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1. 发明授权

US07547803B2 Process for producing a high purity aromatic polycarboxylic acid 有权
标题翻译：高纯度芳族多元羧酸的制备方法
公开(公告)号：US07547803B2
公开(公告)日：2009-06-16
申请号：US10861497
申请日：2004-06-07
申请人： Shinichi Nagao , Masato Inari , Jitsuo Oishi , Kenji Nakaya , Hiroshi Machida
发明人： Shinichi Nagao , Masato Inari , Jitsuo Oishi , Kenji Nakaya , Hiroshi Machida
IPC分类号： C07C51/42
CPC分类号： C07C51/43 , C07C51/487 , C07C63/333 , C07C63/38
摘要： A process for producing a high purity aromatic polycarboxylic acid (APA) by purification of a crude APA comprises: (I) aging a slurry of the crude APA in a first dispersion medium at 180 to 300° C. for 10 minutes or longer under stirring; (II) introducing the aged slurry of the APA into a column for substituting dispersion media, bringing the slurry into contact with a second dispersion medium and separating the resultant fluid into a fluid of the first dispersion medium containing impurities and a slurry of the second dispersion medium containing crystals of the high purity APA; and (III) separating the crystals of the high purity APA from the slurry of the second dispersion medium. A high purity APA having excellent hue and particle diameter can be industrially advantageously produced while the construction of the process is simplified and the consumption of energy is decreased.
摘要翻译：通过粗制APA的纯化生产高纯度芳族多元羧酸（APA）的方法包括：（I）在搅拌下将第一分散介质中粗APA的浆料在180-300℃下老化10分钟或更长时间 ; （II）将APA的老化浆液引入用于代替分散介质的塔中，使浆料与第二分散介质接触，并将所得流体分离成含有杂质的第一分散介质的流体和第二分散体的浆料含有高纯度APA晶体的介质; 和（III）将高纯度APA的晶体与第二分散介质的浆料分离。具有优异的色相和粒径的高纯度APA可以在工业上有利地产生，同时简化了工艺的构造并降低了能量的消耗。

2. 发明授权

US06642412B2 Process for producing a high purity aromatic polycarboxylic acid 有权
标题翻译：高纯度芳族多元羧酸的制备方法
公开(公告)号：US06642412B2
公开(公告)日：2003-11-04
申请号：US10215773
申请日：2002-08-12
申请人： Ryusuke Shigematsu , Masayoshi Hayashi , Shinichi Nagao , Jitsuo Oishi , Akio Hashimoto
发明人： Ryusuke Shigematsu , Masayoshi Hayashi , Shinichi Nagao , Jitsuo Oishi , Akio Hashimoto
IPC分类号： C07C5142
CPC分类号： C07C51/44 , C07C51/43 , C07C51/487 , C07C63/333 , C07C63/38
摘要： A process for producing a high purity aromatic polycarboxylic acid by purifying a crude aromatic polycarboxylic acid in accordance with the steps of (I) forming an amine salt of an aromatic polycarboxylic acid from the crude polycarboxylic acid and an amine, (II) continuously decomposing the salt in a salt decomposition reactor in operations of (i) supplying an aqueous solution of the amine salt of an organic polycarboxylic acid formed in the step of forming a salt, (ii) removing the amine and water by distillation under heating and (iii) taking out a slurry containing crystallized aromatic polycarboxylic acid, and (III) separating and recovering crystals of the aromatic polycarboxylic acid from the slurry which is taken out in the step of decomposing the salt. A high purity aromatic polycarboxylic acid having excellent hue and large particle diameters can be produced from a crude aromatic polycarboxylic acid industrially with stability at a low cost of production in accordance with a process having a simple construction.
摘要翻译：通过根据（I）从粗多羧酸和胺形成芳族多元羧酸的胺盐的步骤，通过纯化粗芳族多元羧酸来制备高纯度芳族多元羧酸的方法，（II）连续分解在（i）提供在形成盐的步骤中形成的有机多元羧酸的胺盐的水溶液的操作中的盐分解反应器中的盐，（ii）在加热下通过蒸馏除去胺和水，以及（iii）取出含有结晶的芳族多元羧酸的浆料，（III）从分解盐的步骤中取出的浆料中分离回收芳族多元羧酸的结晶。一种具有优异色调和大颗粒的高纯度芳族多元羧酸直径可以由工业上粗芳香族多元羧酸以与生产成本相当低的稳定性生产具有简单的结构。

3. 发明授权

US06455731B2 Process for producing a high purity aromatic polycarboxylic acid 有权
标题翻译：高纯度芳族多元羧酸的制备方法
公开(公告)号：US06455731B2
公开(公告)日：2002-09-24
申请号：US09858487
申请日：2001-05-17
申请人： Ryusuke Shigematsu , Masayoshi Hayashi , Shinichi Nagao , Jitsuo Oishi , Akio Hashimoto
发明人： Ryusuke Shigematsu , Masayoshi Hayashi , Shinichi Nagao , Jitsuo Oishi , Akio Hashimoto
IPC分类号： C07C5142
CPC分类号： C07C51/44 , C07C51/43 , C07C51/487 , C07C63/333 , C07C63/38
摘要： A process for producing a high purity aromatic polycarboxylic acid by purify a crude aromatic polycarboxylic acid in accordance with the steps of (I) forming an amine salt of an aromatic polycarboxylic acid from the crude polycarboxylic acid and an amine, (II) continuously decomposing the salt in a salt decomposition reactor in operations of (i) supplying an aqueous solution of the amine salt of an organic polycarboxylic acid formed in the step of forming a salt, (ii) removing the amine and water by distillation under heating and (iii) taking out a slurry containing crystallized aromatic polycarboxylic acid, and (III) separating and recovering crystals of the aromatic polycarboxylic acid from the slurry which is taken out in the step of decomposing the salt. A high purity aromatic polycarboxylic acid having excellent hue and large particle diameters can be produced from a crude aromatic polycarboxylic acid industrially with stability at a low cost of production in accordance with a process having a simple construction.
摘要翻译：通过根据（I）从粗多羧酸和胺形成芳族多元羧酸的胺盐的步骤纯化粗芳族多元羧酸来制备高纯度芳族多元羧酸的方法，（II）连续分解在（i）提供在形成盐的步骤中形成的有机多元羧酸的胺盐的水溶液的操作中的盐分解反应器中的盐，（ii）在加热下通过蒸馏除去胺和水，以及（iii）取出含有结晶芳香族多元羧酸的浆料，（III）从分解盐的工序中取出的浆料中分离回收芳族多元羧酸的结晶。具有优异的色相和大粒径的高纯度芳族多元羧酸可以根据具有简单结构的方法在工业上以粗制芳族多元羧酸以低成本生产的稳定性产生。

4. 发明授权

US08759588B2 Process for producing xylylenediamine 有权
标题翻译：生产苯二甲胺的方法
公开(公告)号：US08759588B2
公开(公告)日：2014-06-24
申请号：US13062334
申请日：2009-08-27
申请人： Shinichi Nagao , Tatsuyuki Kumano , Kenji Nakaya , Ryusuke Shigematsu , Kinji Kato
发明人： Shinichi Nagao , Tatsuyuki Kumano , Kenji Nakaya , Ryusuke Shigematsu , Kinji Kato
IPC分类号： C07C209/00
CPC分类号： C07C209/48 , C07C211/27
摘要： The invention provides a process for producing xylylenediamine, including supplying a solution of phthalonitrile dissolved in a solvent to a reactor filled with a catalyst and hydrogenating the phthalonitrile to produce xylylenediamine, characterized in that the process includes halting supply of the solution; (2) bringing a washing liquid into contact with the catalyst, the washing liquid having a phthalonitrile content of 3 mass % or less and a xylylenediamine content of 1 mass % or more; and after completion of the contact, resuming supply of the solution, and employing the catalyst continuously in hydrogenation. Through the production process of the invention, the catalyst can be employed continuously for a long period of time, and the catalyst-related cost can be considerably reduced.
摘要翻译：本发明提供了一种生产苯二甲胺的方法，包括将溶于溶剂中的邻苯二甲腈溶液供应到填充有催化剂的反应器中，并使邻苯二甲腈氢化以产生苯二甲胺，其特征在于该方法包括停止溶液的供应; （2）使洗涤液与催化剂接触，洗涤液的邻苯二腈含量为3质量％以下，苯二甲胺含量为1质量％以上; 接触完成后，恢复溶液的供应，并在催化剂中连续使用催化剂。通过本发明的制造方法，能够长时间连续使用催化剂，能够显着降低催化剂成本。

5. 发明申请

US20110245540A1 PROCESS FOR PRODUCING XYLYLENEDIAMINE 有权
标题翻译：生产XYLYLEDEDIAMINE的方法
公开(公告)号：US20110245540A1
公开(公告)日：2011-10-06
申请号：US13062334
申请日：2009-08-27
申请人： Shinichi Nagao , Tatsuyuki Kumano , Kenji Nakaya , Ryusuke Shigematsu , Kinji Kato
发明人： Shinichi Nagao , Tatsuyuki Kumano , Kenji Nakaya , Ryusuke Shigematsu , Kinji Kato
IPC分类号： C07C209/48
CPC分类号： C07C209/48 , C07C211/27
摘要： The invention provides a process for producing xylylenediamine, including supplying a solution of phthalonitrile dissolved in a solvent to a reactor filled with a catalyst and hydrogenating the phthalonitrile to produce xylylenediamine, characterized in that the process includes halting supply of the solution; (2) bringing a washing liquid into contact with the catalyst, the washing liquid having a phthalonitrile content of 3 mass % or less and a xylylenediamine content of 1 mass % or more; and after completion of the contact, resuming supply of the solution, and employing the catalyst continuously in hydrogenation. Through the production process of the invention, the catalyst can be employed continuously for a long period of time, and the catalyst-related cost can be considerably reduced.
摘要翻译：本发明提供了一种生产苯二甲胺的方法，包括将溶于溶剂中的邻苯二甲腈溶液供应到填充有催化剂的反应器中，并使邻苯二甲腈氢化以产生苯二甲胺，其特征在于该方法包括停止溶液的供应; （2）使洗涤液与催化剂接触，洗涤液的邻苯二腈含量为3质量％以下，苯二甲胺含量为1质量％以上; 接触完成后，恢复溶液的供应，并在催化剂中连续使用催化剂。通过本发明的制造方法，能够长时间连续使用催化剂，能够显着降低催化剂成本。

6. 发明授权

US08212080B2 Production method of xylylenediamine 有权
标题翻译：苯二甲胺的生产方法
公开(公告)号：US08212080B2
公开(公告)日：2012-07-03
申请号：US12633223
申请日：2009-12-08
申请人： Tatsuyuki Kumano , Kenji Nakaya , Shinichi Nagao
发明人： Tatsuyuki Kumano , Kenji Nakaya , Shinichi Nagao
IPC分类号： C07C209/00 , C07C211/00
CPC分类号： C07C211/27 , C07C209/48
摘要： A method of producing xylylenediamine by the hydrogenation of dicyanobenzene obtained by the ammoxidation of xylene in a high yield while prolonging the catalyst life. In the method, a molten dicyanobenzene from which compounds having a boiling point lower than that of dicyanobenzene have been removed but compounds having a boiling point higher than that of dicyanobenzene are not removed is dissolved in a solvent containing liquid ammonia. By this dissolution, at least part of dicyanobenzene polymers precipitates as insolubles. The precipitates are removed by a solid-liquid separation. By subjecting the resulting solution containing the dicyanobenzene polymers in a reduced amount to hydrogenation, xylylenediamine is produced in a high yield and the life time of hydrogenation catalyst is prolonged.
摘要翻译：通过二甲苯氨氧化得到的二氰基苯加氢制备苯二甲胺的方法，同时延长了催化剂的使用寿命。在该方法中，除去沸点低于二氰基苯的化合物的熔融二氰基苯，但没有除去沸点高于二氰基苯的沸点的化合物溶解在含有液氨的溶剂中。通过这种溶解，至少部分二氰基苯聚合物作为不溶物沉淀。通过固液分离除去沉淀物。通过将含有二氰基苯聚合物的所得溶液以减少的量进行氢化，以高产率生产苯二甲胺，延长氢化催化剂的使用寿命。

7. 发明申请

US20100168474A1 PRODUCTION METHOD OF XYLYLENEDIAMINE 有权
标题翻译： XYLYLENEDIAMINE的生产方法
公开(公告)号：US20100168474A1
公开(公告)日：2010-07-01
申请号：US12633223
申请日：2009-12-08
申请人： Tatsuyuki KUMANO , Kenji Nakaya , Shinichi Nagao
发明人： Tatsuyuki KUMANO , Kenji Nakaya , Shinichi Nagao
IPC分类号： C07C211/43
CPC分类号： C07C211/27 , C07C209/48
摘要： A method of producing xylylenediamine by the hydrogenation of dicyanobenzene obtained by the ammoxidation of xylene in a high yield while prolonging the catalyst life. In the method, a molten dicyanobenzene from which compounds having a boiling point lower than that of dicyanobenzene have been removed but compounds having a boiling point higher than that of dicyanobenzene are not removed is dissolved in a solvent containing liquid ammonia. By this dissolution, at least part of dicyanobenzene polymers precipitates as insolubles. The precipitates are removed by a solid-liquid separation. By subjecting the resulting solution containing the dicyanobenzene polymers in a reduced amount to hydrogenation, xylylenediamine is produced in a high yield and the life time of hydrogenation catalyst is prolonged.
摘要翻译：通过二甲苯氨氧化得到的二氰基苯加氢制备苯二甲胺的方法，同时延长了催化剂的使用寿命。在该方法中，除去沸点低于二氰基苯的化合物的熔融二氰基苯，但没有除去沸点高于二氰基苯的沸点的化合物溶解在含有液氨的溶剂中。通过这种溶解，至少部分二氰基苯聚合物作为不溶物沉淀。通过固液分离除去沉淀物。通过将含有二氰基苯聚合物的所得溶液以减少的量进行氢化，以高产率生产苯二甲胺，延长氢化催化剂的使用寿命。

8. 发明授权

US08730292B2 Scanning optical device that scans photoreceptor with laser light and image forming apparatus 有权
标题翻译：用激光扫描感光体的扫描光学装置和成像装置
公开(公告)号：US08730292B2
公开(公告)日：2014-05-20
申请号：US13478248
申请日：2012-05-23
申请人： Ryo Hasegawa , Shinji Morita , Yuji Okugawa , Shinichi Nagao
发明人： Ryo Hasegawa , Shinji Morita , Yuji Okugawa , Shinichi Nagao
IPC分类号： B41J15/14 , B41J27/00
CPC分类号： G03G15/04072 , G02B26/125 , G03G15/0409
摘要： A scanning optical device that scans a photoreceptor with laser light includes a light source, a light outputting section, and a projection. The laser light from the light source is output through the light outputting section so that the photoreceptor is irradiated with the laser light. The projection projects through a partition wall toward the photoreceptor. The light outputting section is disposed in a position separated from the photoreceptor by the partition wall. The projection contains a polygon motor that rotates a polygon mirror to reflect the laser light.
摘要翻译：用激光扫描感光体的扫描光学装置包括光源，光输出部和投影。来自光源的激光通过光输出部分输出，使得感光体被激光照射。突起通过分隔壁朝向感光体突出。光输出部分设置在与感光体通过分隔壁分离的位置。该投影包含多面镜马达，其旋转多面镜以反射激光。

9. 发明授权

US08359413B2 Data stream buffer control using reference time and decoding time 有权
标题翻译：数据流缓存控制使用参考时间和解码时间
公开(公告)号：US08359413B2
公开(公告)日：2013-01-22
申请号：US12706126
申请日：2010-02-16
申请人： Shinichi Nagao , Takahiro Hosoi , Nobutoshi Shida
发明人： Shinichi Nagao , Takahiro Hosoi , Nobutoshi Shida
IPC分类号： G06F3/00 , G06F15/16
CPC分类号： H04N21/44004 , H04N19/61 , H04N21/4302 , H04N21/4392
摘要： A buffer control device includes a reference time generation unit configured to generate a reference time based on time information included in a data stream input, a buffer configured to receive an encoded data extracted from the data stream, store the encoded data, and output the encoded data at a decoding time or a reproducing time of the encoded data, and a control unit configured to control an input of the encoded data to the buffer based on a relativity between the decoding time or the reproducing time of the encoded data and the reference time.
摘要翻译：一种缓冲器控制装置，包括：基准时间生成部，其基于包含在数据流输入中的时间信息生成基准时刻;缓冲器，被配置为接收从数据流提取的编码数据，存储编码数据，并输出编码数据数据在编码数据的解码时刻或再现时间，以及控制单元，被配置为基于编码数据的解码时间或再现时间与参考时间之间的相对性来控制对缓冲器的编码数据的输入。

10. 发明授权

US08124825B2 Method of purifying 2,7-dimethylnaphthalene 失效
标题翻译：纯化2,7-二甲基萘的方法
公开(公告)号：US08124825B2
公开(公告)日：2012-02-28
申请号：US11910774
申请日：2006-04-06
申请人： Shinichi Nagao , Hiroshi Ogawa
发明人： Shinichi Nagao , Hiroshi Ogawa
IPC分类号： C07C7/12
CPC分类号： C07C5/41 , C07C2/66 , C07C5/2737 , C07C7/13 , C07C15/24 , C07C2521/06 , C07C2523/04 , C07C2529/18 , C07C15/44
摘要： To provide a method of purifying 2,7-dimethylnaphthalene comprising the step of bringing a raw oil containing a mixture of 1,7-dimethylnaphthalene and 2,7-dimethylnaphthalene together with a developing solvent into contact with L-type zeolite to thereby effect adsorption of 1,7-dimethylnaphthalene.
摘要翻译：提供一种纯化2,7-二甲基萘的方法，其包括将含有1,7-二甲基萘和2,7-二甲基萘的混合物的原油与显影溶剂一起与L型沸石接触以进行吸附的步骤的1,7-二甲基萘。

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