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1. 发明授权

US07084295B2 Perfluoroadamantyl acrylate compound and intermediate therefor 失效
标题翻译：全氟金刚烷基丙烯酸酯化合物及其中间体
公开(公告)号：US07084295B2
公开(公告)日：2006-08-01
申请号：US10499305
申请日：2002-12-20
申请人： Shinji Tanaka , Toshihide Yoshitome , Kouichi Kodoi , Hidetoshi Ono , Naoyoshi Hatakeyama
发明人： Shinji Tanaka , Toshihide Yoshitome , Kouichi Kodoi , Hidetoshi Ono , Naoyoshi Hatakeyama
IPC分类号： C07C69/00
CPC分类号： C07C69/653 , C07C35/52 , C07C2603/74 , C08F297/04 , C08L33/04 , C08L33/06 , C08L33/08 , C08L53/02 , C08L53/025 , C08L2666/24 , C08L33/00 , C08L2666/04 , C08L2666/02
摘要： A perfluoroadamantyl acrylate compound which is highly useful as a raw material for functional resins,etc.;and an intermediate therefore. The perfluoroadamantyl acrylate compound comprises perfluoroadamantane having a CH2═C(R)COO group(wherein R is a hydrogen atom, a methyl group or a trifluoromethyl group) at the 1-position, at each of the 1- and 3-positions, at each of the 1-, 3- and 5-positions, at each of the 1-, 3-, 5- and 7-positions, or at the 2-position.
摘要翻译：作为功能性树脂的原料高度有用的丙烯酸全氟金刚烷酯化合物等;以及中间体。全氟金刚烷基丙烯酸酯化合物包括在1位上具有CH 2 -S（R）COO基团（其中R是氢原子，甲基或三氟甲基）的全氟金刚烷，在1-，3-，5-和7-位，或2-位中的每个位置，1-和3-位上的1-和3-位。

2. 发明申请

US20050131247A1 Perfluoroadamantly acrylate compound and intermediate therefor 失效
标题翻译：全氟多官能丙烯酸酯化合物及其中间体
公开(公告)号：US20050131247A1
公开(公告)日：2005-06-16
申请号：US10499305
申请日：2002-12-20
申请人： Shinji Tanaka , Toshihide Yoshitome , Kouichi Kodoi , Hidetoshi Ono , Naoyoshi Hatakeyama
发明人： Shinji Tanaka , Toshihide Yoshitome , Kouichi Kodoi , Hidetoshi Ono , Naoyoshi Hatakeyama
IPC分类号： C07C69/54 , C07C35/52 , C07C69/00 , C07C69/013 , C07C69/653 , C08F20/22 , C08F297/04 , C08L33/06 , C08L33/08 , C08L53/02 , C07C69/62 , C07C35/22 , C07C69/52
CPC分类号： C07C69/653 , C07C35/52 , C07C2603/74 , C08F297/04 , C08L33/04 , C08L33/06 , C08L33/08 , C08L53/02 , C08L53/025 , C08L2666/24 , C08L33/00 , C08L2666/04 , C08L2666/02
摘要： A perfluoroadamantyl acrylate compound which is highly useful as a raw material for functional resins,etc.;and an intermediate therefore. The perfluoroadamantyl acrylate compound comprises perfluoroadamantane having a CH2═C(R)COO group(wherein R is a hydrogen atom, a methyl group or a trifluoromethyl group) at the 1-position, at each of the 1- and 3-positions, at each of the 1-,3- and 5-positions, at each of the 1-,3-,5- and 7-positions, or at the 2-position.
摘要翻译：作为功能性树脂的原料高度有用的丙烯酸全氟金刚烷酯化合物等;以及中间体。全氟金刚烷基丙烯酸酯化合物包括在1位上具有CH 2 -C（R）COO基团（其中R是氢原子，甲基或三氟甲基）的全氟金刚烷，在1 - ，3 - ，5 - 和7 - 位，或2-位的每个位置上，在1 - ，3 - 和5 - 位的每个位置上有1 - 和3 - 位。

3. 发明授权

US06833388B2 Adamantane derivative 失效
标题翻译：金刚烷衍生物
公开(公告)号：US06833388B2
公开(公告)日：2004-12-21
申请号：US10480255
申请日：2003-12-17
申请人： Shinji Tanaka , Toshihide Yoshitome , Takashi Nakagawa , Kouichi Kodoi
发明人： Shinji Tanaka , Toshihide Yoshitome , Takashi Nakagawa , Kouichi Kodoi
IPC分类号： A61K31215
CPC分类号： C07C69/753 , C07C2603/74 , C08K5/12 , G03F7/0045 , G03F7/0392
摘要： There is provided a trisadamantane based compound which is useful not only as a photoresist additive but also as pharmaceuticals, an agrochemical intermediate, a resin additive (heat resistance improver) and the like, and which is represented by the general formula (I): wherein R1 and R2 are each an alkyl group having 1 to 8 carbon atoms; X1 and X2 are each hydrogen atom, a halogen atom, an alkyl group having 1 to 8 carbon atoms, hydroxyl group, an alkoxy group having 1 to 8 carbon atoms, carboxyl group or COOR3 in which R3 is an alkyl group having 1 to 8 carbon atoms.
摘要翻译：提供了三金刚烷类化合物，其不仅可用作光致抗蚀剂添加剂，而且可用作药物，农药中间体，树脂添加剂（耐热改进剂）等，并且由通式（I）表示：其中 R 1和R 2各自为具有1至8个碳原子的烷基; X 1和X 2各自为氢原子，卤素原子，具有1至8个碳原子的烷基，羟基，具有1至8个碳原子的烷氧基，羧基或COOR 3，其中 R 3是具有1至8个碳原子的烷基。

4. 发明授权

US07193106B2 Halogenoacetoxyadamantane derivatives and process for production thereof 有权
标题翻译：卤代乙酰氧基金刚烷衍生物及其制备方法
公开(公告)号：US07193106B2
公开(公告)日：2007-03-20
申请号：US10511600
申请日：2003-04-28
申请人： Kouichi Kodoi , Shinji Tanaka , Toshihide Yoshitome
发明人： Kouichi Kodoi , Shinji Tanaka , Toshihide Yoshitome
IPC分类号： C07C69/03
CPC分类号： C07C69/63 , C07C67/14 , C07C2603/74
摘要： Provided are a novel halogenoacetoxyadamantane derivative which is useful as a modifying agent for a resin for a photoresist and a dry etching resistance-improving agent in the photolithography field, agricultural and medical intermediates and a compound for other various industrial products and a process for producing the same. To be specific, provided are a halogenoacetoxyadamantane derivative having a halogenoacetoxy group in an adamantane skeleton and a process for producing a halogenoacetoxyadamantane derivative, comprising the step of reacting a hydroxyl group of an adamantane skeleton with halogenoacetic halide or reacting the above hydroxyl group with a lithiation agent to derive it into a lithiumoxy group and then reacting halogenoacetic halide to introduce a halogenoacetoxy group.
摘要翻译：提供了一种新的卤代乙酰氧基金刚烷衍生物，其可用作光刻胶树脂中的改性剂和光刻领域中的耐干蚀刻性改进剂，农业和医疗中间体以及其它各种工业产品的化合物和用于制备相同。具体而言，提供在金刚烷骨架中具有卤代乙酰氧基的卤代乙酰氧基金刚烷衍生物和卤代乙酰氧基金刚烷衍生物的制造方法，包括使金刚烷骨架的羟基与卤代乙酰卤反应或使上述羟基与锂化反应的步骤将其衍生为锂氧基，然后使卤代乙酰卤反应引入卤代乙酰氧基。

5. 发明申请

US20050258395A1 Halogenoacetoxyadamantane derivatives and process for production thereof 有权
标题翻译：卤代乙酰氧基金刚烷衍生物及其制备方法
公开(公告)号：US20050258395A1
公开(公告)日：2005-11-24
申请号：US10511600
申请日：2003-04-28
申请人： Kouichi Kodoi , Shinji Tanaka , Toshihide Yoshitome
发明人： Kouichi Kodoi , Shinji Tanaka , Toshihide Yoshitome
IPC分类号： C07C67/14 , C07C69/00 , C09K13/00
CPC分类号： C07C69/63 , C07C67/14 , C07C2603/74
摘要： Provided are a novel halogenoacetoxyadamantane derivative which is useful as a modifying agent for a resin for a photoresist and a dry etching resistance-improving agent in the photolithography field, agricultural and medical intermediates and a compound for other various industrial products and a process for producing the same. To be specific, provided are a halogenoacetoxyadamantane derivative having a halogenoacetoxy group in an adamantane skeleton and a process for producing a halogenoacetoxyadamantane derivative, comprising the step of reacting a hydroxyl group of an adamantane skeleton with halogenoacetic halide or reacting the above hydroxyl group with a lithiation agent to derive it into a lithiumoxy group and then reacting halogenoacetic halide to introduce a halogenoacetoxy group.
摘要翻译：提供了一种新的卤代乙酰氧基金刚烷衍生物，其可用作光刻胶树脂中的改性剂和光刻领域中的耐干蚀刻性改进剂，农业和医疗中间体以及其它各种工业产品的化合物和用于制备相同。具体而言，提供在金刚烷骨架中具有卤代乙酰氧基的卤代乙酰氧基金刚烷衍生物和卤代乙酰氧基金刚烷衍生物的制造方法，包括使金刚烷骨架的羟基与卤代乙酰卤反应或使上述羟基与锂化反应的步骤将其衍生为锂氧基，然后使卤代乙酰卤反应引入卤代乙酰氧基。

6. 发明授权

US06531635B1 Precursors of 3-alkoxyalkanols and processes for the preparation of 3-alkoxyalkanols 失效
标题翻译： 3-烷氧基烷醇的前体和3-烷氧基链烷醇的制备方法
公开(公告)号：US06531635B1
公开(公告)日：2003-03-11
申请号：US09926549
申请日：2001-11-19
申请人： Toshihide Yoshitome , Hiroshi Kawasaki , Naoya Kawano
发明人： Toshihide Yoshitome , Hiroshi Kawasaki , Naoya Kawano
IPC分类号： C07C4500
CPC分类号： C07C45/71 , C07C41/26 , C07C41/28 , C07C41/50 , C07C45/515 , C07C45/84 , C07C47/198 , C07C43/315 , C07C43/13
摘要： Processes for the preparation of 3-alkoxyalkanols useful as solvents for coating materials, photoresists, or the like. Specifically, (1) a process which comprises reacting an &agr;,&bgr;-unsaturated aldehyde with an alcohol in the presence of an acidic catalyst and subjecting the obtained product to hydrolysis and hydrogenation successively; (2) a process which comprises subjecting a reaction mixture obtained by the reaction of an &agr;,&bgr;-unsaturated aldehyde with an alcohol and comprising the corresponding 1,1,3-trialkoxyalkane and 3-alkoxyalkanal to hydrolysis and hydrogenation at the same time; (3) a process which comprises recovering a 3-alkoxyalkanal through distillation as an azeotropic mixture thereof with water from a reaction solution obtained by the reaction of an alcohol with acid-containing acrolein or methacrolein prepared by the oxidation of propylene or isobutylene, and hydrogenating the recovered 3-alkoxyalkanal into the corresponding 3-alkoxyalkanol; and (4) a process which comprises bringing a gas produced by the oxidation of propylene or isobutylene into contact with an alcohol, conducting the reaction of the gas with the alcohol to form the corresponding 1,1,3-trialkoxyalkane, and subjecting it to hydrolysis and hydrogenation.
摘要翻译：制备用作涂料，光致抗蚀剂等的溶剂的3-烷氧基烷醇的方法。具体地说，（1）一种方法，该方法包括在酸性催化剂存在下使α，β-不饱和醛与醇反应，并使得到的产物依次进行水解和氢化; （2）一种方法，其包括使α，β-不饱和醛与醇反应得到的反应混合物与包含相应的1,1,3-三烷氧基烷烃和3-烷氧基烷烃的物质同时进行水解和氢化; （3）一种方法，其包括通过蒸馏作为其与水的共沸混合物从由与丙烯或异丁烯氧化制备的含酸丙烯醛或异丁烯醛反应得到的反应溶液中回收3-烷氧基亚油酸，以及氢化将回收的3-烷氧基亚烷醛转化为相应的3-烷氧基烷醇; 和（4）包括使由丙烯或异丁烯的氧化产生的气体与醇接触的方法，使气体与醇反应形成相应的1,1,3-三烷氧基烷烃，并使其水解和氢化。

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