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1. 发明授权

US5491267A Etherification process using post separation recycle 失效
标题翻译：使用后分离回收的醚化方法
公开(公告)号：US5491267A
公开(公告)日：1996-02-13
申请号：US207525
申请日：1994-03-07
申请人： Stanley J. Frey , David W. Liu , Charles P. Luebke , Terry L. Marker
发明人： Stanley J. Frey , David W. Liu , Charles P. Luebke , Terry L. Marker
IPC分类号： C07C41/06 , C07C41/42 , C07C43/02
CPC分类号： C07C41/42 , C07C41/06
摘要： In a process for the production of tertiary ethers by the reaction of an alcohol and isoalkene, a sidecut stream is selected from the etherification separation zone and recycled back to the etherification reaction zone. When this sidecut stream is characterized by an isoalkene to tertiary ether molar concentration ratio that is greater than the isoalkene to tertiary ether molar concentration ratio of the etherification reaction effluent (which is normally at equilibrium conditions), the conversion of isoalkene to tertiary ether is increased.
摘要翻译：在通过醇和异烯烃的反应生产叔醚的方法中，从醚化分离区中选择一条流，并循环回到醚化反应区。当该侧流的特征是异烯烃与叔醚摩尔浓度比大于醚化反应流出物（通常在平衡条件下）的异烯烃与叔醚摩尔浓度比时，异烯烃转化为叔乙醚的转化率增加。

2. 发明授权

US5689014A Integrated process for producing diisopropyl ether and an isopropyl tertiary alkyl ether 失效
标题翻译：用于生产二异丙醚和异丙基叔烷基醚的一体化方法
公开(公告)号：US5689014A
公开(公告)日：1997-11-18
申请号：US539577
申请日：1995-10-05
申请人： Stanley J. Frey , Robert J. Schmidt , Terry L. Marker , Richard E. Marinangeli
发明人： Stanley J. Frey , Robert J. Schmidt , Terry L. Marker , Richard E. Marinangeli
IPC分类号： C07C41/05 , C07C41/06
CPC分类号： C07C41/06 , C07C41/09 , Y02P20/125
摘要： A highly integrated process for concurrently producing diisopropyl ether and an isopropyl tertiary alkyl ether has been developed. In a first reactor, propylene and water are reacted to form isopropyl alcohol, a portion of which is further reacted to form diisopropyl ether. After removing unreacted propylene, the effluent of the first reactor is separated into an ether rich stream, a water rich stream and an alcohol rich stream. The alcohol rich stream and isobutylene, isoamylene or a mixture thereof are reacted to form an isopropyl tertiary alkyl ether in a second reactor. The water present in the alcohol rich stream also reacts with the iso-olefin to form tertiary alcohol. The effluent from the second reactor is water washed to produce an oxygenate product stream and an aqueous alcohol recycle stream. Some tertiary alcohol is recycled to the first reactor where it is reacted with propylene to form additional isopropyl tertiary alkyl ether. The isopropyl tertiary alkyl ether and some tertiary alcohol is collected along with the diisopropyl ether in the mixed oxygenate product stream from the water wash.
摘要翻译：已经开发了用于同时生产二异丙醚和异丙基叔烷基醚的高度一体化的方法。在第一反应器中，使丙烯和水反应形成异丙醇，其中一部分进一步反应形成二异丙醚。在除去未反应的丙烯之后，将第一反应器的流出物分离成富醚流，富水流和富醇流。使富含醇的物流和异丁烯，异戊烯或其混合物在第二反应器中反应形成异丙基叔烷基醚。存在于富酒精料流中的水也与异烯烃反应形成叔醇。将来自第二反应器的流出物进行水洗以产生含氧化合物产物流和含水酒精循环流。一些叔醇被再循环到第一反应器中，在其中与丙烯反应形成另外的异丙基叔烷基醚。异丙基叔烷基醚和一些叔醇与来自水洗的混合的含氧化合物产物流中的二异丙醚一起收集。

3. 发明授权

US5705712A Integrated process for producing diisopropyl ether, an isopropyl tertiary alkyl ether and isopropyl alcohol 失效
标题翻译：用于生产二异丙醚，异丙基叔烷基醚和异丙醇的一体化方法
公开(公告)号：US5705712A
公开(公告)日：1998-01-06
申请号：US539394
申请日：1995-10-05
申请人： Stanley J. Frey , Robert J. Schmidt , Terry L. Marker , Richard E. Marinangeli
发明人： Stanley J. Frey , Robert J. Schmidt , Terry L. Marker , Richard E. Marinangeli
IPC分类号： C07C41/05 , C07C41/06 , C07C41/00
CPC分类号： C07C41/06 , C07C41/09 , Y02P20/125
摘要： A highly integrated process for concurrently producing diisopropyl ether and an isopropyl tertiary alkyl ether has been developed. Optionally, high purity isopropyl alcohol may also be collected as a product. In a first reactor, propylene and water are reacted to form isopropyl alcohol, a portion of which is further reacted to form diisopropyl ether. After removing unreacted propylene, the effluent of the first reactor is separated into an ether rich stream, a water rich stream and an alcohol rich stream. The alcohol rich stream is dried to provide dry isopropyl alcohol. A portion of the dry isopropyl alcohol may be removed and collected as a product. A portion of the dry isopropyl alcohol and isobutylene, isoamylene or a mixture thereof are reacted to form an isopropyl tertiary alkyl ether in a second reactor. Unreacted iso-olefins and inert compounds are then removed from the second reactor effluent. A mixture of the effluent from the second reactor and the ether rich and the water rich streams separated from the first reactor are water washed to produce a mixed ethers product stream and an aqueous isopropyl alcohol recycle stream. The isopropyl tertiary alkyl ether is collected along with the diisopropyl ether in the mixed ethers product stream from the water wash. A modified flowscheme of the process is also discussed.
摘要翻译：已经开发了用于同时生产二异丙醚和异丙基叔烷基醚的高度一体化的方法。任选地，也可以收集高纯度异丙醇作为产物。在第一反应器中，使丙烯和水反应形成异丙醇，其中一部分进一步反应形成二异丙醚。在除去未反应的丙烯之后，将第一反应器的流出物分离成富醚流，富水流和富醇流。将富醇流干燥以提供干燥的异丙醇。干燥的异丙醇的一部分可以作为产品被去除和收集。一部分干异丙醇和异丁烯，异戊烯或其混合物在第二反应器中反应形成异丙基叔烷基醚。然后从第二反应器流出物中除去未反应的异烯烃和惰性化合物。将来自第二反应器的流出物和富含醚的混合物和从第一反应器分离的富水物流的混合物进行水洗以产生混合醚产物流和异丙醇水反应物水。异丙基叔烷基醚与来自水洗的混合醚产物流中的二异丙醚一起收集。还讨论了该过程的修改流程。

4. 发明申请

US20130012746A1 PRODUCTION OF PARAFFINIC FUEL FROM RENEWABLE FEEDSTOCKS 有权
标题翻译：从可再生原料生产配方燃料
公开(公告)号：US20130012746A1
公开(公告)日：2013-01-10
申请号：US13616915
申请日：2012-09-14
申请人： Charles P. Luebke , Stanley J. Frey
发明人： Charles P. Luebke , Stanley J. Frey
IPC分类号： C10G3/00 , C07C1/22
CPC分类号： C10G45/04 , C10G3/50 , C10G3/60 , C10G2300/1014 , C10G2300/1018 , C10G2300/4081 , C10G2400/02 , C10G2400/04 , C10G2400/08 , Y02P30/20
摘要： A process has been developed for producing fuel from renewable feedstocks such as plant and animal oils and greases. The process involves treating a first portion of a renewable feedstock by hydrogenating and deoxygenating in a first reaction zone and a second portion of a renewable feedstock by hydrogenating and deoxygenating in a second reaction zone to provide a diesel boiling point range fuel hydrocarbon product. If desired, the hydrocarbon product can be isomerized to improve cold flow properties. A portion of the hydrocarbon product is recycled to the first reaction zone to increase the hydrogen solubility of the reaction mixture.
摘要翻译：已经开发了用于从可再生原料如植物油和动物油和油脂生产燃料的方法。该方法包括通过在第二反应区中通过氢化和脱氧来在第一反应区和第二部分可再生原料中进行氢化和脱氧处理可再生原料的第一部分以提供柴油沸点范围的燃料烃产物。如果需要，烃产物可被异构化以改善冷流动性能。一部分烃产物再循环到第一反应区以提高反应混合物的氢溶解度。

5. 发明授权

US08766025B2 Production of paraffinic fuel from renewable feedstocks 有权
标题翻译：从可再生原料生产石蜡燃料
公开(公告)号：US08766025B2
公开(公告)日：2014-07-01
申请号：US13616915
申请日：2012-09-14
申请人： Charles P. Luebke , Stanley J. Frey
发明人： Charles P. Luebke , Stanley J. Frey
IPC分类号： C07C1/00 , C10G45/04 , C10G3/00
CPC分类号： C10G45/04 , C10G3/50 , C10G3/60 , C10G2300/1014 , C10G2300/1018 , C10G2300/4081 , C10G2400/02 , C10G2400/04 , C10G2400/08 , Y02P30/20
摘要： A process has been developed for producing fuel from renewable feedstocks such as plant and animal oils and greases. The process involves treating a first portion of a renewable feedstock by hydrogenating and deoxygenating in a first reaction zone and a second portion of a renewable feedstock by hydrogenating and deoxygenating in a second reaction zone to provide a diesel boiling point range fuel hydrocarbon product. If desired, the hydrocarbon product can be isomerized to improve cold flow properties. A portion of the hydrocarbon product is recycled to the first reaction zone to increase the hydrogen solubility of the reaction mixture.
摘要翻译：已经开发了用于从可再生原料如植物油和动物油和油脂生产燃料的方法。该方法包括通过在第二反应区中通过氢化和脱氧来在第一反应区和第二部分可再生原料中进行氢化和脱氧处理可再生原料的第一部分以提供柴油沸点范围燃料烃产物。如果需要，烃产物可被异构化以改善冷流动性能。一部分烃产物再循环到第一反应区以提高反应混合物的氢溶解度。

6. 发明申请

US20100305380A1 Process for Improved Meta-Xylene Yield from C8 Aromatics 有权
标题翻译： C8芳烃改进二甲苯产率的方法
公开(公告)号：US20100305380A1
公开(公告)日：2010-12-02
申请号：US12622824
申请日：2009-11-20
申请人： Stanley J. Frey , Jason T. Corradi , Richard S. Kempf , David W. Liu
发明人： Stanley J. Frey , Jason T. Corradi , Richard S. Kempf , David W. Liu
IPC分类号： C07C5/00 , C07C15/08
CPC分类号： C07C7/04 , C07C5/2737 , C07C7/13 , C07C15/08
摘要： Meta-xylene is recovered from admixture with other C8 aromatic hydrocarbons including ortho-xylene by liquid phase adsorptive separation. Performance is improved by reducing the concentration of ortho-xylene through adding a sidecut to a prefractionator preparing the feedstock to adsorptive separation.
摘要翻译：通过液相吸附分离从与其它C8芳族烃（包括邻二甲苯）混合中回收元二甲苯。通过向准备原料进行吸附分离的初步分选机中添加一次侧馏分，可以降低邻二甲苯的浓度来提高性能。

7. 发明授权

US07960600B2 Process for improved meta-xylene yield from C8 aromatics 有权
标题翻译：改进C8芳族化合物的间二甲苯产率的方法
公开(公告)号：US07960600B2
公开(公告)日：2011-06-14
申请号：US12622824
申请日：2009-11-20
申请人： Stanley J. Frey , Jason T. Corradi , Richard S. Kempf , David W. Liu
发明人： Stanley J. Frey , Jason T. Corradi , Richard S. Kempf , David W. Liu
IPC分类号： C07C7/12 , C07C7/04
CPC分类号： C07C7/04 , C07C5/2737 , C07C7/13 , C07C15/08
摘要： Meta-xylene is recovered from admixture with other C8 aromatic hydrocarbons including ortho-xylene by liquid phase adsorptive separation. Performance is improved by reducing the concentration of ortho-xylene through adding a sidecut to a prefractionator preparing the feedstock to adsorptive separation.
摘要翻译：通过液相吸附分离从与其它C8芳族烃（包括邻二甲苯）混合中回收元二甲苯。通过向准备原料进行吸附分离的初步分选机中添加一次侧馏分来降低邻二甲苯的浓度来提高性能。

8. 发明申请

US20130116495A1 ENERGY EFFICIENCY IN ADSORPTIVE SEPARATION 有权
标题翻译：吸收分离能量效率
公开(公告)号：US20130116495A1
公开(公告)日：2013-05-09
申请号：US13292713
申请日：2011-11-09
申请人： Stanley J. Frey , Lewis H. Pettengill , Michael R. Van de Cotte
发明人： Stanley J. Frey , Lewis H. Pettengill , Michael R. Van de Cotte
IPC分类号： C07C7/12
CPC分类号： C07C7/12 , B01D15/1828 , Y02P20/123 , Y02P20/57 , C07C15/08
摘要： The present process comprises a means for energy savings in one or more process pumps by driving the one or more pumps with a variable-speed driving means. The invention is particularly useful in the separation of an adsorbed product from a mixture of components using simulated-moving-bed adsorption associated with a large circulating stream pumped with variable-speed driving means for conservation of energy relative to the known art. The improvement is particularly applicable to a process for the separation of para-xylene from mixed C8 aromatics.
摘要翻译：本方法包括通过用变速驱动装置驱动一个或多个泵来在一个或多个处理泵中节能的装置。本发明特别可用于使用与用已知技术节约能源的可变速度驱动装置泵送的大循环流相关联的模拟移动床吸附分离吸附产物与组分混合物。该改进特别适用于从混合的C8芳族化合物中分离对二甲苯的方法。

9. 发明授权

US08283509B2 Thermal-separation process with absorption heat pump 有权
标题翻译：吸热式热分离工艺
公开(公告)号：US08283509B2
公开(公告)日：2012-10-09
申请号：US12630195
申请日：2009-12-03
申请人： Paul A. Sechrist , Stanley J. Frey
发明人： Paul A. Sechrist , Stanley J. Frey
IPC分类号： C07C7/04
CPC分类号： B01D3/007 , B01D3/143 , Y02B30/52
摘要： The invention comprises an absorption heat pump to supply energy to a distillation process or an outside process. The streams used to effect the absorption heat pump are to be combined in any case as a feedstream to a conversion process, and energy thus is conserved by avoiding the necessity of reseparating the streams.
摘要翻译：本发明包括一个用于向蒸馏过程或外部过程供应能量的吸收式热泵。用于影响吸收式热泵的流在任何情况下都将作为进料流组合到转化过程中，因此通过避免重新分离流的需要来节省能量。

10. 发明授权

US08198502B2 Process for separating para-xylene from a mixture of C8 and C9 aromatic hydrocarbons 有权
标题翻译：从C8和C9芳烃的混合物中分离对二甲苯的方法
公开(公告)号：US08198502B2
公开(公告)日：2012-06-12
申请号：US12719410
申请日：2010-03-08
申请人： Leonid Bresler , Stanley J. Frey
发明人： Leonid Bresler , Stanley J. Frey
IPC分类号： C07C7/13
CPC分类号： C07C7/005 , C07C7/13 , C07C15/08
摘要： The invention is an adsorptive separation process for producing a para-xylene product from a feed stream comprising para-xylene, at least one other C8 aromatic, and a C9 aromatic. An adsorbent comprising X or Y zeolite and a desorbent comprising para-diethylbenzene (p-DEB) are used in an adsorptive separation zone to produce an extract stream comprising para-xylene, p-DEB, and the C9 aromatic and a raffinate stream comprising the at least one other C8 aromatic, the C9 aromatic, and p-DEB. The extract stream is separated in an extract distillation zone to produce a second desorbent stream comprising the C9 aromatic and p-DEB and the raffinate stream is separated in a raffinate distillation zone to produce a third desorbent stream comprising the C9 aromatic and p-DEB. At least a portion of at least one of the second desorbent stream and the third desorbent stream is further separated in a desorbent distillation zone to produce a stream comprising the C9 aromatic.
摘要翻译：本发明是用于从包含对二甲苯，至少一种其它C 8芳族和C 9芳族的进料流产生对二甲苯产物的吸附分离方法。包含X或Y沸石的吸附剂和包含对二乙基苯（p-DEB）的解吸剂用于吸附分离区，以产生包含对二甲苯，p-DEB和C9芳族化合物的萃取物料流和含有至少一种其它C 8芳族，C 9芳族和p-DEB。萃取物流在提取蒸馏区中分离以产生包含C 9芳族和p-DEB的第二解吸流，并且萃余物流在萃余液蒸馏区中分离以产生包含C 9芳族和p-DEB的第三解吸流。第二解吸流和第三解吸流中的至少一个的至少一部分在解吸蒸馏区进一步分离以产生包含C 9芳族的物流。

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