会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 3. 发明申请
    • Methods of controlling the morphology of perovskite submicron-sized particles
    • 控制钙钛矿亚微米尺寸颗粒形态的方法
    • US20100129286A1
    • 2010-05-27
    • US12587491
    • 2009-10-06
    • Stanislaus S. WongHongjun Zhou
    • Stanislaus S. WongHongjun Zhou
    • C01G25/02
    • C01G25/00C01P2002/72C01P2004/03C01P2004/04C01P2004/32C01P2004/38C01P2004/61C01P2004/62
    • The present invention includes a method of making a plurality of nanoparticles comprising single crystalline spherical BaZrO3 particles, cubic BaZrO3 particles or a mixture of both. The method comprises: providing a mixture of a barium precursor, a zirconium precursor and a hydroxide salt or hydroxide salts; heating the mixture to an isothermic annealing temperature, wherein the annealing temperature is in a range of from about 470° C. to about 800° C.; annealing the mixture at the isothermic annealing temperature for an annealing time of in a range of about 15 minutes to about 280 minutes; and cooling the mixture at a fixed cooling rate to form the plurality of nanoparticles, wherein the cooling rate is in a range of from about 2° C./minute to about 200° C./minute. The ratio of spherical particles to cubic particles in the plurality is greater if the isothermic annealing temperature is at the higher end of the range; the ratio of spherical particles to cubic particles in the plurality is greater if the annealing time is at the higher end of the range; and the ratio of spherical particles to cubic particles in the plurality is greater if the cooling rate is at the lower end of the range.
    • 本发明包括制造包含单晶球形BaZrO 3颗粒,立方BaZrO 3颗粒或两者的混合物的多种纳米颗粒的方法。 该方法包括:提供钡前体,锆前体和氢氧化物盐或氢氧化物盐的混合物; 将混合物加热到等温退火温度,其中退火温度在约470℃至约800℃的范围内; 在等温退火温度下退火混合物,退火时间为约15分钟至约280分钟; 并以固定的冷却速度冷却混合物以形成多个纳米颗粒,其中冷却速率在约2℃/分钟至约200℃/分钟的范围内。 如果等温退火温度在该范围的较高端,多颗粒中的球形颗粒与立方颗粒的比率更大; 如果退火时间在该范围的较高端,则多个球形颗粒与立方体颗粒的比例更大; 如果冷却速率在该范围的较低端,则多个球形颗粒与立方体颗粒的比例更大。