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1. 发明授权

US07129195B2 Heterogenically catalysed gas-phase partial oxidation method for precursor compounds of (meth)acrylic acid 失效
标题翻译：（甲基）丙烯酸前体化合物的异相催化气相部分氧化法
公开(公告)号：US07129195B2
公开(公告)日：2006-10-31
申请号：US10466244
申请日：2002-01-12
申请人： Raimund Felder , Signe Unverricht , Heiko Arnold , Jochen Petzoldt
发明人： Raimund Felder , Signe Unverricht , Heiko Arnold , Jochen Petzoldt
IPC分类号： B01J23/00 , B01J21/00
CPC分类号： C07C51/235 , B01J19/30 , B01J23/28 , B01J23/31 , B01J23/8876 , B01J23/8877 , B01J35/002 , B01J35/026 , B01J2219/30223 , B01J2219/30242 , B01J2219/30475 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： The invention relates to a method for the heterogenically catalyed gas-phase partial oxidation of precursor compounds of (meth)acrylic acid in a fixed catalyst bed, containing as the catalyst an activated mass of mixed oxide, shaped to form a geometric body. Said geometric body is a geometric base body, into whose surface a cavity is incorporated.
摘要翻译：本发明涉及在固定催化剂床中异构催化气相部分氧化前体化合物（甲基）丙烯酸的方法，该方法含有形成几何体的成形为混合氧化物的活化物质作为催化剂。所述几何体是几何基体，其表面中并入有空腔。

2. 发明申请

US20070032680A1 Heterogeneously catalyzed gas-phase partial oxidation of precursor compounds of (meth)acrylic acid 审中-公开
标题翻译：（甲基）丙烯酸前体化合物的非均相催化气相部分氧化
公开(公告)号：US20070032680A1
公开(公告)日：2007-02-08
申请号：US11443135
申请日：2006-05-31
申请人： Raimund Felder , Signe Unverricht , Heiko Arnold , Jochen Petzoldt
发明人： Raimund Felder , Signe Unverricht , Heiko Arnold , Jochen Petzoldt
IPC分类号： C07C51/16 , C07C51/235
CPC分类号： C07C51/235 , B01J19/30 , B01J23/28 , B01J23/31 , B01J23/8876 , B01J23/8877 , B01J35/002 , B01J35/026 , B01J2219/30223 , B01J2219/30242 , B01J2219/30475 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： In a process for the heterogeneously catalyzed gas-phase partial oxidation of precursor compounds of (meth)acrylic acid over a fixed catalyst bed which contains, as a catalyst, a mixed oxide active material shaped into a geometric body, the geometric body is a geometric base body into whose surface a cavity has been introduced.
摘要翻译：在（甲基）丙烯酸前体化合物在固定催化剂床上的非均相催化气相部分氧化的方法中，该固定催化剂床含有形成几何体的混合氧化物活性物质作为催化剂，几何体是几何体基体已经被引入其表面。

3. 发明授权

US06794539B2 Method for producing multiple-phase multi-metal oxide materials 失效
标题翻译：多相多金属氧化物材料的制造方法
公开(公告)号：US06794539B2
公开(公告)日：2004-09-21
申请号：US10380159
申请日：2003-03-17
申请人： Signe Unverricht , Raimund Felder , Heiko Arnold , Jochen Petzoldt
发明人： Signe Unverricht , Raimund Felder , Heiko Arnold , Jochen Petzoldt
IPC分类号： C07C5116
CPC分类号： B01J37/00 , B01J23/002 , B01J23/887 , B01J35/0006 , B01J2523/00 , C07C51/252 , C07C57/04 , B01J2523/17 , B01J2523/55 , B01J2523/68 , B01J2523/69
摘要： In a process for preparing a multiplephase multimetal oxide composition comprising Mo, V, Cu and, if desired, further elements, at least one phase is preformed separately and dispersed in a plastically deformable precursor composition of a further phase. The mixture is dried and calcined. The multimetal oxide composition is suitable as active composition of catalysts for the catalytically oxidation of organic compounds in the gas phase, in particular for the oxidation of acrolein to acrylic acid.
摘要翻译：在制备包含Mo，V，Cu的多相多金属氧化物组合物的方法中，并且如果需要，另外的元素，至少一个相分别预成型并分散在另一相的可塑变形的前体组合物中。将混合物干燥并煅烧。多金属氧化物组合物适合用作气相中有机化合物催化氧化的催化剂的活性组合物，特别是用于将丙烯醛氧化成丙烯酸。

4. 发明授权

US06881702B2 Method for producing a multi metal oxide catalyst, method for producing unsaturated aldehydes and/or carboxylic acids and band calcination device 有权
标题翻译：多金属氧化物催化剂的制造方法，不饱和醛和/或羧酸的制造方法以及带烧结装置
公开(公告)号：US06881702B2
公开(公告)日：2005-04-19
申请号：US10363856
申请日：2001-09-20
申请人： Heiko Arnold , Signe Unverricht , Raimund Felder , Klaus Harth , Klaus Joachim Müller-Engel
发明人： Heiko Arnold , Signe Unverricht , Raimund Felder , Klaus Harth , Klaus Joachim Müller-Engel
IPC分类号： B01J6/00 , B01J19/18 , B01J19/22 , B01J23/88 , B01J23/888 , B01J35/00 , B01J37/08 , C07B61/00 , C07C27/14 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/38 , C07C47/22 , C07C51/215 , C07C51/25 , C07C57/05 , B01J23/00 , B01J21/08 , B01J21/12 , B01J21/14 , B01J27/192
CPC分类号： C07C51/215 , B01J6/004 , B01J19/1862 , B01J19/22 , B01J23/002 , B01J23/88 , B01J23/8885 , B01J35/0006 , B01J37/08 , B01J2219/00132 , B01J2219/00157 , B01J2219/182 , B01J2523/00 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/38 , C07C51/252 , C07C47/22 , C07C57/04 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845
摘要： A catalyst suitable for the gas-phase oxidation of organic compounds to α,β-unsaturated aldehydes and/or carboxylic acids and having an active phase comprising a multimetal oxide material is prepared by a process in which a particulate catalyst precursor which contains oxides and/or compounds of the elements other than oxygen which constitute the multimetal oxide material, which compounds can be converted into oxides, is prepared and said catalyst precursor is converted by calcination into a catalytically active form, wherein a stream of the particulate catalyst precursor is passed at substantially constant speed through at least one calcination zone at constant temperature for calcination.
摘要翻译：适合于将有机化合物气相氧化成α，β-不饱和醛和/或羧酸并且具有包含多金属氧化物材料的活性相的催化剂通过以下方法制备，其中含有氧化物和/ 或构成多金属氧化物材料的氧以外的元素的化合物，该化合物可以转化为氧化物，并且将所述催化剂前体通过煅烧转化为催化活性形式，其中将颗粒状催化剂前体的流通过通过至少一个煅烧区在恒定温度下用于煅烧的基本上恒定的速度。

5. 发明申请

US20090171117A1 METHOD FOR PRODUCING A MULTI METAL OXIDE CATALYST, METHOD FOR PRODUCING UNSATURATED ALDEHYDES AND/OR CARBOXYLIC ACIDS AND BAND CALCINATION DEVICE 审中-公开
标题翻译：用于生产多金属氧化物催化剂的方法，用于生产不饱和醛和/或羧酸的方法和带计算装置
公开(公告)号：US20090171117A1
公开(公告)日：2009-07-02
申请号：US12396292
申请日：2009-03-02
申请人： Heiko Arnold , Signe Unverricht , Raimund Felder , Klaus Harth , Klaus Joachim Muller-Engel
发明人： Heiko Arnold , Signe Unverricht , Raimund Felder , Klaus Harth , Klaus Joachim Muller-Engel
IPC分类号： B01J21/06 , C07C53/00 , C07C51/21 , C07C51/235 , C07C45/29 , C07C45/34 , C07C45/33
CPC分类号： C07C51/215 , B01J6/004 , B01J19/1862 , B01J19/22 , B01J23/002 , B01J23/88 , B01J23/8885 , B01J35/0006 , B01J37/08 , B01J2219/00132 , B01J2219/00157 , B01J2219/182 , B01J2523/00 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/38 , C07C51/252 , C07C47/22 , C07C57/04 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845
摘要： A catalyst suitable for the gas-phase oxidation of organic compounds to α,β-unsaturated aldehydes and/or carboxylic acids and having an active phase comprising a multimetal oxide material is prepared by a process in which a particulate catalyst precursor which contains oxides and/or compounds of the elements other than oxygen which constitute the multimetal oxide material, which compounds can be converted into oxides, is prepared and said catalyst precursor is converted by calcination into a catalytically active form, wherein a stream of the particulate catalyst precursor is passed at substantially constant speed through at least one calcination zone at constant temperature for calcination.
摘要翻译：适合于将有机化合物气相氧化成α，β-不饱和醛和/或羧酸并且具有包含多金属氧化物材料的活性相的催化剂通过以下方法制备，其中含有氧化物和/ 或构成多金属氧化物材料的氧以外的元素的化合物，该化合物可以转化为氧化物，并且将所述催化剂前体通过煅烧转化为催化活性形式，其中将颗粒状催化剂前体的流通过通过至少一个煅烧区在恒定温度下用于煅烧的基本上恒定的速度。

6. 发明授权

US07589046B2 Thermal treatment of the precursor material of a catalytically active material 有权
标题翻译：催化活性材料的前体材料的热处理
公开(公告)号：US07589046B2
公开(公告)日：2009-09-15
申请号：US10843632
申请日：2004-05-12
申请人： Martin Dieterle , Wolfgang Juergen Poepel , Silke Berndt , Raimund Felder , Signe Unverricht , Klaus Joachim Mueller-Engel
发明人： Martin Dieterle , Wolfgang Juergen Poepel , Silke Berndt , Raimund Felder , Signe Unverricht , Klaus Joachim Mueller-Engel
IPC分类号： B01J23/00
CPC分类号： B01J23/002 , B01J23/885 , B01J37/0009 , B01J37/0045 , B01J37/0223 , B01J37/08 , B01J2523/00 , C07C51/252 , C21B13/006 , C21B13/0073 , C21B13/08 , C21B2100/44 , C22B1/216 , C22B34/00 , C22B34/30 , Y02P10/136 , C07C57/04 , B01J2523/17 , B01J2523/55 , B01J2523/68 , B01J2523/69
摘要： In a process for the thermal treatment of the precursor material of a catalytically active material in a rotary tube furnace through which a gas stream flows, at least a proportion of the gas stream flowing through the rotary tube furnace is circulated, and the associated rotary tube furnace apparatus and tube-bundle reactors for the partial gas-phase oxidation of acrolein to acrylic acid are loaded with catalysts whose catalytically active material is obtainable by the process for the thermal treatment.
摘要翻译：在用于热处理旋转管式炉中的催化活性材料的前体材料的方法中，气流流过该方法，使流过旋转管式炉的气流的至少一部分循环，并将相关的旋转管用于将丙烯醛部分气相氧化成丙烯酸的炉装置和管束反应器装载有催化活性物质可通过热处理方法获得的催化剂。

7. 发明授权

US06383976B1 Multimetal oxide material for gas-phase catalytic oxidation of organic compounds 有权
标题翻译：用于气相催化氧化有机化合物的多金属氧化物材料
公开(公告)号：US06383976B1
公开(公告)日：2002-05-07
申请号：US09452452
申请日：1999-12-02
申请人： Heiko Arnold , Klaus Harth , Hans-Peter Neumann , Ulrich Hammon , Raimund Felder
发明人： Heiko Arnold , Klaus Harth , Hans-Peter Neumann , Ulrich Hammon , Raimund Felder
IPC分类号： B01J2300
CPC分类号： C07C45/35 , B01J23/002 , B01J23/8876 , B01J2523/00 , C01G39/006 , C01G49/009 , C07C45/33 , C07C45/34 , C07C51/252 , C07C47/22 , C07C57/04 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/845
摘要： The multimetal oxide materials essentially consisting of Mo12BiaX1bFecX2dX3eOy (I) where: X1 is Co and/or Ni, X2 is Si and/or Al, X3 is an alkali metal, 0.3≦a≦1, 2≦b≦10, 0.5≦c≦10, 0≦d≦10, 0≦e≦0.5 and y is the absolute value of the number which, assuming charge neutrality, is obtained from the sum of the valences and the stoichiometric coefficients of the other elements, the crystalline fractions containing, in addition to &bgr;-X1MoO4 as the main component, Fe2(MoO4)3 as a secondary component and no MoO3.
摘要翻译：基本上由以下组成的多金属氧化物材料：X1是Co和/或Ni，X2是Si和/或Al，X3是碱金属，0.3 <= a <= 1,2 <= b <= 10,0.5 <= c <= 10,0 <= d <= 10,0 <= e <= 0.5，并且假定电荷中性是从其他元素的化合价和化学计量系数的和获得的数的绝对值，除了以β-X1MoO4为主要成分之外，还含有Fe2（MoO4）3作为次要组分而不含MoO 3的结晶组分。

8. 发明申请

US20070032377A1 Process for preparing shaped catalyst bodies whose active composition is a multielement oxide 审中-公开
标题翻译：制备活性组合物为多元素氧化物的成型催化剂体的方法
公开(公告)号：US20070032377A1
公开(公告)日：2007-02-08
申请号：US11498795
申请日：2006-08-04
申请人： Hartmut Hibst , Raimund Felder , Heiko Arnold , Andreas Raichle , Klaus Muller-Engel
发明人： Hartmut Hibst , Raimund Felder , Heiko Arnold , Andreas Raichle , Klaus Muller-Engel
IPC分类号： B01J21/02 , B29C67/00
CPC分类号： B01J23/002 , B01J23/8876 , B01J23/8885 , B01J27/198 , B01J27/24 , B01J35/0006 , B01J35/023 , B01J35/026 , B01J35/1009 , B01J35/1038 , B01J37/0009 , B01J37/0045 , B01J37/08 , B01J2523/00 , C07C51/215 , C07C51/235 , C07C51/252 , C07C57/04 , B01J2523/15 , B01J2523/17 , B01J2523/51 , B01J2523/53 , B01J2523/55 , B01J2523/62 , B01J2523/68 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/842 , B01J2523/845 , B01J2523/69 , C07C57/145
摘要： A process for preparing shaped catalyst bodies whose active composition is a multielement oxide, in which a finely divided precursor mixture is shaped to a desired geometry with addition of boron nitride and subsequently treated thermally.
摘要翻译：一种制备其活性组合物为多元素氧化物的成形催化剂体的方法，其中将细分散的前体混合物通过加入氮化硼成型为所需几何形状并随后热处理。

9. 发明授权

US06518220B2 Shaped catalysts 失效
标题翻译：成型催化剂
公开(公告)号：US06518220B2
公开(公告)日：2003-02-11
申请号：US09782307
申请日：2001-02-14
申请人： Christian Walsdorff , Otto Hofstadt , Raimund Felder , Ruprecht Meissner , Klaus Harth
发明人： Christian Walsdorff , Otto Hofstadt , Raimund Felder , Ruprecht Meissner , Klaus Harth
IPC分类号： B01J2370
CPC分类号： C07C51/252 , B01J19/30 , B01J23/72 , B01J23/78 , B01J27/122 , B01J35/026 , B01J2219/30223 , B01J2219/30475 , B01J2219/312 , C07C17/15 , C07C17/156 , C07C51/215 , C07C51/265 , Y10T428/13 , Y10T428/1397 , C07C19/045 , C07C57/145 , C07C57/04 , C07C63/16
摘要： Shaped catalysts for heterogeneously catalyzed reactions are in the form of hollow cylinders or annular tablets whose end faces are rounded both to the outer edge and to the edge of the central hole, i.e. have no right-angled edges.
摘要翻译：用于非均相催化反应的成型催化剂是中空圆柱体或环形片剂的形式，其端面向外边缘和中心孔的边缘成圆形，即没有直角的边缘。

10. 发明申请

US20110313207A1 PROCESS FOR DISTILLATIVE WORKUP OF A METHANOL/WATER MIXTURE AND PROCESS FOR PREPARING ALKALI METAL METHOXIDES 审中-公开
标题翻译：甲醇/水混合物的分解工艺及制备碱金属甲醇的方法
公开(公告)号：US20110313207A1
公开(公告)日：2011-12-22
申请号：US13203504
申请日：2010-02-17
申请人： Gerd Kaibel , Tilman Sirch , Raimund Felder , Josef Guth
发明人： Gerd Kaibel , Tilman Sirch , Raimund Felder , Josef Guth
IPC分类号： B01D3/00 , C07C29/00
CPC分类号： B01D3/009 , B01D1/2856 , B01D3/14 , C07C29/70 , Y02P20/127 , C07C31/30
摘要： The invention relates to a process for distillative workup of a methanol/water mixture, in which a methanol/water mixture is added to a distillation column (1), an essentially methanol-comprising vapor stream is withdrawn at the top of the distillation column (1) and an essentially water-comprising bottom stream at the bottom of the distillation column (1), at least a portion of the essentially methanol-comprising vapor stream is compressed and the compressed vapor stream is added as heating vapor to an evaporator (11) in which at least a portion of the methanol/water mixture to be separated is evaporated. The invention further relates to a process for preparing alkali metal methoxides in a reaction column (31) by adding methanol and alkali metal hydroxide solution to the reaction column (31), withdrawing alkali metal methoxide dissolved in methanol at the lower end of the reaction column (31) and withdrawing a methanol/water mixture at the upper end of the reaction column (31), and working up the methanol/water mixture by the process for distillative workup.
摘要翻译：本发明涉及一种用于甲醇/水混合物的蒸馏处理方法，其中将甲醇/水混合物加入到蒸馏塔（1）中，基本上含甲醇的蒸气流在蒸馏塔的顶部排出（ 1）和在蒸馏塔（1）底部的基本上含水的底部流，至少部分基本上含甲醇的蒸气流被压缩，并将压缩的蒸气流作为加热蒸气加入到蒸发器（11 ），其中要分离的至少一部分甲醇/水混合物蒸发。本发明还涉及通过向反应塔（31）中加入甲醇和碱金属氢氧化物溶液，在反应塔（31）的下端除去溶解在甲醇中的碱金属甲醇盐，在反应塔（31）中制备碱金属甲醇盐的方法（31），并在反应塔（31）的上端取出甲醇/水混合物，并通过蒸馏处理方法处理甲醇/水混合物。

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