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1. 发明授权

US4839458A Preparation with controlled amounts of polycarbonate carbon tetrachloride 失效
标题翻译：用可控量的聚碳酸酯四氯化碳制备
公开(公告)号：US4839458A
公开(公告)日：1989-06-13
申请号：US63001
申请日：1987-06-17
申请人： Shinichiro Koga , Akira Matsuno , Katsuyuki Sakata , Yoshiaki Ohtani , Isao Akihara
发明人： Shinichiro Koga , Akira Matsuno , Katsuyuki Sakata , Yoshiaki Ohtani , Isao Akihara
IPC分类号： C08G64/24 , C08G64/40
CPC分类号： C08G64/24 , C08G64/406
摘要： Disclosed herein is a process for producing a resin having carbonate bonding, comprising polymerizing a hydroxydiaryl compound and phosgene in an organic solvent of methylene chloride such that the concentration of carbon tetrachloride in phosgene and methylene chloride in the polymerization system satisfies the following equation:A+5B.ltoreq.200(wherein A represents carbon tetrachloride concentration (ppm) in phosgene and B represents carbon tetrachloride concentration (ppm) in methylene chloride).
摘要翻译：本发明公开了一种生产具有碳酸酯键合的树脂的方法，包括在二氯甲烷的有机溶剂中使羟基二芳基化合物和光气聚合，使得聚合体系中光气和二氯甲烷中的四氯化碳的浓度满足下列等式：A + 5B（其中A表示碳酰氯中的四氯化碳浓度（ppm），B表示二氯甲烷中的四氯化碳浓度（ppm））。

2. 发明授权

US4661555A Polycarbonate resin composition and process for its production 失效
标题翻译：聚碳酸酯树脂组合物及其生产方法
公开(公告)号：US4661555A
公开(公告)日：1987-04-28
申请号：US802448
申请日：1985-11-27
申请人： Shinichiro Koga , Katsuhisa Kohyama , Katsuyuki Sakata
发明人： Shinichiro Koga , Katsuhisa Kohyama , Katsuyuki Sakata
IPC分类号： C08G64/40 , C08K3/04 , C08K7/06 , C08L69/00
CPC分类号： C08K3/04 , C08G64/40 , C08K7/06
摘要： A particulate polycarbonate resin composition which is separated from a solution of an inorganic filler-containing polycarbonate in an organic solvent at a temperature lower than the melting point of the polycarbonate, and contains an inorganic filler, said composition having a particle size distribution n of from 3 to 8 as represented by the following Rosin-Rammler distribution equationR=100 exp (-b Dp.sup.n)where R is an on-sieve amount (% by weight), Dp is a particle diameter (mm), and b is a constant, the particle diameter of the 50% on-sieve weight integration being from 0.5 to 6 mm, and the bulk density being from 0.1 to 0.7 g/ml.
摘要翻译：一种颗粒状聚碳酸酯树脂组合物，其在低于聚碳酸酯的熔点的温度下从有机溶剂中的含无机填料的聚碳酸酯的溶液中分离，并且含有无机填料，所述组合物的粒度分布n为 3〜8，由以下Rosin-Rammler分布方程式表示：R = 100exp（-b Dpn）其中，R为筛分量（重量％），Dp为粒径（mm），b为常数，50％筛子重量积分的粒径为0.5至6mm，堆积密度为0.1至0.7g / ml。

3. 发明授权

US4369303A Process for producing an aromatic polyesterpolycarbonate 失效
标题翻译：芳香族聚酯聚碳酸酯的制造方法
公开(公告)号：US4369303A
公开(公告)日：1983-01-18
申请号：US200596
申请日：1980-10-24
申请人： Hazime Mori , Katsuhisa Kohyama , Katsuhiko Nakamura , Katsuyuki Sakata , Akira Matsuno
发明人： Hazime Mori , Katsuhisa Kohyama , Katsuhiko Nakamura , Katsuyuki Sakata , Akira Matsuno
IPC分类号： C08G63/00 , C08G63/64
CPC分类号： C08G63/64
摘要： A process for producing an aromatic polyesterpolycarbonate, which comprises polycondensing (a) a dihydroxydiaryl compound, (b) a terephthaloyl chloride and/or isophthaloyl chloride reactant, and (c) phosgene by an interfacial polymerization process in the presence of water, methylene chloride and an acid binding agent thereby preparing an aromatic polyesterpolycarbonate product containing structural units of the formula: ##STR1## wherein X is a divalent group, and the aromatic rings may be substituted, and structural units of the formula: ##STR2## wherein X is a divalent group, and the aromatic rings may be substituted, said condensation reaction being characterized in that after at least 95% of the total --COCl groups in the terephthaloyl chloride and/or isophthaloyl chloride and phosgene starting materials has reacted, a chloroformate compound or additional phosgene is added to the reaction mixture in an amount to bring the concentration of --COCl groups to a level of 10 to 1000 .mu.eq/g relative to the total amount of the above starting materials to complete the reaction.
摘要翻译：一种制备芳族聚酯聚碳酸酯的方法，其包括缩聚（a）二羟基二芳基化合物，（b）对苯二甲酰氯和/或间苯二甲酰氯反应物，和（c）通过界面聚合方法在水，二氯甲烷和由此制备含有下式结构单元的芳族聚酯聚碳酸酯产物：其中X是二价基团，芳环可以被取代，并具有下式的结构单元：（II））其中X是二价基团，芳环可以被取代，所述缩合反应的特征在于在对苯二酰氯和/或间苯二酰氯和光气原料中的至少95％的-COCl基团已经反应后，将氯甲酸酯化合物或另外的光气加入到反应混合物中，其量使得-COCl基团的浓度达到10至1000的水平相对于上述起始原料的总量，相对于完成反应来说，μeq / g。

4. 发明授权

US4429103A Method for preparation of aromatic polyester-polycarbonate 失效
标题翻译：芳香族聚酯 - 聚碳酸酯的制备方法
公开(公告)号：US4429103A
公开(公告)日：1984-01-31
申请号：US360000
申请日：1982-03-19
申请人： Katsuhisa Kohyama , Katsuyuki Sakata , Shinji Ono
发明人： Katsuhisa Kohyama , Katsuyuki Sakata , Shinji Ono
IPC分类号： C08G63/00 , C08G63/64 , C08G64/22
CPC分类号： C08G63/64
摘要： An aromatic polyesterpolycarbonate containing a dihydroxy-diaryl compound residue, a terephthalic acid residue and/or isophthalic acid residue, and a carbonate bond in a molar ratio of 1:0.25-0.75:0.75-0.25 is prepared by first mixing and reacting an aqueous alkaline solution of a dihydroxy-diaryl compound, an organic solvent solution of terephthaloyl chloride and/or isophthaloyl chloride, and phosgene to obtain a polyesterpolycarbonate oligomer having --OCOCl groups, --COCl groups and --OH groups as end groups and then subjecting the oligomer to polycondensation with a caustic alkali in the substantial absence of the dihydroxy-diaryl compound.
摘要翻译：含有二羟基 - 二芳基化合物残基，对苯二甲酸残基和/或间苯二甲酸残基的芳族聚酯聚碳酸酯和摩尔比为1:0.25-0.75:0.75-0.25的碳酸酯键通过首先将碱性水溶液二羟基 - 二芳基化合物的溶液，对苯二甲酰氯和/或间苯二甲酰氯的有机溶剂溶液和光气，得到具有-OCOCl基团，-COCl基和-OH基团的聚酯聚碳酸酯低聚物作为端基，然后使低聚物缩聚其中基本上不存在二羟基 - 二芳基化合物的苛性碱。

5. 发明授权

US4260731A Aromatic polyester-polycarbonate 失效
标题翻译：芳香聚酯 - 聚碳酸酯
公开(公告)号：US4260731A
公开(公告)日：1981-04-07
申请号：US68067
申请日：1979-08-20
申请人： Hajime Mori , Katsuhisa Kohyama , Katsuhiko Nakamura , Katsuyuki Sakata
发明人： Hajime Mori , Katsuhisa Kohyama , Katsuhiko Nakamura , Katsuyuki Sakata
IPC分类号： C08G63/64 , C08G63/66
CPC分类号： C08G63/64 , C08G63/66
摘要： An aromatic polyester-polycarbonate resin which comprises a polymer material composed of repeating units of structures I-III: ##STR1## wherein X is a divalent organic radical and the divalent aromatic entities in structures I, II and III may be substituted by hydrocarbon residues.
摘要翻译：一种芳族聚酯 - 聚碳酸酯树脂，其包含由结构I-III的重复单元组成的聚合物材料：其中X是二价有机基团，并且结构I，II中的二价芳族物质和III可以被烃残基取代。

6. 发明授权

US4252939A Method for manufacture of aromatic polyester-polycarbonate 失效
标题翻译：芳香族聚酯 - 聚碳酸酯的制造方法
公开(公告)号：US4252939A
公开(公告)日：1981-02-24
申请号：US47796
申请日：1979-06-12
申请人： Hajime Mori , Katsuhisa Kohyama , Katsuhiko Nakamura , Katsuyuki Sakata
发明人： Hajime Mori , Katsuhisa Kohyama , Katsuhiko Nakamura , Katsuyuki Sakata
IPC分类号： C08G63/00 , C08G63/64 , C08G63/688 , C08G64/06
CPC分类号： C08G64/06 , C08G63/64 , C08G63/688
摘要： An aromatic polyester-polycarbonate is prepared by(a) forming a low molecular weight polyester oligomer possessing terminal -OH groups by reacting a solution of a terephthaloyl chloride compound in an organic solvent with a dihydroxy-diaryl compound in an aqueous alkaline solution;(b) reacting said oligomer with phosgene thereby converting said terminal -OH groups to terminal -OCOCl groups; and(c) preparing the desired aromatic polyester-polycarbonate product by polycondensing the product of step (b) with a dihydroxy-diaryl compound in an aqueous alkaline solution.
摘要翻译：通过以下方法制备芳族聚酯 - 聚碳酸酯：（a）通过使碱性溶液中的对苯二甲酰氯化合物在有机溶剂中的溶液与二羟基 - 二芳基化合物反应形成具有末端-OH基团的低分子量聚酯低聚物; （b）使所述低聚物与光气反应，从而将所述末端-OH基团转化为末端-OCOCl基团; 和（c）通过将步骤（b）的产物与二羟基 - 二芳基化合物在碱性水溶液中缩聚来制备所需的芳族聚酯 - 聚碳酸酯产物。

7. 发明授权

US4239882A Process for producing polyester 失效
标题翻译：生产聚酯的方法
公开(公告)号：US4239882A
公开(公告)日：1980-12-16
申请号：US609964
申请日：1975-09-03
申请人： Tsuneo Kimura , Katsuhisa Kohyama , Takehiro Okada , Katsuyuki Sakata
发明人： Tsuneo Kimura , Katsuhisa Kohyama , Takehiro Okada , Katsuyuki Sakata
IPC分类号： C08G63/00 , C08G63/78 , C08G17/013
CPC分类号： C08G63/78 , Y02P20/582
摘要： A polyester is produced in an improved process by esterification or interesterification of an aromatic dicarboxylic acid or an alkyl ester thereof with 1,4-butanediol followed by polycondensation of the resulting ester characterized in reusing the 1,4-dibutanediol mixture distilled in the polycondensation step without purification as a starting material for production of more polyester.
摘要翻译：通过芳族二羧酸或其烷基酯与1,4-丁二醇的酯化或酯交换，然后通过所得酯的缩聚反应生产聚酯，其特征在于重复使用在缩聚步骤中蒸馏的1,4-二丁二醇混合物没有纯化作为生产更多聚酯的起始原料。

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