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1. 发明授权

US07288182B1 Hydroprocessing using bulk Group VIII/Group VIB catalysts 有权
标题翻译：使用本体VIII / VIB族催化剂进行加氢处理
公开(公告)号：US07288182B1
公开(公告)日：2007-10-30
申请号：US09869984
申请日：2000-01-14
申请人： Stuart Leon Soled , Sabato Miseo , Roman Krycak , Hilda B. Vroman , Teh Chung Ho , Kenneth Lloyd Riley
发明人： Stuart Leon Soled , Sabato Miseo , Roman Krycak , Hilda B. Vroman , Teh Chung Ho , Kenneth Lloyd Riley
IPC分类号： C10G73/02 , C10G11/00 , B01J29/70 , B01J23/00 , B01J23/70
CPC分类号： B01J23/002 , B01J23/85 , B01J23/88 , B01J23/883 , B01J23/8878 , B01J23/888 , B01J23/8885 , B01J37/03 , B01J37/082 , B01J2523/00 , C08F8/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G65/04 , C10G65/08 , C10G65/12 , C10G2400/10 , C10G2400/14 , C08F240/00 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/842 , B01J2523/67 , B01J2523/31 , B01J2523/41
摘要： A process for hydroprocessing petroleum and chemical feedstocks by use of a bulk multimetallic catalyst comprised of at least one Group VIII non-noble metal and at least one, preferably two Group VIB metal wherein the ratio of Group VIB metal to Group VIII metal is from about 10:1 to 1:10.
摘要翻译：通过使用由至少一种VIII族非贵金属和至少一种，优选两种VIB族金属组成的本体多金属催化剂加氢处理石油和化学原料的方法，其中VIB族金属与VIII族金属的比例为约 10：1到1:10。

2. 发明授权

US5728644A Dispersed metal sulfide catalysts for hydroprocessing 失效
标题翻译：用于加氢处理的分散金属硫化物催化剂
公开(公告)号：US5728644A
公开(公告)日：1998-03-17
申请号：US524228
申请日：1995-09-05
申请人： Teh Chung Ho , Stuart Leon Soled , Sabato Miseo , Gary Brice Mc Vicker , Michel Daage , Viktor Buchholz
发明人： Teh Chung Ho , Stuart Leon Soled , Sabato Miseo , Gary Brice Mc Vicker , Michel Daage , Viktor Buchholz
IPC分类号： B01J31/22 , B01J23/887 , B01J23/889 , B01J27/051 , B01J37/08 , B01J37/20 , C07B35/02 , C10G45/46 , C10G45/50 , B01J27/047 , B01J23/63 , B01J31/00
CPC分类号： B01J37/086 , B01J23/887 , B01J23/8878 , B01J23/8892 , B01J27/051 , B01J37/20 , C10G45/46 , C10G45/50
摘要： The present invention is directed toward a catalyst composition comprising a catalyst prepared by a process comprising: (a) impregnating an oxide precursor selected from the group consisting of rare earth oxide precursors, yttria precursors and mixtures thereof, onto an inorganic refractory oxide support; (b) drying said support at a temperature of about 100.degree. to about 120.degree. C. followed by calcining said support at a temperature of about 400.degree. to about 600.degree. C.; and (c) compositing or depositing on said support of step (b), a catalyst precursor salt represented by (ML)(Mo.sub.y W.sub.1-y O.sub.4).sub.a wherein M comprises Cr and/or one or more divalent promoter metals selected from the group consisting of Mn, Fe, Co, Ni, Cu, Zn and mixtures thereof, wherein y is any value ranging from 0 to 1, and wherein L is one or more neutral, nitrogen-containing ligands at least one of which is a chelating polydentate ligand; a=1 when chromium is not one of the promoter metals and 0.5.ltoreq.a.ltoreq.3 when Cr is one of the promoter metals. (d) sulfiding said deposited or composited supports of step (c) with an excess amount of sulfur in the form of one or more sulfur bearing compounds and at a temperature of at least about 250.degree. C. to form catalysts. In a preferred embodiment, the process will further comprise decomposing the composited or deposited supports of step (c) in a nonoxidizing atmosphere at a temperature of at least about 250.degree. C. prior to said sulfiding step (d). In a second aspect of the invention there is provided an improved aromatics hydrogenation process.
摘要翻译：本发明涉及一种催化剂组合物，其包含通过以下方法制备的催化剂，所述催化剂包括：（a）将选自稀土氧化物前体，氧化钇前体及其混合物的氧化物前体浸渍到无机耐火氧化物载体上; （b）在约100至约120℃的温度下干燥所述载体，然后在约400至约600℃的温度下煅烧所述载体; 和（c）在步骤（b）的所述载体上合成或沉积由（ML）（MoyW1-yO4）a表示的催化剂前体盐，其中M包含Cr和/或一种或多种选自以下的二价助催化剂金属： Mn，Fe，Co，Ni，Cu，Zn及其混合物，其中y是0至1的任何值，并且其中L是一种或多种中性含氮配体，其中至少一种是螯合多齿配体; 当Cr不是助催化剂金属之一时，a = 1，当Cr是助催化剂金属之一时，a = 1。（d）用一种或多种带硫化合物形式的过量硫磺和至少约250℃的温度硫化所述步骤（c）的沉积或复合载体以形成催化剂。在优选的实施方案中，该方法还包括在所述硫化步骤（d）之前，在至少约250℃的温度下，在非氧化气氛中分解步骤（c）的复合或沉积的载体。在本发明的第二方面，提供了一种改进的芳族化合物氢化方法。

3. 发明授权

US07232515B1 Hydrofining process using bulk group VIII/Group VIB catalysts 有权
标题翻译：使用本体VIII / VIB族催化剂的加氢精制方法
公开(公告)号：US07232515B1
公开(公告)日：2007-06-19
申请号：US09869987
申请日：2000-01-14
申请人： Richard Alan Demmin , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
发明人： Richard Alan Demmin , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
IPC分类号： C10G45/60
CPC分类号： B01J23/002 , B01J23/85 , B01J23/88 , B01J23/883 , B01J23/8878 , B01J23/888 , B01J23/8885 , B01J37/03 , B01J37/082 , B01J2523/00 , C08F8/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G65/04 , C10G65/08 , C10G65/12 , C10G2400/10 , C10G2400/14 , C08F240/00 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/842 , B01J2523/67 , B01J2523/31 , B01J2523/41
摘要： A process for hydrofining a lubricating oil feedstock comprising contacting the feedstock with a hydrofining catalyst in a hydrofining zone under hydrofining conditions wherein the hydrofining catalyst comprises a bulk metal catalyst containing non-noble Group VIII metal molybdate in which at least a portion but less than all of the molybdenum is replaced by tungsten.
摘要翻译：一种用于加氢精炼润滑油原料的方法，包括在加氢精炼条件下在加氢精炼区中将原料与加氢精制催化剂接触，其中加氢精制催化剂包含含有非贵金属VIII族金属钼酸盐的本体金属催化剂，其中至少一部分但少于全部的钼被钨取代。

4. 发明授权

US06783663B1 Hydrotreating using bulk multimetallic catalysts 有权
标题翻译：使用大量多金属催化剂加氢处理
公开(公告)号：US06783663B1
公开(公告)日：2004-08-31
申请号：US09869988
申请日：2001-08-22
申请人： Kenneth Lloyd Riley , Darryl Patrick Klein , Zhiguo Hou , Stuart Leon Soled , Michael Charles Kerby , Gary Brice McVicker , Edward Stanley Ellis , Michele Sue Touvelle , Sabato Miseo
发明人： Kenneth Lloyd Riley , Darryl Patrick Klein , Zhiguo Hou , Stuart Leon Soled , Michael Charles Kerby , Gary Brice McVicker , Edward Stanley Ellis , Michele Sue Touvelle , Sabato Miseo
IPC分类号： C10G4504
CPC分类号： B01J23/002 , B01J23/85 , B01J23/88 , B01J23/883 , B01J23/8878 , B01J23/888 , B01J23/8885 , B01J37/03 , B01J37/082 , B01J2523/00 , C07C29/16 , C08F8/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G65/04 , C10G65/08 , C10G65/12 , C10G2400/10 , C10G2400/14 , C08F240/00 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/842 , B01J2523/67 , B01J2523/31 , B01J2523/41
摘要： A hydroprocessing process, comprising: contacting a feedstock, at hydrotreating conditions, with a bulk multimetallic catalyst comprised of at least one Group VIII non-noble metal and at least two Group VIB metals and wherein the ratio of Group VIB metal to Group VIII non-noble metal is from about 10:1 to about 1:10 to form a hydrotreated product.
摘要翻译：一种加氢处理方法，包括：在加氢处理条件下使原料与由至少一种第八族非贵金属和至少两种第VIB族金属组成的本体多金属催化剂接触，并且其中VIB族金属与VIII族非金属的比率，贵金属为约10:1至约1:10以形成加氢处理的产物。

5. 发明授权

US06620313B1 Hydroconversion process using bulk group VIII/Group VIB catalysts 有权
标题翻译：使用本体VIII / VIB族催化剂的加氢转化法
公开(公告)号：US06620313B1
公开(公告)日：2003-09-16
申请号：US09869986
申请日：2001-08-22
申请人： Richard Alan Demmin , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
发明人： Richard Alan Demmin , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
IPC分类号： C10G7306
CPC分类号： B01J23/002 , B01J23/85 , B01J23/88 , B01J23/883 , B01J23/8878 , B01J23/888 , B01J23/8885 , B01J37/03 , B01J37/082 , B01J2523/00 , C07C29/16 , C08F8/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G65/04 , C10G65/08 , C10G65/12 , C10G2400/10 , C10G2400/14 , C08F240/00 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/842 , B01J2523/67 , B01J2523/31 , B01J2523/41
摘要： Hydroconversion process of petroleum and chemical feedstocks using bulk Group VIII/Group VIB catalysts. Preferred catalysts include those comprised of Ni—Mo—W.
摘要翻译：石油和化学原料的加氢转化工艺使用大量第VIII / VIB族催化剂。优选的催化剂包括由Ni-Mo-W组成的催化剂。

6. 发明授权

US06635599B1 Mixed metal catalyst, its preparation by co-precipitation, and its use 有权
标题翻译：混合金属催化剂，其共沉淀制备及其用途
公开(公告)号：US06635599B1
公开(公告)日：2003-10-21
申请号：US09482811
申请日：2000-01-13
申请人： Sonja Eijsbouts , Bob Gerardus Oogjen , Hermannus Willem Homan Free , Marinus Bruce Cerfontain , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
发明人： Sonja Eijsbouts , Bob Gerardus Oogjen , Hermannus Willem Homan Free , Marinus Bruce Cerfontain , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
IPC分类号： B01J2300
CPC分类号： B01J23/8885 , B01J23/85 , B01J23/883 , B01J37/0009 , B01J37/0236 , B01J37/031 , B01J37/082 , B01J37/20 , C10G45/08 , C10G49/04
摘要： The present invention relates to a process for the preparation of a hydroprocessing catalyst, to the catalyst composition obtainable by said process, and to the use of said catalyst composition in hydroprocessing applications. The process comprises the steps of combining and reacting at least one Group VIII non-noble metal component in solution and at least two Group VIB metal components in solution in a reaction mixture to obtain an oxygen-stable precipitate, and sulfiding the precipitate.
摘要翻译：本发明涉及一种制备加氢处理催化剂的方法，可通过所述方法获得的催化剂组合物以及所述催化剂组合物在加氢处理应用中的用途。该方法包括以下步骤：将至少一种溶液中的第VIII族非贵金属组分和至少两种VIB族金属组分混合并在反应混合物中溶解，得到氧稳定的沉淀物，并使沉淀物硫化。

7. 发明授权

US06534437B2 Process for preparing a mixed metal catalyst composition 有权
公开(公告)号：US06534437B2
公开(公告)日：2003-03-18
申请号：US09836101
申请日：2001-04-17
申请人： Sonja Eijsbouts , Bob Gerardus Oogjen , Harmannus Willem Homan Free , Marinus Bruce Cerfontain , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
发明人： Sonja Eijsbouts , Bob Gerardus Oogjen , Harmannus Willem Homan Free , Marinus Bruce Cerfontain , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
IPC分类号： B01J27043
CPC分类号： B01J35/002 , B01J23/85 , B01J23/8885 , B01J35/0053 , B01J35/008 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J37/0009 , B01J37/0236 , B01J37/031 , B01J37/20 , C10G49/04
摘要： The invention pertains to a process for preparing a catalyst composition comprising bulk catalyst particles comprising at least one Group VIII non-noble metal and at least two Group VIB metals. The process comprises combining and reacting at least one Group VIII non-noble metal component with at least two Group VIB metal components in the presence of a protic liquid, with at least one of the metal components remaining at least partly in the solid state during the entire process. The Group VIII and Group VIB metals comprise from about 50 wt. % to about 100 wt. %, calculated as oxides, of the total weight of said bulk catalyst particles, with the solubility of those of the metal components which are at least partly in the solid state during the reaction being less than 0.05 mol/100 ml water at 18° C. The invention also covers a catalyst composition made by that process and a process for the hydroprocessing of a hydrocarbon feedstock by contacting the feedstock with that catalyst at hydroprocessing conditions.

8. 发明授权

US06383366B1 Wax hydroisomerization process 失效
标题翻译：蜡加氢异构化工艺
公开(公告)号：US06383366B1
公开(公告)日：2002-05-07
申请号：US09601858
申请日：2000-11-14
申请人： Kenneth Lloyd Riley , William John Murphy , Ian Alfred Cody , Stuart Leon Soled , Gary Brice McVicker , Sabato Miseo
发明人： Kenneth Lloyd Riley , William John Murphy , Ian Alfred Cody , Stuart Leon Soled , Gary Brice McVicker , Sabato Miseo
IPC分类号： C10G35085
CPC分类号： C10G45/64 , C10G45/62 , C10G2400/10
摘要： Waxy feeds are treated under hydroisomerization conditions to produce good yields of an isomerate product of high VI by using a silica-alumina based catalyst in which the silica-alumina has a pore volume less of 0.99 ml/gm (H2O), an alumina content in the range of 35 to 55 wt % and an isoelectric point in the range of 4.5 to 6.5. A lube fraction of the isomerate is dewaxed to provide a lube basestock of high VI. The silica-alumina may be modified with a rare earth oxide or yttria or boria or magnesia in which instance the modified catalyst has an isoelectric point greater than but no more than 2 points greater than base the silica-alumina.
摘要翻译：在加氢异构化条件下处理蜡进料，通过使用二氧化硅 - 氧化铝基催化剂，其中二氧化硅 - 氧化铝的孔体积小于0.99ml / gm（H 2 O），氧化铝含量为 35〜55重量％的范围，等电点为4.5〜6.5。将异构体的润滑部分脱蜡以提供高VI的润滑油基础油料。二氧化硅 - 氧化铝可以用稀土氧化物或氧化钇或氧化硼或氧化镁进行改性，其中改性催化剂的等电点大于但不超过二氧化硅 - 氧化铝基质的2分。

9. 发明授权

US06652738B2 Process for preparing a mixed metal catalyst composition 有权
标题翻译：制备混合金属催化剂组合物的方法
公开(公告)号：US06652738B2
公开(公告)日：2003-11-25
申请号：US10346018
申请日：2003-01-16
申请人： Sonja Eijsbouts , Bob Gerardus Oogjen , Harmannus Willem Homan Free , Marinus Bruce Cerfontain , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
发明人： Sonja Eijsbouts , Bob Gerardus Oogjen , Harmannus Willem Homan Free , Marinus Bruce Cerfontain , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
IPC分类号： C10G4504
CPC分类号： B01J35/002 , B01J23/85 , B01J23/8885 , B01J35/0053 , B01J35/008 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J37/0009 , B01J37/0236 , B01J37/031 , B01J37/20 , C10G49/04
摘要： The invention pertains to a process for the hydroprocessing of a hydrocarbon feedstock wherein said feedstock is contacted at hydroprocessing conditions with a catalyst composition which comprises bulk catalyst particles which comprise at least one Group VIII non-noble metal and at least two Group VIB metals. The Group VIII and Group VIB metals comprise from about 50 wt. % to about 100 wt. %, calculated as oxides, of the total weight of the bulk catalyst particles. The metals are present in the catalyst composition in their oxidic and/or sulfidic state. The catalyst composition has an X-ray diffraction pattern in which the characteristic full width at half maximum does not exceed 2.5° when the Group VIB metals are molybdenum, tungsten, and, optionally, chromium, or does not exceed 4.0° when the Group VIB metals are molybdenum and chromium or tungsten and chromium.
摘要翻译：本发明涉及烃原料的加氢处理方法，其中所述原料在加氢处理条件下与催化剂组合物接触，所述催化剂组合物包含包含至少一种VIII族非贵金属和至少两种VIB族金属的本体催化剂颗粒。 VIII族和VIB族金属包含约50wt。％至约100重量％以体积催化剂颗粒的总重量计算的氧化物％。金属以其氧化和/或硫化态存在于催化剂组合物中。催化剂组合物具有X射线衍射图，其中当VIB族金属为钼，钨和任选的铬时，半峰的特征全宽度不超过2.5°，当VIB族VIB金属为不超过4.0°时金属是钼和铬或钨和铬。

10. 发明授权

US06582590B1 Multistage hydroprocessing using bulk multimetallic catalyst 有权
标题翻译：使用大量多金属催化剂的多级加氢处理
公开(公告)号：US06582590B1
公开(公告)日：2003-06-24
申请号：US09869982
申请日：2001-08-22
申请人： Kenneth Lloyd Riley , Darryl Patrick Klein , Zhiguo Hou , Stuart Leon Soled , Michael Charles Kerby , Gary Brice McVicker , Edward Stanley Ellis , Michele Sue Touvelle , Sabato Miseo
发明人： Kenneth Lloyd Riley , Darryl Patrick Klein , Zhiguo Hou , Stuart Leon Soled , Michael Charles Kerby , Gary Brice McVicker , Edward Stanley Ellis , Michele Sue Touvelle , Sabato Miseo
IPC分类号： C10G4500
CPC分类号： B01J23/002 , B01J23/85 , B01J23/88 , B01J23/883 , B01J23/8878 , B01J23/888 , B01J23/8885 , B01J37/03 , B01J37/082 , B01J2523/00 , C07C29/16 , C08F8/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G65/04 , C10G65/08 , C10G65/12 , C10G2400/10 , C10G2400/14 , C08F240/00 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/842 , B01J2523/67 , B01J2523/31 , B01J2523/41
摘要： Sulfur content of distillate feedstock, which is greater than 3,000 wppm, is reduced using multi-stage hydrodesulfurization by reacting the feestream in stages with reaction zone(s) containing bulk multimetallic catalyst comprised of Group VIII non-noble metal(s) and at least two group VIB metals. The ratio of Group VIB to Group VIII non-noble metals is 10:1 to 1:10.
摘要翻译：通过使用多级加氢脱硫，通过使包含阶段的发泡与包含第VIII族非贵金属的多体金属催化剂和至少包含第一组的多元金属催化剂的反应区反应来减少大于3,000wppm的馏出物原料的硫含量两组VIB金属。 VIB族与VIII族非贵金属的比例为10：1〜1:10。

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