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1. 发明授权

US06391510B1 Toner for developing electrostatic latent image, process for producing the same, developer and process for producing image 失效
标题翻译：用于显影静电潜像的调色剂，其制造方法，显影剂和制备图像的方法
公开(公告)号：US06391510B1
公开(公告)日：2002-05-21
申请号：US09641563
申请日：2000-08-18
申请人： Takao Ishiyama , Manabu Serizawa , Takeshi Shoji , Yasuo Matsumura , Hideo Maehata
发明人： Takao Ishiyama , Manabu Serizawa , Takeshi Shoji , Yasuo Matsumura , Hideo Maehata
IPC分类号： G03G908
CPC分类号： G03G9/08795 , G03G9/0821 , G03G9/08797
摘要： The invention relates to a toner for developing an electrostatic latent image, a process for producing the same, a developer for an electrostatic latent image, and a process for forming an image, and the toner contains a binder resin and a coloring agent and has a molecular weight between crosslinking points Mc obtained by a measurement of temperature dispersion on dynamic viscoelasticity of from 3.6×106 to 7.5×108, and the molecular weight between crosslinking points Mc and a crosslinking density Me satisfying the relationship 14.0≦Log10(Mc/Me)≦16.5.
摘要翻译：本发明涉及用于显影静电潜像的调色剂，其制备方法，静电潜像用显影剂和形成图像的方法，调色剂含有粘合剂树脂和着色剂，并且具有通过测量动态粘弹性为3.6×10 6至7.5×10 8的温度分散获得的交联点之间的分子量以及交联点之间的分子量Mc和满足关系14.0的交联密度Me（Log10（Mc / Me） = 16.5。

2. 发明授权

US06294302B1 Toner for developing static image, developer for developing static image, and image forming method 有权
标题翻译：用于开发静态图像的调色剂，用于开发静态图像的显影剂和图像形成方法
公开(公告)号：US06294302B1
公开(公告)日：2001-09-25
申请号：US09516165
申请日：2000-02-29
申请人： Manabu Serizawa , Takao Ishiyama , Takeshi Shoji , Yukiko Watanabe , Hideo Maehata
发明人： Manabu Serizawa , Takao Ishiyama , Takeshi Shoji , Yukiko Watanabe , Hideo Maehata
IPC分类号： G03G9087
CPC分类号： G03G13/20 , G03G9/08795 , G03G9/08797
摘要： It is to easily form a fixed image, especially a full color image, that exhibits a small difference in gloss depending on the fixing conditions of the toner, is excellent in smoothness, exhibits small unevenness of gloss, and has high image quality and high reliability. A toner for developing a static image to be fixed by heat on a fixing substrate, wherein a fixed image has a gloss Gm of about 20% or more, and a maximum value of a degree of change Gs of the gloss per 1° C. of a difference of a surface temperature within a range of about from 140 to 170° C. of a fixing member as a heating and fixing unit is 1.8% or less per 1° C.; and a developer for a static image and a process for producing an image using the toner are provided.
摘要翻译：根据调色剂的定影条件容易地形成表现出微小的光泽差异的固定图像，特别是全色图像，平滑度优异，光泽不均匀性好，图像质量高，可靠性高。一种调色剂，用于在固定基材上显影用于固定的静态图像，其中固定图像具有约20％以上的光泽度Gm，并且每1℃的光泽度的变化度Gs的最大值。作为加热和定影单元的固定构件的表面温度在约140至170℃的范围内的差异为每1℃为1.8％以下。并且提供了用于静态图像的显影剂和使用调色剂产生图像的过程。

3. 发明授权

US06329114B1 Electrostatic image developing toner, production method thereof, electrostatic image developer and image-forming process 有权
标题翻译：静电图像显影调色剂，其制备方法，静电图像显影剂和成像方法
公开(公告)号：US06329114B1
公开(公告)日：2001-12-11
申请号：US09453822
申请日：1999-12-03
申请人： Yukiko Watanabe , Takao Ishiyama , Manabu Serizawa , Takeshi Shoji , Yasuo Matsumura
发明人： Yukiko Watanabe , Takao Ishiyama , Manabu Serizawa , Takeshi Shoji , Yasuo Matsumura
IPC分类号： G03G9087
CPC分类号： G03G9/0821 , G03G9/0819 , G03G9/09 , G03G9/097
摘要： An electrostatic image developing toner wherein in the dynamic viscoelasticity of the toner, the lowest temperature at which the value of the storage elastic modulus (G′) of the toner coincides with the value of the loss elastic modulus (G″) of the toner obtained under a frequency of 6.28 rad/second in a temperature dispersion measurement at a temperature of at least 0° C. is in the range of from 60 to 75° C., or the weight average molecular weight of the toner obtained by a GPC measurement is in the range of from 20,000 to 65,000 and the peak area that the molecular weight of the toner obtained by the GPC measurement is not larger than 1,000 is 3.0% or lower. The toner is excellent in the document offset property, the bending resistance of the fixed image, the releasing property of the fixing sheet, and transparency of as optically projected image, has charging uniformity and a high stability, gives no fog and toner scattering, and can form images of excellent quality.
摘要翻译：一种静电图像显影调色剂，其中在调色剂的动态粘弹性中，调色剂的储能弹性模量（G'）的值与调色剂的损耗弹性模量（G“）的值一致的最低温度在温度至少为0℃的温度分散测量中以6.28rad /秒的频率获得的值在60至75℃的范围内，或通过GPC获得的调色剂的重均分子量测量范围为20,000至65,000，并且通过GPC测量获得的调色剂的分子量不大于1,000的峰面积为3.0％以下。调色剂在文档偏移性，耐弯曲性方面优异的固定图像，固定片的释放特性和作为光学投影图像的透明度具有充电均匀性和高稳定性，不会产生雾和调色剂飞散，并且可以形成优质的图像。

4. 发明授权

US06440627B2 Toner for developing electrostatic image, process for preparation of the same, developer for electrostatic image, and process for forming image 有权
标题翻译：用于静电图像显影的调色剂，其制备方法，静电图像显影剂和形成图像的方法
公开(公告)号：US06440627B2
公开(公告)日：2002-08-27
申请号：US09776905
申请日：2001-02-06
申请人： Takeshi Shoji , Shuji Sato , Takao Ishiyama , Manabu Serizawa , Masaaki Suwabe , Yasuo Matsumura
发明人： Takeshi Shoji , Shuji Sato , Takao Ishiyama , Manabu Serizawa , Masaaki Suwabe , Yasuo Matsumura
IPC分类号： G03G909
CPC分类号： G03G9/09 , G03G9/0825 , G03G9/0906
摘要： A toner for developing an electrostatic image excellent in fixing property and particularly in light transmissibility and coloring property and satisfying high image quality and high reliability, and a process for producing the same, as well as a developer for an electrostatic image and a process for forming an image are provided. The toner for developing an electrostatic image contains at least a resin component and colorant particles, and the colorant particles exhibit a dispersion state inside the toner observed by a transmission electron microscope. The dispersion state satisfies two conditions, where (1) the colorant particles have a dispersion average particle diameter of 100 nm or less, and (2) the colorant particles have a content of coarse particles of a diameter of 400 nm or more 5% by number or less of the total of the colorant particles.
摘要翻译：用于显影定影性优异，特别是透光性和着色性，并且满足高图像质量和高可靠性的静电图像的调色剂及其制造方法以及静电图像显影剂和成型方法提供图像。用于显影静电图像的调色剂至少包含树脂组分和着色剂颗粒，并且着色剂颗粒在透射电子显微镜观察到的调色剂内表现出分散状态。分散状态满足两个条件，其中（1）着色剂颗粒的分散平均粒径为100nm以下，（2）着色剂颗粒的直径为400nm以上的粗大粒子的含量为5％以上数量或更少的着色剂颗粒总数。

5. 发明授权

US6132921A Toner for electrostatic-charged image developer and production method thereof, electrostatic-charged image developer, and image-forming process 有权
标题翻译：静电荷图像显影剂用调色剂及其制造方法，静电带电显影剂及成像方法
公开(公告)号：US6132921A
公开(公告)日：2000-10-17
申请号：US516555
申请日：2000-02-29
申请人： Takao Ishiyama , Manabu Serizawa , Takeshi Shoji , Yukiko Watanabe , Yasuo Matsumura
发明人： Takao Ishiyama , Manabu Serizawa , Takeshi Shoji , Yukiko Watanabe , Yasuo Matsumura
IPC分类号： G03G9/09 , G03G9/08 , G03G9/087 , G03G9/097
CPC分类号： G03G9/0821 , G03G9/08793
摘要： An electrostatic-charged image developing toner containing a binder resin and a coloring agent, which is excellent in the fixing characteristics, has high charging uniformity and stability, and gives excellent images, wherein the crosslinking molecular weight Mc of the toner obtained by a temperature dispersion measurement in the dynamic viscoelasticity of the toner is from about 1.6.times.10.sup.4 to 3.5.times.10.sup.6, or the crosslinking density Me thereof is from about 1.6.times.10.sup.-8 to 3.5.times.10.sup.-6 /Kmol.
摘要翻译：包含固色特性优异的粘合剂树脂和着色剂的静电带电图像显影调色剂具有高的充电均匀性和稳定性，并且得到优异的图像，其中通过温度分散得到的调色剂的交联分子量Mc 调色剂的动态粘弹性测量值为约1.6×10 4至3.5×10 6，或其交联密度Me为约1.6×10-8至3.5×10-6 / Kmol。

6. 发明授权

US6080519A Toner for developing electrostatic charge and process for producing same, developer and process for forming image 有权
标题翻译：用于显影静电荷的调色剂及其制造方法，用于形成图像的显影剂和工艺
公开(公告)号：US6080519A
公开(公告)日：2000-06-27
申请号：US377180
申请日：1999-08-19
申请人： Takao Ishiyama , Manabu Serizawa , Atsuhiko Eguchi , Takeshi Shoji , Yasuo Matsumura
发明人： Takao Ishiyama , Manabu Serizawa , Atsuhiko Eguchi , Takeshi Shoji , Yasuo Matsumura
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0821 , G03G9/08782 , G03G9/08791
摘要： It is to provide a toner for developing static charge and a process for producing the same that is excellent in peelability of the fixing sheet, adhesion of the fixed image, bending resistance of the fixed image, Dispersibility of the releasing agent in the toner and transparency on an OHP sheet, and can provide a high quality fixed image, as well as a developer and a process for forming an image. It relates to a toner for developing electrostatic charge of the invention including a coloring agent and a binder resin and a process for producing the same, wherein the relaxation modulus of elasticity G(t) at a relaxation time t=10.times.Dt (wherein Dt represents a heating time on fixing) obtained from measurement of dynamic viscoelasticity is adjusted to a range of from 2.0.times.10.sup.2 to 3.0.times.10.sup.3 Pa, or the relaxation modulus of elasticity G(t=0.01) at a relaxation time of 0.01 sec obtained from measurement of dynamic viscoelasticity is adjusted to a range of from 2.0.times.10.sup.2 to 3.0.times.10.sup.4 Pa, and the ratio G(r) (G(t=0.01)/G(t=0.1)) of the relaxation modulus of elasticity G(t=0.01) to a relaxation modulus of elasticity G(t=0.1) at a relaxation time of 0.1 sec is adjusted to a range of from 1.0 to 18.0, as well as a developer and a process for forming an image using the developer.
摘要翻译：提供用于显影静电的调色剂及其制造方法，其定影片的可剥离性优异，固定图像的粘附性，固定图像的抗弯曲性，调色剂中的脱模剂的分散性和透明性在OHP片材上，并且可以提供高质量的固定图像，以及用于形成图像的显影剂和工艺。本发明涉及包含着色剂和粘合剂树脂的本发明的静电电荷用调色剂及其制造方法，其中松弛时间t = 10×Dt时的弛豫弹性模量G（t）（式中，Dt表示通过动态粘弹性测定获得的动态粘弹性测定得到的固化时的加热时间调整为2.0×102〜3.0×103Pa的范围，或松弛弹性模量G（t = 0.01）调节到2.0×102〜3.0×104Pa的范围，松弛弹性模量G（t = 0.01）的比G（r）（G（t = 0.01）/ G（t = 0.1））将弛豫时间为0.1秒的松弛弹性模量G（t = 0.1）调节至1.0〜18.0的范围，以及显影剂和使用显影剂形成图像的工序。

7. 发明授权

US06333131B1 Toner for the development of electrostatic image, process for the preparation thereof, electrostatic image developer, and process for the formation of image 有权
标题翻译：用于静电图像显影的调色剂，其制备方法，静电图像显影剂和用于形成图像的方法
公开(公告)号：US06333131B1
公开(公告)日：2001-12-25
申请号：US09663381
申请日：2000-09-15
申请人： Takao Ishiyama , Manabu Serizawa , Takeshi Shoji , Shuji Sato , Takashi Inukai
发明人： Takao Ishiyama , Manabu Serizawa , Takeshi Shoji , Shuji Sato , Takashi Inukai
IPC分类号： G03G9097
CPC分类号： G03G9/0819 , G03G9/0821 , G03G9/0823 , G03G9/09708 , G03G9/09725
摘要： There is provided a toner for the development of an electrostatic image having a complex viscosity &eegr;* of from 3.0×102 to 1.2×103 Pas at 160° C. and a loss tangent tan &dgr; of from 0.60 to 1.60 as determined by temperature dispersion measurement method by sinusoidal oscillation method, a method for manufacturing the toner by a coaggregation fusion composite method, developer, and an image forming method.
摘要翻译：提供了一种调色剂，用于在160℃下开发具有3.0×102至1.2×103 Pas的复数粘度eta *的静电图像，并且通过温度分散测量方法测定的损耗角正切tanδ为0.60至1.60 正弦振荡法，通过共焦融合复合法制造调色剂的方法，显影剂和图像形成方法。

8. 发明授权

US5910389A Method for producing toner for developing images of electrostatic charge, toner for developing images of electrostatic charge, developer for images of electrostatic charge and method for forming images 失效
标题翻译：用于显影静电荷图像的调色剂的方法，用于显影静电荷的图像的调色剂，静电荷的图像的显影剂和用于形成图像的方法
公开(公告)号：US5910389A
公开(公告)日：1999-06-08
申请号：US962703
申请日：1997-11-03
申请人： Yasuo Matsumura , Manabu Serizawa , Masaaki Suwabe , Shuji Sato , Yasuo Kadokura , Hisao Morijiri , Takeshi Shoji , Takahiro Mizoguchi
发明人： Yasuo Matsumura , Manabu Serizawa , Masaaki Suwabe , Shuji Sato , Yasuo Kadokura , Hisao Morijiri , Takeshi Shoji , Takahiro Mizoguchi
IPC分类号： G03G9/08 , G03G9/087 , G03G9/16
CPC分类号： G03G9/081 , G03G9/0819 , G03G9/0827 , G03G9/08795 , G03G9/08797
摘要： According to the present invention, the method for producing toner for developing an image of electrostatic charge comprises the steps of producing a dispersion liquid of flocculated particles by forming the flocculated particles in a dispersion liquid comprising at least dispersed resin particles, forming combined particles by dispersing a liquid dispersion comprising dispersed fine resin particles into the dispersion liquid of flocculated particles so that the fine resin particles adhere to the flocculated particles and forming toner particles by fusing the combined particles by heating, wherein the molecular weight distribution curve of the resin in the toner particles by a gel permeation chromatography has at least two peaks or shoulders. According to the present invention, it is possible to produce toner for developing an image of electrostatic charge which is particularly superior in chargeability and the stability of the chargeability.
摘要翻译：根据本发明，用于制造静电荷图像显影用调色剂的方法包括以下步骤：通过在包含至少分散的树脂颗粒的分散液中形成絮凝颗粒来生产絮凝颗粒的分散液，通过分散形成组合颗粒液体分散体，其包括将细小树脂颗粒分散到絮凝颗粒的分散液中，使得细树脂颗粒通过加热熔合组合颗粒而附着于絮凝颗粒并形成调色剂颗粒，其中调色剂中树脂的分子量分布曲线通过凝胶渗透色谱法的颗粒具有至少两个峰或肩。根据本发明，可以生产出带电性和充电性稳定性特别优异的静电荷图像的调色剂。

9. 发明授权

US6022662A Toner for developing electrostatic images, method of producing toner for developing electrostatic images, electrostatic image developer 失效
标题翻译：静电图像显影用调色剂，静电图像显影用调色剂的制造方法，静电图像显影剂
公开(公告)号：US6022662A
公开(公告)日：2000-02-08
申请号：US63349
申请日：1998-04-21
申请人： Yasuo Matsumura , Manabu Serizawa , Masaaki Suwabe , Shuji Sato , Yasuo Kadokura , Hisao Morijiri , Takeshi Shoji , Takahiro Mizuguchi
发明人： Yasuo Matsumura , Manabu Serizawa , Masaaki Suwabe , Shuji Sato , Yasuo Kadokura , Hisao Morijiri , Takeshi Shoji , Takahiro Mizuguchi
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G15/08
CPC分类号： G03G9/0819
摘要： Disclosed is toner for developing an electrostatic image, which toner has a volume average particle size distribution index (GSDv) of 1.3 or less, and a ratio of the volume average particle size distribution index (GSDv) to a number average particle size distribution index (GSDp), i.e., (GSDv/GSDp), of 0.95 or more. A method suited for producing the toner for developing an electrostatic image comprises the steps of producing a dispersion liquid of flocculated particles by forming the flocculated particles in a dispersion liquid containing at least resin particles dispersed therein, forming adhered particles by admixing a liquid dispersion comprising fine particles dispersed therein with the dispersion liquid comprising the flocculated particles so that the fine particles adhere to the flocculated particles, and forming toner particles by fusing the adhered particles upon heating. This method for producing the toner for developing an electrostatic image provides the toner excellent in chargeability and having a long life.
摘要翻译：公开了用于显影静电图像的调色剂，该调色剂的体积平均粒径分布指数（GSDv）为1.3以下，体积平均粒径分布指数（GSDv）与数均粒径分布指数（ GSDp），即（GSDv / GSDp）为0.95以上。一种适于制造用于显影静电图像的调色剂的方法包括以下步骤：通过在至少含有分散在其中的树脂颗粒的分散液中形成絮凝颗粒来形成絮凝颗粒的分散液，通过混合包含细微的液体分散体形成附着颗粒其中分散有包含絮凝颗粒的分散液的颗粒使得细颗粒粘附到絮凝颗粒上，并且通过在加热时熔化附着颗粒而形成调色剂颗粒。用于制造用于显影静电图像的调色剂的方法提供了带电性优异且寿命长的调色剂。

10. 发明授权

US5998078A Method of preparing toner for electrostatic charge image development, toner for electrostatic charge image development, electrostatic charge image developer, and image forming method 失效
标题翻译：制备用于静电荷图像显影的调色剂，用于静电荷图像显影的调色剂，静电荷图像显影剂和图像形成方法的方法
公开(公告)号：US5998078A
公开(公告)日：1999-12-07
申请号：US4343
申请日：1998-01-08
申请人： Masaaki Suwabe , Yasuo Matsumura , Manabu Serizawa , Shuji Sato , Yasuo Kadokura , Hisao Morijiri , Takahiro Mizuguchi , Takeshi Shoji
发明人： Masaaki Suwabe , Yasuo Matsumura , Manabu Serizawa , Shuji Sato , Yasuo Kadokura , Hisao Morijiri , Takahiro Mizuguchi , Takeshi Shoji
IPC分类号： G03G9/09 , G03G9/08 , G03G9/087 , G03G15/08
CPC分类号： G03G9/0804
摘要： The present invention provides a method of preparing a toner for electrostatic charge image development comprising the steps of a liquid mixture preparation process for preparing a liquid mixture by mixing at least a resin particle dispersion prepared by dispersing resin particles in a solution including a dispersing agent having a polarity, and a coloring agent particle dispersion prepared by dispersing coloring agent particles in a solution including a dispersing agent having a polarity, an aggregated particle dispersion preparation process for preparing an aggregated particle dispersion by forming aggregated particles in the liquid mixture, and a fusion process for fusing the aggregated particles by heating, wherein the first dispersing agent and the second dispersing agent have the same polarity, a toner for electrostatic charge image development obtained by the method, an electrostatic charge image developer containing the toner and a carrier for electrophotography, and an image forming method comprising the steps of a process for forming an electrostatic latent image on an electrostatic latent image carrying member, a process for forming a toner image by developing the electrostatic latent image by a developer layer on a developing carrying member, and a transfer process for transferring the toner image onto a transferring member.
摘要翻译：本发明提供一种制备静电荷图像显影用调色剂的方法，包括以下步骤：通过混合至少一种通过将树脂颗粒分散在包含分散剂的溶液中制备的树脂颗粒分散体来制备液体混合物，所述溶液包括具有极性和通过将着色剂颗粒分散在包含具有极性的分散剂的溶液中制备的着色剂颗粒分散体，通过在液体混合物中形成凝集颗粒来制备凝集颗粒分散体的凝集颗粒分散体制备方法，以及熔融通过加热使凝集颗粒熔合的方法，其中第一分散剂和第二分散剂具有相同的极性，通过该方法获得的用于静电荷图像显影的调色剂，含有调色剂的静电荷图像显影剂和用于电子照相的载体，和图像f 该方法包括以下步骤：在静电潜像承载部件上形成静电潜像的方法，通过显影承载部件上的显影剂层使静电潜像显影形成调色剂图像的工艺，以及转印工艺将调色剂图像转印到转印部件上。

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