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1. 发明授权

US6033783A Ultrafine Al particle and production method thereof 失效
标题翻译：超细Al颗粒及其制备方法
公开(公告)号：US6033783A
公开(公告)日：2000-03-07
申请号：US861821
申请日：1997-05-23
申请人： Shun-ichiro Tanaka , BingShe Xu
发明人： Shun-ichiro Tanaka , BingShe Xu
IPC分类号： B22F9/04 , B22F9/30 , C22C21/00 , C23C14/14 , C23C14/30 , C30B23/02 , B32B5/16
CPC分类号： C23C14/30 , B22F9/30 , C23C14/14 , C30B23/002 , C30B29/02 , B22F2999/00 , Y10T428/30
摘要： An ultrafine Al particle consists of an Al multiply twinned particle. The Al multiply twinned particle has a decahedron structure surrounded by {111} planes. The Al multiply twinned decahedral particle has a diameter of 10 to 30 nm. Such an ultrafine Al particle consisting of the Al multiply twinned decahedral particle is obtained as follows. A metastable Al oxide particle is placed on an amorphous carbon substrate having the reduction effect. Then the electron beam is irradiated to the metastable Al oxide particle placed on the amorphous carbon substrate in the vacuum atmosphere. From the metastable Al oxide particle, Al atoms or Al clusters are emitted and adsorbed to the substrate. By adjusting the electron beam intensity so that the ultrafine Al particle in the above procedure has a diameter from 10 to 30 nm, the Al multiply twinned particle having a decahedron is obtained.
摘要翻译：超细Al颗粒由Al多重孪晶颗粒组成。 Al多重孪晶颗粒具有被{111}平面包围的十面体结构。 Al多重双晶十面体粒子的直径为10〜30nm。由Al多重双晶十面体粒子组成的这种超细Al粒子如下获得。将亚稳态Al氧化物颗粒放置在具有还原效果的非晶碳衬底上。然后在真空气氛中将电子束照射到放置在非晶碳基板上的亚稳态Al氧化物颗粒。从亚稳态Al氧化物颗粒中，Al原子或Al簇被发射并吸附到衬底上。通过调整电子束强度，使上述方法中的超细Al粒子的直径为10〜30nm，得到具有十面体的Al倍增孪晶粒子。

2. 发明授权

US06440562B1 Tungsten super fine particle and method for producing the same 失效
标题翻译：钨超细颗粒及其制造方法
公开(公告)号：US06440562B1
公开(公告)日：2002-08-27
申请号：US09646831
申请日：2000-09-22
申请人： Yoshitaka Tamou , Shun-ichiro Tanaka , BingShe Xu
发明人： Yoshitaka Tamou , Shun-ichiro Tanaka , BingShe Xu
IPC分类号： B32B1502
CPC分类号： B82Y30/00 , B22F1/0018 , B22F9/30 , B22F2998/00 , B22F2999/00 , C23C14/22 , C23C14/30 , Y10T428/30 , B22F2202/11
摘要： A particle of W oxide 2 such as a particle of WO3 is disposed on an amorphous carbon support film 1, onto the particle of W oxide 2 in an atmosphere of high vacuum an electron beam of an intensity of 1023 to 1024 e/cm2·sec being irradiated. Due to the irradiation of an electron beam 3 of such an intensity, ultra fine particles of W 4 of a particle diameter of for instance 10 nm or less are generated. The ultra fine particles of W consist of W effected to detach from the particle of W oxide.
摘要翻译：将氧化物2的颗粒如WO3的颗粒在高真空气氛中在1023至1024e / cm2的强度的电子束上设置在无定形碳载体膜1上的W氧化物2的颗粒上。秒被照射。由于照射这样的强度的电子束3，产生粒径为10nm以下的W 4的超细颗粒。 W的超细颗粒由W形成以从W氧化物的颗粒分离。

3. 发明授权

US5945176A Graphite intercalation compound and production method thereof 失效
标题翻译：石墨插层化合物及其制备方法
公开(公告)号：US5945176A
公开(公告)日：1999-08-31
申请号：US41966
申请日：1998-03-13
申请人： BingShe Xu , Shun-ichiro Tanaka
发明人： BingShe Xu , Shun-ichiro Tanaka
IPC分类号： C01B31/00 , C01B31/02 , C01B31/04 , B05D3/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B31/0206 , C01B31/0415
摘要： An onion-like graphite 2 is produced by irradiating an electron beam to an amorphous carbon 3 under an active aluminum nanoparticle 1. By further irradiating the electron beam to the onion-like graphite 2 to intercalate aluminum atoms constituting the aluminum nanoparticle 1 in a space between (001) plane and (002) plane of the onion-like graphite 2 having a layer structure, an intercalation compound 4 is produced. Or, after the aluminum nanoparticles were driven and disposed on the onion-like graphite by electron beam, or the like, by irradiating the electron beam to intercalate aluminum atoms in the space between the (001) plane and the (002) plane of the onion-like graphite having a layer structure, the intercalation compound is produced.
摘要翻译：通过向活性铝纳米颗粒1下方的无定形碳3照射电子束来制造洋葱状石墨2.通过进一步向洋葱状石墨2照射电子束，将构成铝纳米粒子1的铝原子插入空间在具有层结构的洋葱状石墨2的（001）面和（002）面之间，形成插层化合物4。或者，在通过电子束等将铝纳米粒子驱动并配置在洋葱状石墨上之后，通过照射电子束将铝原子插入到（001）面和（002）面之间的空间中具有层结构的洋葱状石墨，生成插层化合物。

4. 发明授权

US06017630A Ultrafine particle and production method thereof, production method of ultrafine particle bonded body, and fullerene and production method thereof 失效
标题翻译：超细颗粒及其制造方法，超细颗粒粘结体的制造方法，富勒烯及其制造方法
公开(公告)号：US06017630A
公开(公告)日：2000-01-25
申请号：US861019
申请日：1997-05-21
申请人： Shun-ichiro Tanaka , BingShe Xu
发明人： Shun-ichiro Tanaka , BingShe Xu
IPC分类号： B01J19/08 , B01J19/12 , B22F1/00 , B22F9/02 , B22F9/06 , C01B31/02 , B32B5/16
CPC分类号： B82Y30/00 , B01J19/081 , B01J19/121 , B01J19/122 , B22F1/0018 , B22F9/02 , B22F9/06 , B82Y40/00 , C01B31/0206 , C01B31/0213 , B22F2999/00 , Y10T428/12493 , Y10T428/2982 , Y10T428/30
摘要： A target material having pores is disposed on a substrate. A high energy beam is irradiated to the inner walls of the pores of the target material in a slanting direction. Constituent atoms or molecules of the target material are detached from it to obtain a single or plurality of ultrafine particles separated as a unit substance. The superfine particles are formed at desired positions corresponding to the pores of the target material. Besides, by using an amorphous carbon substrate as the substrate, fullerenes such as an onion-like graphite are formed with the ultrafine particles as nucleation points. When the high energy beam is irradiated to at least two neighboring metal ultrafine particles, these metal ultrafine particles are bonded mutually. When the obtained metal ultrafine particle bonded body has a corresponding grain boundary, the high energy beam is further irradiated to lower value .SIGMA. of the corresponding grain boundary of the bonded interface. Besides, the metal ultrafine particle bonded body can also be made into a monocrystal grain or a polycrystal grain. Such a metal ultrafine particle bonded body is stable.
摘要翻译：具有孔的目标材料设置在基板上。高能量束以倾斜方向照射到目标材料的孔的内壁。将目标材料的成分原子或分子与其分离以获得作为单位物质分离的单个或多个超微粒子。超细颗粒形成在对应于目标材料的孔的所需位置。此外，通过使用无定形碳基板作为基板，以超细粒子为核心点形成诸如洋葱状石墨的富勒烯。当高能束照射到至少两个相邻的金属超细颗粒时，这些金属超细颗粒相互粘合。当所得到的金属超微粒子接合体具有相应的晶界时，将高能束进一步照射到键合界面的相应晶界的较低值SIGMA。此外，金属超微粒子接合体也可以制成单晶粒或多晶粒。这种金属超微粒粘结体是稳定的。

5. 发明授权

US5762898A Graphite intercalation compound 失效
标题翻译：石墨插层化合物
公开(公告)号：US5762898A
公开(公告)日：1998-06-09
申请号：US626457
申请日：1996-04-02
申请人： BingShe Xu , Shun-ichiro Tanaka
发明人： BingShe Xu , Shun-ichiro Tanaka
IPC分类号： C01B31/00 , C01B31/02 , C01B31/04 , B01D31/02 , B01D31/04 , B01D31/30
CPC分类号： B82Y30/00 , B82Y40/00 , C01B31/0206 , C01B31/0415
摘要： An onion-like graphite 2 is produced by irradiating an electron beam to an amorphous carbon 3 under an active aluminum nanoparticle 1. By further irradiating the electron beam to the onion-like graphite 2 to intercalate aluminum atoms constituting the aluminum nanoparticle 1 in a space between (001) plane and (002) plane of the onion-like graphite 2 having a layer structure, an intercalation compound 4 is produced. Or, after the aluminum nanoparticles were driven and disposed on the onion-like graphite by electron beam, or the like, by irradiating the electron beam to intercalate aluminum atoms in the space between the (001) plane and the (002) plane of the onion-like graphite having a layer structure, the intercalation compound is produced.
摘要翻译：通过向活性铝纳米颗粒1下方的无定形碳3照射电子束来制造洋葱状石墨2.通过进一步向洋葱状石墨2照射电子束，将构成铝纳米粒子1的铝原子插入空间在具有层结构的洋葱状石墨2的（001）面和（002）面之间，形成插层化合物4。或者，在通过电子束等将铝纳米粒子驱动并配置在洋葱状石墨上之后，通过照射电子束将铝原子插入到（001）面和（002）面之间的空间中具有层结构的洋葱状石墨，生成插层化合物。

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