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1. 发明申请

US20070052131A1 Method of producing a weld-cut sealing/heat-shrinkable packaging film formed of a polyethylene terephthalate-based block copolymer polyester 审中-公开
标题翻译：由聚对苯二甲酸乙二醇酯类嵌段共聚物聚酯形成的熔接密封/热收缩性包装膜的制造方法
公开(公告)号：US20070052131A1
公开(公告)日：2007-03-08
申请号：US10572674
申请日：2004-09-21
申请人： Takashi Fujimaki , Yukio Kobayashi , Takashi Nakamoto , Hiroshi Shibano
发明人： Takashi Fujimaki , Yukio Kobayashi , Takashi Nakamoto , Hiroshi Shibano
IPC分类号： B29C71/00
CPC分类号： C08G59/42
摘要： A PET-based polyester packaging film capable of weld-cut sealing and heat-shrinkage refers to a film obtained by biaxially orienting a material prepared through block copolymerization of a PET/PETG/polyester elastomer with an epoxy resin and a catalyst. This film eliminates the most serious weak points in physical properties of conventional PET films, and is useful for packaging of books, bottlesets, food containers, etc., for general packaging, packaging of industrial materials, and the like, and is further useful in the field of packing and packaging of daily commodities, civil engineering and construction members, electric and electronic members, and automobile vehicle members, etc. Moreover, this film can be produced through effective use of the huge amount of recycled PET bottles and inexpensive PET for fiber as a prepolymer, and thus is also highly beneficial socially. Still further, even if incinerated after use, this film produces a combustion heat value lower than that of a polyethylene or polypropylene. Thus, this film barely damages incinerators or the like, and emits no toxic gases.
摘要翻译：能够进行切割密封和热收缩的PET系聚酯包装膜是指通过PET / PETG /聚酯弹性体与环氧树脂和催化剂的嵌段共聚制备的材料双轴取向而获得的膜。该膜消除了常规PET膜的物理性能中最严重的弱点，并且用于包装书籍，瓶子，食品容器等，用于一般包装，工业材料包装等，并且还可用于日用品包装和包装领域，土木工程施工人员，电气电子部件和汽车用品等。此外，该膜可以通过有效利用大量的回收PET瓶和廉价的PET来生产纤维作为预聚物，因此在社会上也是非常有益的。此外，即使在使用后焚烧，该膜产生低于聚乙烯或聚丙烯的燃烧热值。因此，该膜几乎不损坏焚烧炉等，并且不产生有毒气体。

2. 发明申请

US20060043646A1 Method of manufacturing heat-resistant mould articles made of polyethylene terephthalate polyesters 有权
标题翻译：制造由聚对苯二甲酸乙二醇酯聚酯制成的耐热模具制品的方法
公开(公告)号：US20060043646A1
公开(公告)日：2006-03-02
申请号：US10927118
申请日：2004-08-27
申请人： Yukio Kobayashi , Takashi Fujimaki , Takashi Nakamoto
发明人： Yukio Kobayashi , Takashi Fujimaki , Takashi Nakamoto
IPC分类号： B29C35/10 , B29C47/76 , B29C47/88 , B29C51/02 , B29C51/10
CPC分类号： C08J3/226 , B29C47/0004 , B29C47/0019 , B29C47/0021 , B29C47/0054 , B29C47/0057 , B29C47/8805 , B29C47/8845 , B29C47/90 , B29C47/904 , B29C51/002 , B29C51/10 , B29C67/246 , B29C2035/046 , B29C2791/006 , B29C2791/007 , B29K2063/00 , B29K2067/00 , B29K2105/0014 , B29K2105/256 , B29K2105/26 , B29K2995/0017 , B29K2995/0026 , B29L2007/002 , C08J2367/02 , C08J2467/00 , C08K5/098 , C08L63/00 , C08L67/02 , C08L2666/22
摘要： The present invention provides a method of manufacturing high-melting-tension heat-resistant transparent or opaque sheets, boards, and moulds from polyethylene terephthalate (PET). The method is characterised in that a mixture of: (1) PET polyester whose melt flow rate (MFR) is 45-130 g/10 minutes (a); (2) coupling agent master batch (f) comprising coupling agent (d) and substrate (e), wherein coupling agent (d) is a mixture of compounds containing 2 epoxy groups (b) and compounds containing 3 or more epoxy groups (c); and (3) catalyst master batch (i) comprising coupling reaction catalyst (g) and substrate (h); is melted in a reaction-extruder to give PET polyester whose MFR is 40 g/10 minutes or less. The resulting PET polyester is moulded into amorphous sheets or boards, and then heated again to a predetermined temperature to give transparent heat-resistant sheets or boards; or then vacuum-, pressure-, or vacuum-pressure-formed following heat-setting to give transparent heat-resistant or white opaque highly-heat-resistant mould articles.
摘要翻译：本发明提供一种由聚对苯二甲酸乙二醇酯（PET）制造高熔点耐热透明或不透明片材，板材和模具的方法。该方法的特征在于：（1）熔体流动速率（MFR）为45〜130g / 10分钟（a）的PET聚酯的混合物; （2）包含偶联剂（d）和底物（e）的偶联剂母料（f），其中偶联剂（d）是含有2个环氧基团（b）和含有3个或更多个环氧基团的化合物的混合物（c））; 和（3）包含偶联反应催化剂（g）和底物（h）的催化剂母料（i）; 在反应挤出机中熔融，得到MFR为40g / 10分钟以下的PET聚酯。将所得的PET聚酯模制成非晶片或板，然后再次加热至预定温度，得到透明的耐热片或板; 然后在热定型之后进行真空，压力或真空压力成形，以提供透明的耐热或白色不透明的高耐热模具制品。

3. 发明授权

US07993569B2 Method of manufacturing heat-resistant mould articles made of polyethylene terephthalate polyesters 有权
标题翻译：制造由聚对苯二甲酸乙二醇酯聚酯制成的耐热模具制品的方法
公开(公告)号：US07993569B2
公开(公告)日：2011-08-09
申请号：US10927118
申请日：2004-08-27
申请人： Yukio Kobayashi , Takashi Fujimaki , Takashi Nakamoto
发明人： Yukio Kobayashi , Takashi Fujimaki , Takashi Nakamoto
IPC分类号： B29C51/02 , B29C51/42
CPC分类号： C08J3/226 , B29C47/0004 , B29C47/0019 , B29C47/0021 , B29C47/0054 , B29C47/0057 , B29C47/8805 , B29C47/8845 , B29C47/90 , B29C47/904 , B29C51/002 , B29C51/10 , B29C67/246 , B29C2035/046 , B29C2791/006 , B29C2791/007 , B29K2063/00 , B29K2067/00 , B29K2105/0014 , B29K2105/256 , B29K2105/26 , B29K2995/0017 , B29K2995/0026 , B29L2007/002 , C08J2367/02 , C08J2467/00 , C08K5/098 , C08L63/00 , C08L67/02 , C08L2666/22
摘要： The present invention provides a method of manufacturing high-melting-tension heat-resistant transparent or opaque sheets, boards, and molds from polyethylene terephthalate (PET). The method is characterized in that a mixture of: (1) PET polyester whose melt flow rate (MFR) is 45-130 g/10 minutes (a); (2) coupling agent master batch (f) comprising coupling agent (d) and substrate (e), wherein coupling agent (d) is a mixture of compounds containing 2 epoxy groups (b) and compounds containing 3 or more epoxy groups (c); and (3) catalyst master batch (i) comprising coupling reaction catalyst (g) and substrate (h); is melted in a reaction-extruder to give PET polyester whose MFR is 40 g/10 minutes or less. The resulting PET polyester is molded into amorphous sheets or boards, and then heated again to a predetermined temperature to give transparent heat-resistant sheets or boards; or then vacuum-, pressure-, or vacuum-pressure-formed following heat-setting to give transparent heat-resistant or white opaque highly-heat-resistant mould articles.
摘要翻译：本发明提供一种由聚对苯二甲酸乙二醇酯（PET）制造高熔点耐热透明或不透明片材，板材和模具的方法。该方法的特征在于：（1）熔体流动速率（MFR）为45〜130g / 10分钟（a）的PET聚酯的混合物; （2）包含偶联剂（d）和底物（e）的偶联剂母料（f），其中偶联剂（d）是含有2个环氧基团（b）和含有3个或更多个环氧基团的化合物的混合物（c））; 和（3）包含偶联反应催化剂（g）和底物（h）的催化剂母料（i）; 在反应挤出机中熔融，得到MFR为40g / 10分钟以下的PET聚酯。将所得的PET聚酯模制成非晶片或板，然后再次加热至预定温度，得到透明的耐热片或板; 然后在热定型之后进行真空，压力或真空压力成形，以提供透明的耐热或白色不透明的高耐热模具制品。

4. 发明授权

US08258239B2 Production method of polyethylene terephthalate graft copolymerized resin and molded product thereof 有权
标题翻译：聚对苯二甲酸乙二醇酯接枝共聚树脂的制造方法及其成型体
公开(公告)号：US08258239B2
公开(公告)日：2012-09-04
申请号：US12667312
申请日：2007-12-28
申请人： Takashi Fujimaki , Yoshitomo Urata , Hiroshi Shibano
发明人： Takashi Fujimaki , Yoshitomo Urata , Hiroshi Shibano
IPC分类号： C08L67/03
CPC分类号： C08G63/916 , C08J9/04 , C08J2367/02 , C08L63/00
摘要： The present invention provides a method of producing a polyethylene terephthalate graft copolymerized resin, comprising subjecting the following mixture to a homogeneous reaction at a temperature of 250° C. or higher to impart a high melt viscosity to the mixture, the mixture containing (A) 100 parts by weight of a polyethylene terephthalate polyester as a main material, (B) 0.01 to 2 parts by weight of a polymeric polyfunctional epoxy compound containing 7 to 100 epoxy groups in a molecule and having a molecular weight of 1,000 to 300,000 as a coupling agent, (C) 0.01 to 1 part by weight of a metal salt of an organic acid as a coupling reaction catalyst, and (D) 0 to 100 parts by weight of an aromatic alicyclic polyester and/or an aromatic aliphatic polyester each having a carboxyl group in an aromatic nucleus as an auxiliary material.
摘要翻译：本发明提供了一种聚对苯二甲酸乙二醇酯接枝共聚树脂的制造方法，其特征在于，在250℃以上的温度下对下述混合物进行均相反应，赋予混合物高熔融粘度，含有（A） 100重量份的聚对苯二甲酸乙二醇酯聚酯作为主要材料，（B）0.01至2重量份的分子中含有7至100个环氧基并且分子量为1,000至300,000的环氧基的聚合多官能环氧化合物作为偶联剂（C）0.01〜1重量份的作为偶联反应催化剂的有机酸的金属盐，和（D）0〜100重量份的芳族脂环族聚酯和/或芳香族脂肪族聚酯，芳族核中的羧基作为辅助材料。

5. 发明申请

US20100201015A1 PRODUCTION METHOD OF POLYETHYLENE TEREPHTHALATE GRAFT COPOLYMERIZED RESIN AND MOLDED PRODUCT THEREOF 有权
标题翻译：聚乙烯三烯丙酸酯共聚树脂及其成型产品的生产方法
公开(公告)号：US20100201015A1
公开(公告)日：2010-08-12
申请号：US12667312
申请日：2007-12-28
申请人： Takashi Fujimaki , Yoshitomo Urata , Hiroshi Shibano
发明人： Takashi Fujimaki , Yoshitomo Urata , Hiroshi Shibano
IPC分类号： C08L67/02 , B29C47/14 , B29C44/20
CPC分类号： C08G63/916 , C08J9/04 , C08J2367/02 , C08L63/00
摘要： The present invention provides a method of producing a polyethylene terephthalate graft copolymerized resin, comprising subjecting the following mixture to a homogeneous reaction at a temperature of 250° C. or higher to impart a high melt viscosity to the mixture, the mixture containing (A) 100 parts by weight of a polyethylene terephthalate polyester as a main material, (B) 0.01 to 2 parts by weight of a polymeric polyfunctional epoxy compound containing 7 to 100 epoxy groups in a molecule and having a molecular weight of 1,000 to 300,000 as a coupling agent, (C) 0.01 to 1 part by weight of a metal salt of an organic acid as a coupling reaction catalyst, and (D) 0 to 100 parts by weight of an aromatic alicyclic polyester and/or an aromatic aliphatic polyester each having a carboxyl group in an aromatic nucleus as an auxiliary material.
摘要翻译：本发明提供了一种聚对苯二甲酸乙二醇酯接枝共聚树脂的制造方法，其特征在于，在250℃以上的温度下对下述混合物进行均相反应，赋予混合物高熔融粘度，含有（A） 100重量份的聚对苯二甲酸乙二醇酯聚酯作为主要材料，（B）0.01至2重量份的分子中含有7至100个环氧基并且分子量为1,000至300,000的环氧基的聚合多官能环氧化合物作为偶联剂（C）0.01〜1重量份的作为偶联反应催化剂的有机酸的金属盐，和（D）0〜100重量份的芳族脂环族聚酯和/或芳香族脂肪族聚酯，芳族核中的羧基作为辅助材料。

6. 发明授权

US06803442B2 Masterbatch method for processing polyester resin and articles thereof 失效
标题翻译：用于加工聚酯树脂的母粒方法及其制品
公开(公告)号：US06803442B2
公开(公告)日：2004-10-12
申请号：US10297177
申请日：2002-12-03
申请人： Takashi Fujimaki , Yukio Kobayashi , Yoshitomo Urata , Toshio Tanaka
发明人： Takashi Fujimaki , Yukio Kobayashi , Yoshitomo Urata , Toshio Tanaka
IPC分类号： C08G6302
CPC分类号： C08J3/226 , C08J11/04 , C08J2367/00 , C08J2367/02 , C08J2463/00 , Y02P20/143 , Y02W30/70
摘要： The present invention provides a masterbatch method for producing a polyester resin and articles thereof; comprising reacting following materials uniformly at a temperature equal to or greater than the melting point of a polyester, the materials comprising: (1) 100 parts by weight of saturated straight-chain polyester A; (2) 1 to 10 parts by weight of binder masterbatch D comprising: a mixture containing a compound having two epoxy groups and a compound having an average number of epoxy groups of 2.1 or more; (3) 0.25 to 10 parts by weight of catalyst masterbatch G comprising: a metal carboxylate, whereby the melt viscosity of the polyester increases so that the melt flow rate (MFR) becomes 50 g/10 min or less, and the degree of swelling of the polyester increases to between 5% and 200%, thus resulting in a high-quality resin having excellent mechanical properties. The resin can be advantageously used for films, sheets, foamed materials, pipes, cushioning, heat insulators, packing materials, and so forth.
摘要翻译：本发明提供一种生产聚酯树脂的母料及其制品; 包括在等于或大于聚酯熔点的温度下均匀地使下列材料反应，所述材料包括：（1）100重量份的饱和直链聚酯A; （2）1〜10重量份粘合剂母料D，其包含：含有具有两个环氧基的化合物和平均环氧基数为2.1以上的化合物的混合物; （3）0.25至10重量份的催化剂母料G，其包含：金属羧酸盐，由此聚酯的熔体粘度增加，使得熔体流动速率（MFR）变为50g / 10min或更小，并且溶胀度的聚酯增加到5％至200％之间，从而得到具有优异机械性能的高品质树脂。树脂可以有利地用于薄膜，片材，发泡材料，管材，缓冲，绝热体，包装材料等。

7. 发明申请

US20100006214A1 METHOD FOR PRODUCTION OF TRANSPARENT, HEAT-RESISTANT, OIL-RESISTANT LAMINATE NAME PLATE COMPRISING POLYETHYLENE TEREPHTHALATE 审中-公开
标题翻译：用于生产包含聚乙烯三烯丙酸酯的透明耐热，耐油层压板名称板的方法
公开(公告)号：US20100006214A1
公开(公告)日：2010-01-14
申请号：US12443923
申请日：2007-10-02
申请人： Takashi Fujimaki , Kiyohiko Yamada
发明人： Takashi Fujimaki , Kiyohiko Yamada
IPC分类号： B32B37/06 , B32B37/12
CPC分类号： B32B27/36 , B29C48/00 , B29C48/05 , B29C48/08 , B29C48/914 , B29C48/919 , B29C2795/002 , B29K2067/00 , B29K2995/0026 , B29L2007/004 , B29L2009/00 , B32B7/12 , B32B27/08 , B32B27/10 , B32B27/32 , B32B37/142 , B32B37/185 , B32B2250/03 , B32B2250/40 , B32B2307/306 , B32B2307/412 , B32B2307/518 , B32B2307/7265 , B32B2457/00 , B32B2605/00
摘要： Provided is a method of producing a transparent, heat-resistant, oil-resistant laminate name tag, which includes the steps of laminating a newly developed heat-resistant, oil-resistant polyethylene terephthalate (PET) resin and a adhesive polyolefin resin on each other to form a pouch film including a two-resin three-layered film (F), sandwiching a printed article (L4) having a moisture evaporation rate of 3% or less between the pouch films, and welding the resulting product by heating, in which the two-resin three-layered film (F) is formed of, from the outside: a first layer including a transparent, heat-resistant, stretched polyester film (L1); a second layer including a heat-resistant, oil-resistant, adhesive polyester film (L2); and a third layer including an adhesive polyolefin film (L3).
摘要翻译：提供一种透明，耐热，耐油层压板名称的制造方法，其包括将新开发的耐热，耐油的聚对苯二甲酸乙二醇酯（PET）树脂和粘合性聚烯烃树脂彼此层合的步骤形成包含双树脂三层膜（F）的袋膜，夹在袋膜之间具有3％以下的水分蒸发率的印刷品（L4），并通过加热焊接所得到的产品，其中双树脂三层膜（F）由外部形成：包含透明耐热拉伸聚酯膜（L1）的第一层; 第二层，包括耐热，耐油，粘合的聚酯膜（L2）; 以及包含粘合性聚烯烃膜（L3）的第三层。

8. 发明授权

US5436056A Method of producing a high molecular weight aliphatic polyester and film thereof 失效
标题翻译：高分子量脂肪族聚酯的制造方法及其膜
公开(公告)号：US5436056A
公开(公告)日：1995-07-25
申请号：US107776
申请日：1993-08-18
申请人： Eiichiro Takiyama , Yoshitaka Hatano , Takashi Fujimaki , Shigekatu Seki , Takao Hokari , Tadayuki Hosogane , Noriaki Harigai
发明人： Eiichiro Takiyama , Yoshitaka Hatano , Takashi Fujimaki , Shigekatu Seki , Takao Hokari , Tadayuki Hosogane , Noriaki Harigai
IPC分类号： C08G18/42 , D06N7/04
CPC分类号： C08G18/4286 , C08G18/4241 , C08G2230/00 , C08G2310/00 , Y10T428/24355
摘要： A method for producing a high molecular weight aliphatic polyester, wherein:(A) 100 parts by weight of polyester (a) with a number average molecular weight of at least 10,000, and a weight average molecular weight of at least 30,000, and with end-groups that are substantially hydroxyl groups, and with a melting point of at least 60.degree. C., the polyester (a) having been obtained by reacting the following three ingredients: (i) a glycol ingredient; (ii) an aliphatic dicarboxylic acid ingredient; and (iii) a trifunctional or tetrafunctional ingredient reacts with(B) 0.1-3 parts by weight of a poly-isocyanate in a melted state of the polyester (a).The method provides a high molecular weight aliphatic polyester which has good properties and a melt viscosity required for molding and forming and has a wide molecular weight distribution. The high molecular weight aliphatic polyester is applicable to a variety of fields, such as films, moldings and formings, fibers, etc.
摘要翻译： PCT No.PCT / JP92 / 01671 Sec。 371日期：1993年8月18日 102（e）日期1993年8月18日PCT提交1992年12月21日PCT公布。第WO93 / 13152号公报日本特许公报1993年7月8日。一种高分子量脂肪族聚酯的制造方法，其中：（A）100重量份数均分子量为10,000以上的聚酯（a），重均分子量至少30,000，并且具有基本上为羟基的端基，并且熔点为至少60℃，所述聚酯（a）通过使以下三种成分反应获得：（i）二醇成分; （ii）脂族二羧酸成分; 和（iii）三官能或四官能组分与聚酯（a）熔融状态的（B）0.1-3重量份聚异氰酸酯反应。该方法提供了高分子量脂族聚酯，其具有良好的性能和模塑和成型所需的熔体粘度并且具有宽的分子量分布。高分子量脂肪族聚酯适用于各种领域，如薄膜，成型品，成型品，纤维等。

9. 发明授权

US5071708A Composite diamond grain 失效
标题翻译：复合金刚石颗粒
公开(公告)号：US5071708A
公开(公告)日：1991-12-10
申请号：US372367
申请日：1989-06-20
申请人： Kunio Komaki , Takashi Fujimaki , Masaaki Yanagisawa , Yoichi Hirose
发明人： Kunio Komaki , Takashi Fujimaki , Masaaki Yanagisawa , Yoichi Hirose
IPC分类号： C23C16/27 , C30B25/02
CPC分类号： C23C16/277 , C23C16/271 , C30B25/02 , C30B29/04 , Y10T428/2991 , Y10T428/30
摘要： A composite diamond grain which comprises a heat-resistant grain as a nucleus and discrete diamond crystal particles distributed on the surface of the grain or diamond crystal films formed to cover the entire surface of the grain and a method for producing the composite diamond grain by the vapor-phase process are disclosed. For the filament method which is one form of the vapor-phase method, tantalum is useful as the material for the filament. Since tantalum is susceptible of embrittlement by hydrogen, a treatment to be performed on tantalum for the elimination of this drawback is also disclosed.
摘要翻译： PCT No.PCT / JP88 / 01069 Sec。 371日期1989年6月20日 102（e）1989年6月20日PCT 1988年10月20日PCT。一种复合金刚石晶粒，其包含耐热晶粒作为核，而分散的金刚石晶粒分布在晶粒或金刚石晶体膜的表面上形成覆盖晶粒的整个表面，并且公开了通过气相法制造复合金刚石晶粒的方法。对于作为气相法的一种形式的丝线法，钽可用作丝的材料。由于钽容易受到氢的脆化，所以还公开了在钽上进行的用于消除该缺点的处理。

10. 发明授权

US5714569A Aliphatic polyester resin and method for producing same 失效
标题翻译：脂肪族聚酯树脂及其制造方法
公开(公告)号：US5714569A
公开(公告)日：1998-02-03
申请号：US696997
申请日：1996-08-21
申请人： Mitsuhiro Imaizumi , Hideharu Kimura , Ryutaro Fujihira , Yasushi Ichikawa , Jun Suzuki , Yoshihiro Moteki , Takashi Fujimaki , Eiichiro Takiyama
发明人： Mitsuhiro Imaizumi , Hideharu Kimura , Ryutaro Fujihira , Yasushi Ichikawa , Jun Suzuki , Yoshihiro Moteki , Takashi Fujimaki , Eiichiro Takiyama
IPC分类号： C08G18/42 , C08G18/80 , C08G63/20 , C08G63/685 , C08G63/91 , C08L101/16 , C08G63/02
CPC分类号： C08G18/4241 , C08G18/4238 , C08G18/8022 , C08G63/20 , C08G63/91 , C08G2230/00
摘要： An aliphatic polyester resin having a .lambda. value representing the magnitude of non-linearity of elongational viscosity of 1.5 to 8.0, said .lambda. value being defined by the following formula (1): .lambda.=.lambda..sub.1 /.lambda..sub.0 ( 1) wherein .lambda..sub.0 denotes the elongational viscosity at the transition point and .lambda..sub.1 denotes the elongational viscosity when strain become twice that of a transition point, said transition point meaning a point between a linear region, i.e., the infinitesimal-deformation region, and a non-linear region, i.e., the large-deformation region. According to the present invention, an aliphatic polyester resin having excellent formability and forming stability as well as good biodegradability is provided.
摘要翻译： PCT No.PCT / JP95 / 02616 Sec。 371日期：1996年8月21日 102（e）日期1996年8月21日PCT提交1995年12月20日PCT公布。出版物WO96 / 日期1996年6月27日具有λ值为拉伸粘度非线性大小的λ值为1.5〜8.0的脂肪族聚酯树脂，所述λ值由下式（1）定义：λ=λ1 /λ0（1 ）其中λ0表示转变点处的伸长粘度，λ1表示当应变变为转变点的两倍时的拉伸粘度，所述转变点表示线性区域即无穷小变形区域和非线性区域，即大变形区域。根据本发明，提供了具有优异的成形性和形成稳定性以及良好生物降解性的脂肪族聚酯树脂。

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