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1. 发明授权

US4022152A Apparatus for making particulate materials, particularly oxides, hydrophobic 失效
标题翻译：用于制造疏水性颗粒材料，特别是氧化物的装置
公开(公告)号：US4022152A
公开(公告)日：1977-05-10
申请号：US533675
申请日：1974-12-17
申请人： Siegmar Laufer , Waldemar Roy
发明人： Siegmar Laufer , Waldemar Roy
IPC分类号： C01B13/14 , C01B33/113 , C07F7/12 , C08K9/06 , C08K9/08 , C09C1/30 , C09C1/40 , C09C3/00 , C09C3/12 , C23C13/08
CPC分类号： C09C3/12 , C01B13/145 , C01B33/18 , C08K9/06 , C08K9/08 , C09C1/3081 , C09C1/405 , C09C3/006 , C01P2004/82 , C01P2006/80 , C01P2006/90
摘要： An apparatus for making particulate materials hydrophobic has means for activating the material, means for charging the material with a substance capable of imparting hydrophobic characteristics thereto, means for causing reaction between the material and the substance with which it is charged and means for treating the material subsequent to the reaction so as to remove excess of the substance therefrom.
摘要翻译：用于制造疏水性颗粒材料的装置具有用于活化材料的装置，用能够赋予疏水特性的物质对材料进行充填的装置，用于引起材料与被充电的物质之间的反应的装置以及用于处理材料的装置在反应之后，以从其中除去过量的物质。

2. 发明授权

US3948676A Process for preparing hydrophobic particles 失效
标题翻译：制备疏水颗粒的方法
公开(公告)号：US3948676A
公开(公告)日：1976-04-06
申请号：US472924
申请日：1974-05-23
申请人： Siegmar Laufer
发明人： Siegmar Laufer
IPC分类号： C01B13/14 , C01B33/113 , C08K9/06 , C09C1/30 , C09C3/00 , C09C3/12 , C09C1/28
CPC分类号： C09C3/12 , C01B13/145 , C01B33/113 , C08K9/06 , C09C1/30 , C09C1/3081 , C09C1/309 , C09C3/006 , C01P2006/12 , C01P2006/20 , C01P2006/80 , C01P2006/90
摘要： A process for preparing hydrophobic finely divided oxides of metals and/or oxides of silicon comprising activating finely divided particles of oxides of metals and/or oxides of silicon by heating the particles at about 700.degree. - 1000.degree.C for less than about 60 seconds in a stream of inert gas to substantially completely free the particles of not only the physically bonded, but also the chemically bonded water, and contacting the activated particles with at least one organosilicon compound and substantially anhydrous ammonia gas for less than about 60 seconds. The hydrophobic products are useful as fillers in elastomers.
摘要翻译：一种用于制备金属和/或氧化物的疏水性微细氧化物的方法，其包括通过在约700-1000℃下将颗粒加热至少约60秒而活化细碎的金属和/或氧化物的氧化物颗粒惰性气体流，基本上完全不含物理结合的颗粒，也是化学键合的水，并使活化的颗粒与至少一种有机硅化合物和基本上无水的氨气接触少于约60秒。疏水产物可用作弹性体中的填料。

3. 发明授权

US4068024A Process for preparing finely divided hydrophobic oxide particles 失效
标题翻译：制备细分疏水性氧化物颗粒的方法
公开(公告)号：US4068024A
公开(公告)日：1978-01-10
申请号：US496676
申请日：1974-08-12
申请人： Siegmar Laufer
发明人： Siegmar Laufer
IPC分类号： C01B13/14 , C01B33/113 , C08K9/06 , C09C1/30 , C09C3/00 , C09C3/12 , B23K31/02 , B23K35/38
CPC分类号： C09C3/12 , C01B13/145 , C01B33/113 , C08K9/06 , C09C1/30 , C09C1/3081 , C09C1/309 , C09C3/006 , C01P2004/80 , C01P2006/90
摘要： A process for preparing hydrophobic finely divided particles of oxides of metals and/or oxides of silicon by chemically bonding hydrocarbon radicals to the surface of the oxide particles, said process comprising intensively mixing oxide particles having a water content less than about 1% by weight with a hydrolyzable metal or metalloid compound containing OR groups, wherein said compound is an ester of the general formula:Me(OR).sub.4wherein Me is an element from group IV of the periodic table, and each R is independently selected from C.sub.1 -C.sub.8 alkyl radicals or an aryl radical. A hydrophobic silicon dioxide particle is provided. Particles prepared by the process are useful as fillers in elastomers.
摘要翻译：通过将烃基化学键合到氧化物颗粒的表面来制备金属和/或氧化物的氧化物的疏水细碎颗粒的方法，所述方法包括将具有小于约1重量％的水含量的氧化物颗粒与含有OR基团的可水解金属或准金属化合物，其中所述化合物是下列通式的酯：

4. 发明授权

US4007050A Hydrophobic oxides of metals and for metalloids 失效
标题翻译：金属和准金属的疏水性氧化物
公开(公告)号：US4007050A
公开(公告)日：1977-02-08
申请号：US543368
申请日：1975-01-23
申请人： Siegmar Laufer , Roy Waldemar
发明人： Siegmar Laufer , Roy Waldemar
IPC分类号： C01B13/14 , C01B33/113 , C07F7/12 , C08K9/06 , C08K9/08 , C09C1/30 , C09C1/40 , C09C3/00 , C09C3/12
CPC分类号： C09C3/12 , C01B13/145 , C01B33/113 , C08K9/06 , C08K9/08 , C09C1/3081 , C09C1/405 , C09C3/006 , C01P2004/82 , C01P2006/12 , C01P2006/80 , C01P2006/90
摘要： Highly dispersed metal or metalloid oxides are rendered hydrophobic byI. contacting such oxide particles while in the form of an aerogel with a dry inert gas stream in a fluidizing bed at a temperature from 600.degree. to 1000.degree. C and at atmospheric pressure for a period of less than 60 seconds to render the particles absolutely dry and thus activate them;Ii. charging the resultant dried and activated particles in a fluidizing bed with at least one gas-phase organosilicon compound selected from the group consisting of (a) linear organopolysiloxanes (b) cyclic organopolysiloxanes (c) a mixture of both types of siloxanes and (d) a mixture of any of the substances (a)-(c) with an organohalogenosilane at a temperature in the range from 25.degree. to 650.degree. C;Iii. causing said charged particles to react with the organosilicon compounds at a temperature from 35.degree. to 650.degree. C; andIv. finally treating the reaction product with an inert gas stream in a fluidizing bed at temperatures from 500.degree. to 125.degree. C.
摘要翻译：高分散的金属或准金属氧化物通过I使这种氧化物颗粒接触而形成疏水性，同时气态凝胶形式为干燥惰性气流，流化床在600℃至1000℃的温度和大气压下持续一段时间小于60秒以使颗粒绝对干燥并因此激活它们; 二，将所得干燥和活化的颗粒在流化床中用至少一种选自（a）线性有机聚硅氧烷（b）环状有机聚硅氧烷（c）两种类型的硅氧烷和（d）的混合物的气相有机硅化合物）任何物质（a） - （c）与有机卤代硅烷的混合物在25至650℃的温度范围内; 三，使所述带电粒子在35〜650℃的温度下与有机硅化合物反应; 和IV。最后在惰性气流中在500-125℃的温度下在流化床中处理反应产物。

5. 发明授权

US4164509A Process for preparing finely divided hydrophobic oxide particles 失效
标题翻译：制备细分疏水性氧化物颗粒的方法
公开(公告)号：US4164509A
公开(公告)日：1979-08-14
申请号：US847508
申请日：1977-11-01
申请人： Siegmar Laufer
发明人： Siegmar Laufer
IPC分类号： C01B13/14 , C01B33/113 , C08K9/06 , C09C1/30 , C09C3/00 , C09C3/12 , C07F7/04 , C07F7/18
CPC分类号： C09C3/12 , C01B13/145 , C01B33/113 , C08K9/06 , C09C1/30 , C09C1/3081 , C09C1/309 , C09C3/006 , C01P2004/80 , C01P2006/90
摘要： A process for preparing hydrophobic finely divided particles of oxides of metals and/or oxides of silicon by chemically bonding hydrocarbon radicals to the surface of the oxide particles, said process comprising intensively mixing oxide particles having a water content less than about 1% by weight with a hydrolizable metal or metalloid compound containing OR groups, wherein said compound is an ester of the general formula:Me(OR).sub.4wherein Me is an element from group IV of the periodic table, and each R is independently selected from C.sub.1 -C.sub.8 alkyl radicals or an aryl radical. A hydrophobic silicon dioxide particle is provided. Particles prepared by the process are useful as fillers in elastomers.
摘要翻译：通过将烃基化学键合到氧化物颗粒的表面来制备金属和/或氧化物的氧化物的疏水细碎颗粒的方法，所述方法包括将具有小于约1重量％的水含量的氧化物颗粒与含有OR基团的可水解金属或准金属化合物，其中所述化合物是下列通式的酯：

6. 发明授权

US4036933A Highly-active, finely divided super-dry silicon dioxide 失效
标题翻译：高活性，细分的超干二氧化硅
公开(公告)号：US4036933A
公开(公告)日：1977-07-19
申请号：US594710
申请日：1975-07-10
申请人： Siegmar Laufer , Waldemar Roy
发明人： Siegmar Laufer , Waldemar Roy
IPC分类号： C01B33/18 , C09C1/30 , C01B33/16
CPC分类号： C09C1/3027 , C01B33/183 , C01P2002/82 , C01P2006/12 , C01P2006/22 , C01P2006/80 , C01P2006/82 , C01P2006/90
摘要： A highly active superdry silica aerogel free of adsorbed water and hydrogen-bonded silanol groups the infrared spectrum of which is characterized by a single narrow intense band at about 3700 cm.sup..sup.-1 within the range between 4000 and 2000 cm.sup..sup.-1 indicating the presence of free silanol groups and which spectrum is further characterized by the absence of bonds indicating the presence of adsorbed water and hydrogen-bonded silanol groups, the said silica aerogel having been produced by subjecting a pyrolytically produced silica aerogel containing adsorbed water and both free and hydrogen-bonded silanol groups to treatment in a fluidized bed at a temperature between about 700.degree. and 1000.degree. C and at a pressure between 2 torrs and atmospheric pressure for a period between 1 second and a few minutes through which fluidized bed a stream of a dried gas that had been preheated to a temperature between 100.degree. and 300.degree. C was passed.
摘要翻译：一种高活性的超干硅胶气凝胶，不含吸附水和氢键硅烷醇基团，其红外光谱的特征是在4000和2000厘米-1之间的范围内的约3700厘米-1的单个窄的强带，表明游离硅烷醇基团的存在，并且哪个光谱的进一步特征在于不存在指示存在吸附的水和氢键合的硅烷醇基团的键，所述二氧化硅气凝胶是通过对含有吸附水的热解产生的二氧化硅气凝胶和两种游离的和氢键合的硅烷醇基团在流化床中在约700℃至1000℃的温度和在2托和大气压之间的压力下处理1秒至几分钟之间的时间，通过该流化床将流化床将预热至100〜300℃的干燥气体通过。

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