one residue R is a leaving group and none of the residues R contains Si; m is 0, 1, 2, 3, or 4; and n is an integer greater than or equal to 0.
摘要翻译：本发明涉及一种制备硅酸盐化合物的方法，包括（1）提供至少一种层状硅酸盐; 和（2）将所述层状硅酸盐与水和至少一种根据式R 4-m Si [ - （SiR 2）n -R] m的含硅化合物混合，其中至少一个残基R是离去基团，并且没有残基R包含硅; m为0,1,2,3或4; 并且n是大于或等于0的整数。

9. 发明申请

US20130101503A1 Process For The Production Of A Core/Shell Zeolitic Material Having A CHA Framework Structure 有权
标题翻译：具有CHA框架结构的核/壳型沸石材料的生产工艺
公开(公告)号：US20130101503A1
公开(公告)日：2013-04-25
申请号：US13616834
申请日：2012-09-14
申请人： Bilge Yilmaz , Ulrich Müller , Feng-Shou Xiao , Takashi Tatsumi , Dirk de Vos , Xinhe Bao , Weiping Zhang , Hermann Gies , Hiroyuki Imai , Bart Tijsebaert , Limin Ren , Chengguan Yang
发明人： Bilge Yilmaz , Ulrich Müller , Feng-Shou Xiao , Takashi Tatsumi , Dirk de Vos , Xinhe Bao , Weiping Zhang , Hermann Gies , Hiroyuki Imai , Bart Tijsebaert , Limin Ren , Chengguan Yang
IPC分类号： C01B39/00 , C01B39/54
CPC分类号： C01B39/00 , B01D53/02 , B01D53/9418 , B01D2255/2025 , B01D2255/20707 , B01D2255/20715 , B01D2255/2092 , B01D2255/2094 , B01D2255/50 , B01J29/005 , B01J29/7015 , B01J29/83 , B01J29/84 , B01J29/85 , B01J35/002 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1066 , B01J37/02 , B01J37/0221 , B01J37/023 , B01J2229/62 , C01B37/08 , C01B39/48 , C01B39/54 , C01P2002/72 , C01P2004/03 , C01P2006/12 , C07C1/20 , C07C2529/85 , C10G3/49 , C10G11/18 , Y02P20/52 , Y02P30/20 , C07C11/02
摘要： The present invention relates to a process for the preparation of a zeolitic material having a CHA framework structure, said zeolitic material comprising zeolite crystals having a core-shell structure, wherein said process comprises the steps of (1) providing a mixture comprising one or more sources for Z2O5, one or more sources for X2O3, optionally one or more structure directing agents, and seed crystals having a CHA framework structure, wherein the CHA framework structure of the seed crystals comprises YO2, X2O3, and optionally Z2O5, and wherein the seed crystals have a diameter of 450 nm or greater; (2) crystallizing the mixture provided in (1) to afford zeolite crystals comprising a core of seed crystal provided in step (1) and a shell crystallized on the seed crystal; wherein Z is a pentavalent element, Y is a tetravalent element, and X is a trivalent element.
摘要翻译：本发明涉及一种制备具有CHA骨架结构的沸石材料的方法，所述沸石材料包含具有核 - 壳结构的沸石晶体，其中所述方法包括以下步骤：（1）提供包含一种或多种 Z 2 O 5的源，X 2 O 3，任选的一种或多种结构导向剂的一种或多种来源，以及具有CHA骨架结构的晶种，其中晶种的CHA骨架结构包含YO 2，X 2 O 3和任选的Z 2 O 5，并且其中所述种子晶体的直径为450nm以上; （2）使（1）中提供的混合物结晶，得到包含步骤（1）中提供的晶种核心的沸石晶体和在晶种上结晶的壳; 其中Z为五价元素，Y为四价元素，X为三价元素。

10. 发明申请

US20110313226A1 Zeolitic Materials of the LEV-Type Structure And Methods For Their Production 审中-公开
标题翻译： LEV型结构的沸石材料及其生产方法
公开(公告)号：US20110313226A1
公开(公告)日：2011-12-22
申请号：US13163430
申请日：2011-06-17
申请人： Bilge Yilmaz , Ulrich Müller , Bibiana Andrea Betancur Moreno , Hermann Gies , Feng-Shou Xiao , Takashi Tatsumi , Xinhe Bao , Weiping Zhang , Dirk de Vos , Meike Pfaff , Bin Xie , Haiyan Zhang
发明人： Bilge Yilmaz , Ulrich Müller , Bibiana Andrea Betancur Moreno , Hermann Gies , Feng-Shou Xiao , Takashi Tatsumi , Xinhe Bao , Weiping Zhang , Dirk de Vos , Meike Pfaff , Bin Xie , Haiyan Zhang
IPC分类号： C07C1/20 , C07C2/00 , B01D53/94 , C01B39/00 , B01D53/56
CPC分类号： C01B39/48 , B01D2253/108 , B01D2255/50 , B01J20/186 , B01J20/2803 , B01J20/28042 , B01J20/28057 , B01J20/3007 , B01J20/3042 , B01J29/70 , C01B37/02 , C01B39/46 , C10G3/49 , C10G11/18 , C10G25/03 , C10G2300/405 , C10G2300/70 , Y02P30/20
摘要： Described is a process for the production of a zeolitic material having an LEV-type framework structure comprising YO2 and optionally comprising X2O3, wherein said process comprises: (1) preparing a mixture comprising one or more sources for YO2, one or more solvents, and optionally comprising seed crystals; and (2) crystallizing the mixture obtained in step (1);wherein Y is a tetravalent element, and X is a trivalent element, wherein the zeolitic material optionally comprises one or more alkali metals M, wherein the molar ratio of the total amount of the one or more solvents to the total amount of the one or more sources for YO2 based on YO2 is 9.5 or less, and wherein for crystallization temperatures of 175° C. or higher in step (2), the duration of crystallization at those temperatures is less than 14 d, as well as to a zeolitic material, preferably being obtainable or obtained according to the inventive process, said zeolitic material having an LEV-type framework structure comprising YO2 and X2O3, wherein the zeolitic material optionally comprises one or more alkali metals M, and wherein the zeolitic material displays an Y:X atomic ratio of from 1 to 9.4.
摘要翻译：描述了一种生产具有包含YO 2和任选地包含X 2 O 3的LEV型骨架结构的沸石材料的方法，其中所述方法包括：（1）制备包含一种或多种YO 2，一种或多种溶剂的来源的混合物，以及任选地包含晶种; 和（2）使步骤（1）中获得的混合物结晶; 其中Y是四价元素，X是三价元素，其中沸石材料任选地包含一种或多种碱金属M，其中一种或多种溶剂的总量与一种或多种溶剂的总量的摩尔比基于YO 2的YO 2的来源为9.5或更低，并且其中对于步骤（2）中的结晶温度为175℃或更高的温度，在这些温度下的结晶持续时间小于14天，以及沸石材料，所述沸石材料具有包含YO 2和X 2 O 3的LEV型骨架结构，其中所述沸石材料任选地包含一种或多种碱金属M，并且其中所述沸石材料显示Y：X原子比例为1〜9.4。

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