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    • 7. 发明授权
    • Continuous monitoring of organic pollutants
    • 持续监测有机污染物
    • US5435169A
    • 1995-07-25
    • US76414
    • 1993-06-14
    • Somenath Mitra
    • Somenath Mitra
    • G01N30/00G01N30/02G01N30/12G01N30/62G01N33/00G01N33/18G01N30/14
    • G01N33/0049G01N30/00G01N30/12G01N33/0016G01N33/1826G01N2030/025G01N2030/121G01N2030/623G01N2033/0019
    • A method and device for the continuous monitoring of very low level concentrations of materials such as volatile organic compound (VOC) pollutant levels in a fluid (gaseous or liquid) stream, including stack gases and waste water. The fluid stream passes through an on-line micro sorbent trap (OLMT) for entrapment of VOCs. The pollutants are concentrated in the OLMT and electrically rapidly heated to simulate an injection into a gas chromatograph system or other detector. The concentration and heating steps are effected at predetermined time intervals and temperature conditions with correlation to known fluid flow rates. Pollutants separate in the chromatographic column with a chromatograph being obtained with each injection for identification of pollutants and respective pollution levels. Alternatively, without chromatograph, a single peak is obtained which represents the total quantity of pollutants in the fluid stream. The OLMT enhances sensitivity such that low concentrations can be accurately measured on a continuous basis. The device can further include a sampling valve which samples the fluid stream into the OLMT and then connects the OLMT with a GC carrier gas to avoid incompatible gas flow through the OLMT or the GC detector.
    • 用于连续监测流体(气态或液体)流(包括烟气和废水)中非常低浓度物质的挥发性有机化合物(VOC)污染物水平的方法和装置。 流体流通过在线微吸附阱(OLMT),用于捕获VOC。 这些污染物集中在OLMT中,电气快速加热,以模拟注入气相色谱系统或其他检测器。 浓度和加热步骤以与已知流体流速相关的预定时间间隔和温度条件进行。 污染物在色谱柱中分离,每个注射液均可获得色谱,用于鉴定污染物和各自的污染水平。 或者,没有色谱,获得表示流体流中污染物总量的单个峰。 OLMT增强灵敏度,使得可以连续地精确测量低浓度。 该装置还可以包括采样阀,其将流体流采样到OLMT中,然后将OLMT与GC载气连接,以避免与OLMT或GC检测器不相容的气体流。