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1. 发明授权

US07067575B2 Water-soluble film of polyvinyl alcohol 有权
标题翻译：聚乙烯醇水溶性薄膜
公开(公告)号：US07067575B2
公开(公告)日：2006-06-27
申请号：US10703519
申请日：2003-11-10
申请人： Syuichi Kitamura , Tomoyoshi Mizutani , Mitsuhiro Hasegawa , Hideki Oono
发明人： Syuichi Kitamura , Tomoyoshi Mizutani , Mitsuhiro Hasegawa , Hideki Oono
IPC分类号： C08K5/053 , C08L29/04
CPC分类号： C08J5/18 , C08J2329/04 , C08K5/053 , C11D17/044 , C08L29/04
摘要： A water-soluble film made from a resin composition comprising (A) 100 parts by weight of an anionic group-modified polyvinyl alcohol having a viscosity of 10 to 35 mPa·s measured at 20° C. with respect to a 4% by weight aqueous solution thereof, an average degree of hydrolysis of 80.0 to 99.9% by mole and a rate of anionic group modification of 1 to 10% by mole, (B) 20 to 50 parts by weight of a plasticizer, (C) 2 to 30 parts by weight of a filler, and (D) 0.01 to 2.5 parts by weight of a surfactant. The water-soluble film has an excellent water solubility, and is not gelled or insolubilized even if chemicals containing a boric acid substance, particularly sodium perborate, are packaged therein or even if it is put in an aqueous solution of a boric acid substance, particularly sodium perborate.
摘要翻译：一种由树脂组合物制成的水溶性薄膜，其包含（A）100重量份在20℃下测定的粘度为10〜35mPa·s的阴离子性基团改性的聚乙烯醇相对于4重量％水溶液，平均水解度为80.0〜99.9摩尔％，阴离子基团改性率为1〜10摩尔％，（B）20〜50重量份增塑剂，（C）2〜30 （D）0.01〜2.5重量份的表面活性剂。即使含有硼酸物质，特别是过硼酸钠的化学物质也被包装在其中，或者即使放入硼酸物质的水溶液中也不会凝胶化或不溶化，特别是水溶性膜。过硼酸钠。

2. 发明授权

US06759001B2 Method for producing embossed poly(vinyl alcohol) film 有权
标题翻译：生产压花聚（乙烯醇）薄膜的方法
公开(公告)号：US06759001B2
公开(公告)日：2004-07-06
申请号：US09859283
申请日：2001-05-17
申请人： Tomoyoshi Mizutani , Syuichi Kitamura , Kenji Hasegawa , Manabu Miyato , Hideki Oono
发明人： Tomoyoshi Mizutani , Syuichi Kitamura , Kenji Hasegawa , Manabu Miyato , Hideki Oono
IPC分类号： B29C5328
CPC分类号： B29C59/04 , B29K2029/04 , B29K2995/0041 , Y10T428/24628
摘要： A method for producing an embossed PVA film, which includes embossing the film such that the crystallinity index of the emboss top is 0.50-0.90. The invention provides an embossed PVA film superior in resistance to blocking even when in a rolled state, in appearance to show the high quality of products, and in resistance to pinholes.
摘要翻译：一种压花PVA膜的制造方法，其包括使膜压花，使得压花顶部的结晶度为0.50-0.90。本发明提供了即使在轧制状态下，在外观上显示出高质量的产品和耐针孔性的耐粘连性的压花PVA膜。

3. 发明授权

US07754318B2 Water-soluble film 有权
标题翻译：水溶性薄膜
公开(公告)号：US07754318B2
公开(公告)日：2010-07-13
申请号：US11922072
申请日：2005-06-16
申请人： Shuichi Kitamura , Tomoyoshi Mizutani , Mitsuhiro Hasegawa
发明人： Shuichi Kitamura , Tomoyoshi Mizutani , Mitsuhiro Hasegawa
IPC分类号： B32B27/30
CPC分类号： C08J5/18 , C08J2329/04 , C08K3/30 , C08K5/0016 , C08K5/053 , C08L29/04
摘要： The present invention relates to a water-soluble film, which is a polyvinyl alcohol film comprising a polyvinyl alcohol resin (A), wherein the water-soluble film has a time for dissolution in water at 20° C. of not more than 60 seconds in terms of a film thickness of 76 μm, a b-value of the film is not more than 0.5, and a b-value of the film after leaving at 80° C. for 72 hr is not more than 1.0, preferably a water-soluble film comprising: a polyvinyl alcohol resin (A); at least two kinds of plasticizers (B); and a sulfite salt (C), wherein the content of the plasticizer (B) based on 100 parts by weight of the polyvinyl alcohol resin (A) is 5 to 50 parts by weight and the content ratio of the sulfite salt (C) to the plasticizer (B) (C/B: weight ratio) is more than 0.02 and not more than 0.35. According to the invention, there is provided a water-soluble film comprising a PVA resin as a main component, wherein the film is less likely to cause coloration at the time of film formation and coloration with time even upon contact with a chemical.
摘要翻译：本发明涉及一种水溶性膜，其是包含聚乙烯醇树脂（A）的聚乙烯醇膜，其中水溶性膜具有在20℃下在水中溶解不超过60秒的时间膜厚为76μm时，膜的b值不大于0.5，在80℃下放置72小时后的膜的b值不大于1.0，优选为水 - 可溶性膜，其包含：聚乙烯醇树脂（A）; 至少两种增塑剂（B）; 和亚硫酸盐（C），其中，基于100重量份的聚乙烯醇树脂（A），增塑剂（B）的含量为5〜50重量份，亚硫酸盐（C）〜增塑剂（B）（C / B：重量比）大于0.02且不大于0.35。根据本发明，提供了以PVA树脂为主要成分的水溶性薄膜，即使在与化学品接触的情况下，膜也不易于成膜时着色，随时间着色。

4. 发明申请

US20090291282A1 Water-soluble film 有权
标题翻译：水溶性薄膜
公开(公告)号：US20090291282A1
公开(公告)日：2009-11-26
申请号：US11922072
申请日：2005-06-16
申请人： Shuichi Kitamura , Tomoyoshi Mizutani , Mitsuhiro Hasegawa
发明人： Shuichi Kitamura , Tomoyoshi Mizutani , Mitsuhiro Hasegawa
IPC分类号： B32B27/30
CPC分类号： C08J5/18 , C08J2329/04 , C08K3/30 , C08K5/0016 , C08K5/053 , C08L29/04
摘要： The present invention relates to a water-soluble film, which is a polyvinyl alcohol film comprising a polyvinyl alcohol resin (A), wherein the water-soluble film has a time for dissolution in water at 20° C. of not more than 60 seconds in terms of a film thickness of 76 μm, a b-value of the film is not more than 0.5, and a b-value of the film after leaving at 80° C. for 72 hr is not more than 1.0, preferably a water-soluble film comprising: a polyvinyl alcohol resin (A); at least two kinds of plasticizers (B); and a sulfite salt (C), wherein the content of the plasticizer (B) based on 100 parts by weight of the polyvinyl alcohol resin (A) is 5 to 50 parts by weight and the content ratio of the sulfite salt (C) to the plasticizer (B) (C/B: weight ratio) is more than 0.02 and not more than 0.35. According to the invention, there is provided a water-soluble film comprising a PVA resin as a main component, wherein the film is less likely to cause coloration at the time of film formation and coloration with time even upon contact with a chemical.
摘要翻译：本发明涉及一种水溶性膜，其是包含聚乙烯醇树脂（A）的聚乙烯醇膜，其中水溶性膜具有在20℃下在水中溶解不超过60秒的时间膜厚为76μm时，膜的b值不大于0.5，在80℃下放置72小时后的膜的b值不大于1.0，优选为水 - 可溶性膜，其包含：聚乙烯醇树脂（A）; 至少两种增塑剂（B）; 和亚硫酸盐（C），其中，基于100重量份的聚乙烯醇树脂（A），增塑剂（B）的含量为5〜50重量份，亚硫酸盐（C）〜增塑剂（B）（C / B：重量比）大于0.02且不大于0.35。根据本发明，提供了以PVA树脂为主要成分的水溶性薄膜，即使在与化学品接触的情况下，膜也不易于成膜时着色，随时间着色。

5. 发明申请

US20050010010A1 Poly (vinyl alcohol) based film 审中-公开
标题翻译：聚（乙烯醇）基膜
公开(公告)号：US20050010010A1
公开(公告)日：2005-01-13
申请号：US10500082
申请日：2002-12-26
申请人： Shuichi Kitamura , Tomoyoshi Mizutani
发明人： Shuichi Kitamura , Tomoyoshi Mizutani
IPC分类号： C08J5/18 , C08F218/02
CPC分类号： C08J5/18 , C08J2329/04
摘要： A polyvinyl alcohol film which dissolves in water at 20° C. within 10 minutes and has an α/β ratio of not more than 10 wherein α is a storage modulus of the film at 20° C. in a dry atmosphere and β is a storage modulus of the film at 20° C. and 80% RH, and which has an excellent cold water solubility and an excellent durability such that the change in appearance of the film under high humidity is slight and the lowering of the cold water solubility is slight even if the film is stored for a long term.
摘要翻译：聚乙烯醇膜，其在20℃下在10分钟内溶解在水中，并且α/β比不大于10，其中α是在干燥气氛中20℃下的膜的储能模量，β是在20℃和80％RH下的膜的储能模量，并且具有优异的冷水溶解度和优异的耐久性，使得在高湿度下膜的外观变化轻微，并且冷水溶解度的降低为即使电影长期存放也是轻微的。

6. 发明授权

US06657004B2 Film for packaging chemical agents 失效
公开(公告)号：US06657004B2
公开(公告)日：2003-12-02
申请号：US09855467
申请日：2001-05-15
申请人： Tomoyoshi Mizutani
发明人： Tomoyoshi Mizutani
IPC分类号： C08L2904
CPC分类号： C08J5/18 , C08J2329/04 , Y10T428/31511
摘要： The present invention provides a film for packaging chemical agents, which contains an oxyalkylene unit-containing polyvinyl alcohol resin (A) and a carboxyl-containing polyvinyl alcohol resin (B), and preferably further containing a sulfo-containing polyvinyl alcohol resin (C). This film shows fine solubility in water even after a long-term packaging of an acidic chemical agent or alkaline chemical agent, and is superior in mechanical strength. Thus, the film for packaging chemical agents of the present invention is suitably used for packaging a chemical agent, such as powdered soap, synthetic detergent, agricultural chemical, antibacterial, deodorant, insecticide and the like, which is cast into water when in use.

7. 发明申请

US20160205880A1 PLANT CULTIVATION SYSTEM AND A METHOD FOR PLANT CULTIVATION 审中-公开
标题翻译：植物培养系统和植物培养方法
公开(公告)号：US20160205880A1
公开(公告)日：2016-07-21
申请号：US14913125
申请日：2014-08-11
申请人： Hiroshi Yoshioka , Yuichi Mori , Akihiro Okamoto , Shigeki Miura , Tomoyoshi Mizutani , MEBIOL INC.
发明人： Hiroshi Yoshioka , Yuichi Mori , Akihiro Okamoto , Shigeki Miura , Tomoyoshi Mizutani
IPC分类号： A01G31/00 , A01G1/00 , A01G25/02
摘要： [Problems] Prior art technology has a problem in that when a plant is cultivated for a long period of time on a polyvinyl alcohol (PVA) film having its lower surface positioned in contact with a nutrient fluid, plant roots that have formed penetrate through the film.[Means to solve the problems] A plant cultivation system wherein the PVA film has an equilibrium degree of swelling in the range of from 125 to 250% as measured in water at 30° C. and has a loss tangent (tan δ) in the range of from 0.005 to 0.2 as measured in an equilibrium swollen state in water at 30° C., and a method for cultivating a plant by using this plant cultivation system.[Industrial applicability] Plant cultivation can be performed for a long period of time while avoiding infection by bacteria and the like causative of plant diseases. Therefore, the present invention is useful in, e.g., agriculture and the manufacture of pharmaceuticals.
摘要翻译：现有技术存在的问题在于，当将植物长时间培养在其下表面与营养液接触的聚乙烯醇（PVA）膜上时，已经形成的植物根部穿过电影。 [解决问题的方法]一种植物栽培系统，其中在30℃下在水中测量的PVA膜具有在125至250％范围内的平衡膨胀度，并且在其中具有损耗角正切（tanδ）在30℃的水中以平衡溶胀状态测定的0.005〜0.2的范围，以及使用该植物培养体系培养植物的方法。 [工业实用性]植物栽培可以长时间进行，同时避免细菌感染等引起植物病害的发生。因此，本发明在例如农业和药物的制造中是有用的。

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