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1. 发明授权

US5672868A Mass spectrometer system and method for transporting and analyzing ions 失效
标题翻译：离子质谱仪系统及其分析方法
公开(公告)号：US5672868A
公开(公告)日：1997-09-30
申请号：US605346
申请日：1996-02-16
申请人： Alexander Mordehai , Sidney E. Buttrill, Jr.
发明人： Alexander Mordehai , Sidney E. Buttrill, Jr.
IPC分类号： H01J49/04 , H01J49/42 , H01J49/00
CPC分类号： H01J49/0445 , H01J49/063
摘要： A mass spectrometer system for performing a separation of ions from neutrals and mass analyzing ions comprising an ion generating source with an ion introduction system, a radio-frequency ion guide and a mass analyzer disposed within a vacuum chamber. The radio-frequency ion guide is positioned with respect to the ion introduction system so that a main axis of the radio-frequency ion guide is angled toward a central axis of the ion introduction system. The trajectory of the ions is diverted toward the main axis of the radio-frequency ion guide while neutrals continue their flow along the central axis. The ions from the ion introduction system are transported via the radio-frequency ion guide to the mass analyzer.
摘要翻译：一种质谱仪系统，用于从离子中分离出离子并通过离子引入系统质量分析离子，其包括离子发生源，射频离子导向器和质量分析器，设置在真空室内。射频离子引导件相对于离子引入系统定位，使得射频离子导向器的主轴线朝向离子引入系统的中心轴线倾斜。离子的轨迹朝向射频离子导向器的主轴转移，而中性粒子沿中心轴继续流动。来自离子引入系统的离子通过射频离子导向器输送到质量分析器。

2. 发明授权

US5506412A Means for reducing the contamination of mass spectrometer leak detection ion sources 失效
标题翻译：减少质谱仪泄漏检测离子源污染的手段
公开(公告)号：US5506412A
公开(公告)日：1996-04-09
申请号：US357905
申请日：1994-12-16
申请人： Sidney E. Buttrill, Jr.
发明人： Sidney E. Buttrill, Jr.
IPC分类号： G01N27/62 , G01M3/00 , G01M3/02 , G01M3/20 , H01J49/10 , H01J49/14 , H01J49/26
CPC分类号： G01M3/202 , H01J49/14
摘要： In a mass spectrometer leak detector an ion source assembly is disposed in a cavity of a vacuum envelope and is surrounded by a thin removable liner which has means for positioning this liner within the cavity. The liner positioning means limit the thermal contact of the liner with the vacuum envelope and due to heat-radiation relationship of the liner with the ion source the temperature of the ion source region increases and contamination of the ion source decreases.
摘要翻译：在质谱仪泄漏检测器中，离子源组件设置在真空外壳的空腔中，并且被薄的可移除衬套围绕，该衬垫具有用于将该衬套定位在空腔内的装置。衬套定位装置限制了衬套与真空外壳的热接触，并且由于衬套与离子源的热辐射关系，离子源区域的温度升高并且离子源的污染减少。

3. 依法登记的发明

USH414H Surface ionization source 失效
标题翻译：表面电离源
公开(公告)号：USH414H
公开(公告)日：1988-01-05
申请号：US28168
申请日：1987-03-20
申请人： Steven E. Young , Sidney E. Buttrill, Jr.
发明人： Steven E. Young , Sidney E. Buttrill, Jr.
IPC分类号： H01J27/26
CPC分类号： H01J27/26
摘要： An ionization source comprises a housing defining a space, a wire extendingo the space, a temperature control connected to the wire and an alkali metal glass bead attached to the wire to be heated by the temperature control. An ion extraction plate with an orifice therein covers the space and is insulated from the housing by an insulating ring. The housing includes a port for drawing a vacuum from the space and for leaking molecules into the space which are to form quasi ions on the glass bead. A focusing plate may also be provided over the extraction plate with an aperture lying on an ion axis which also extends through the orifice for the focusing of the ion beam.

4. 发明授权

US5818041A Mass spectrometer system and method for transporting and analyzing ions 失效
标题翻译：离子质谱仪系统及其分析方法
公开(公告)号：US5818041A
公开(公告)日：1998-10-06
申请号：US854855
申请日：1997-05-12
申请人： Alexander Mordehai , Sidney E. Buttrill, Jr.
发明人： Alexander Mordehai , Sidney E. Buttrill, Jr.
IPC分类号： H01J49/04 , H01J49/42 , H01J49/00
CPC分类号： H01J49/0445 , H01J49/063
摘要： A mass spectrometer system for performing a separation of ions from neutrals and mass analyzing ions comprising a inductively coupled plasma ion generating source with an ion introducing system, a radio-frequently ion guide and a mass analyzer disposed within a vacuum chamber. The space between the radio-frequency ion guide and the ion introduction system defined an aerodynamic jet region which is used for directing a sample containing ions to be analyzed to the entrance of a radio-frequency ion guide and the via the radio-frequency ion guide to the mass analyzer.
摘要翻译：一种用于执行离子从中性离子和质量分析离子分离的质谱仪系统，其包括具有离子引入系统的电感耦合等离子体离子发生源，设置在真空室内的无线电频率离子导向器和质量分析器。射频离子导向器和离子引入系统之间的空间限定了空气动力学喷射区域，其用于将含有要分析的离子的样品引导到射频离子导向器的入口，并且通过射频离子导向器到质量分析仪。

5. 发明授权

US5569917A Apparatus for and method of forming a parallel ion beam 失效
标题翻译：用于形成平行离子束的装置和方法
公开(公告)号：US5569917A
公开(公告)日：1996-10-29
申请号：US446101
申请日：1995-05-19
申请人： Sidney E. Buttrill, Jr. , Alex V. Mordehai
发明人： Sidney E. Buttrill, Jr. , Alex V. Mordehai
IPC分类号： G01N27/62 , H01J49/10 , H01J49/34 , H01J49/40 , H01J49/42 , B01D59/44 , H01J49/00
CPC分类号： H01J49/424 , H01J49/40
摘要： A time-of-flight mass spectrometer includes an ion beam source having a quadrupole ion trap. To form a parallel ion beam, the ions are simultaneously sucked and pulsed out of an interaction region of the trap through an opening in a front end cap electrode of the trap by applying different polarity voltage pulses at the same time to the front end cap electrode and a back end cap electrode of the trap.
摘要翻译：飞行时间质谱仪包括具有四极离子阱的离子束源。为了形成平行的离子束，通过同时向前端盖电极施加不同极性的电压脉冲，同时将离子从陷阱的相互作用区域中通过陷阱的前端盖电极中的开口脉冲输出和陷阱的后端盖电极。

6. 发明授权

US06867414B2 Electric sector time-of-flight mass spectrometer with adjustable ion optical elements 失效
标题翻译：具有可调式离子光学元件的电扇飞行时间质谱仪
公开(公告)号：US06867414B2
公开(公告)日：2005-03-15
申请号：US10424351
申请日：2003-04-24
申请人： Sidney E. Buttrill, Jr.
发明人： Sidney E. Buttrill, Jr.
IPC分类号： H01J49/28 , H01J49/40
CPC分类号： H01J49/282 , H01J49/408
摘要： The invention provides apparatus and methods for performing time-of-flight (TOF) mass spectrometry. A TOF mass spectrometer of the present invention comprises one or more ion focusing electric sectors. At least one of the electric sectors is associated with an ion optical element. The ion optical elements comprise at least one adjustable electrode, such that the adjustable electrode is able to modify the potential experienced by an ion entering or exiting the electric sector with which it is associated.
摘要翻译：本发明提供了用于执行飞行时间（TOF）质谱的装置和方法。本发明的TOF质谱仪包括一个或多个离子聚焦电扇区。电扇区中的至少一个与离子光学元件相关联。离子光学元件包括至少一个可调电极，使得可调节电极能够改变进入或离开与其相关联的电扇区的离子所经历的电位。

7. 发明授权

US4733073A Method and apparatus for surface diagnostics 失效
标题翻译：表面诊断方法和装置
公开(公告)号：US4733073A
公开(公告)日：1988-03-22
申请号：US865580
申请日：1986-05-16
申请人： Christopher H. Becker , Keith T. Gillen , Sidney E. Buttrill, Jr.
发明人： Christopher H. Becker , Keith T. Gillen , Sidney E. Buttrill, Jr.
IPC分类号： H01L21/00 , H01J49/10
CPC分类号： H01L21/67253 , H01L21/67242
摘要： Method and apparatus for mass spectral analysis of unknown species of matter present on a surface even in extremely low concentrations. A probe beam such as an ion beam, electron beam or laser is directed to the surface under examination to remove a sample of material. An untuned, high-intensity laser is directed to a spatial region proximate to the surface. The laser has sufficient intensity to induce a high degree of nonresonant, and hence non-selective, photoionization of the sample of material within the laser beam. The non-selectively ionized sample is then subjected to mass spectral analysis to determine the nature of the unknown species.
摘要翻译：即使在极低浓度下，表面上存在的未知物质物质的质谱分析方法和装置。诸如离子束，电子束或激光器的探针束被引导到被检查的表面以去除材料样品。一个未经过训练的高强度激光被引导到靠近表面的空间区域。激光器具有足够的强度以诱导激光束内的材料样品的高度非共振，因此导致非选择性的光电离。然后对非选择性离子化样品进行质谱分析以确定未知物种的性质。

8. 发明授权

US4321467A Flow discharge ion source 失效
标题翻译：流量放电离子源
公开(公告)号：US4321467A
公开(公告)日：1982-03-23
申请号：US156511
申请日：1980-06-04
申请人： Sidney E. Buttrill, Jr.
发明人： Sidney E. Buttrill, Jr.
IPC分类号： B01D59/44
CPC分类号： B01D59/44
摘要： A flowing discharge ion source for supplying negative and positive ions to a mass spectrometer has an elongated, confined flow and discharge region through which flow the sample to be analyzed and a reagent gas and in which ionizing discharge electrodes are located. Inlet and outlet gas flow orifices are independently variable so that the reagent gas pressure in the discharge region and flow velocity therethrough are controlled. Controlling flow velocity provides one way for determining reagent and sample gas residence time, which is further controlled by making the position of the discharge electrodes adjustable along the length of the ionization region. A controllable heater is provided upstream of the discharge region to regulate reagent and sample gas temperature.
摘要翻译：用于向质谱仪提供负离子和正离子的流动放电离子源具有细长的限制流动和放电区域，待分析的样品和反应气体的流动，并且其中定位有电离放电电极。入口和出口气体流量孔是独立可变的，从而控制排放区域中的反应气体压力和流过其中的流速。控制流速提供了一种确定试剂和样品气体停留时间的方法，通过使放电电极的位置沿离子化区域的长度可调，进一步控制。在放电区域的上游设置可控加热器，以调节试剂和样品气体温度。

9. 发明授权

US06998606B2 Electric sector time-of-flight mass spectrometer with adjustable ion optical elements 失效
标题翻译：具有可调式离子光学元件的电扇飞行时间质谱仪
公开(公告)号：US06998606B2
公开(公告)日：2006-02-14
申请号：US10758326
申请日：2004-01-14
申请人： Sidney E. Buttrill, Jr.
发明人： Sidney E. Buttrill, Jr.
IPC分类号： H01J49/40
CPC分类号： H01J49/282 , H01J49/408
摘要： The invention provides apparatus and methods for performing time-of-flight (TOF) mass spectrometry. A TOF mass spectrometer of the present invention comprises one or more ion focusing electric sectors. At least one of the electric sectors is associated with an ion optical element. The ion optical elements comprise at least one adjustable electrode, such that the adjustable electrode is able to modify the potential experienced by an ion entering or exiting the electric sector with which it is associated.
摘要翻译：本发明提供了用于执行飞行时间（TOF）质谱的装置和方法。本发明的TOF质谱仪包括一个或多个离子聚焦电扇区。电扇区中的至少一个与离子光学元件相关联。离子光学元件包括至少一个可调电极，使得可调节电极能够改变进入或离开与其相关联的电扇区的离子所经历的电位。

10. 发明授权

US5793038A Method of operating an ion trap mass spectrometer 失效
标题翻译：操作离子阱质谱仪的方法
公开(公告)号：US5793038A
公开(公告)日：1998-08-11
申请号：US763964
申请日：1996-12-10
申请人： Sidney E. Buttrill, Jr.
发明人： Sidney E. Buttrill, Jr.
IPC分类号： H01J49/34 , H01J49/42 , B01D59/44 , H01J49/00
CPC分类号： H01J49/428
摘要： A method of operating a quadrupole ion trap as a mass spectrometer, in which the ion mass to be detected is selected by adjusting the three dimensional quadrupole storage field to make the .beta..sub.z value of the selected mass equal to a fixed, predetermined .beta..sub.z value of a narrow range of frequencies excluded from a broadband supplemental RF electric field. The ions are detected to provide a signal corresponding to the amount of the selected ion mass.
摘要翻译：操作四极离子阱作为质谱仪的方法，其中通过调节三维四极存储场来选择要检测的离子质量，以使选定质量的βz值等于固定的预定β值从宽带补充RF电场排除的窄频率范围。检测离子以提供对应于所选离子质量的量的信号。

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