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    • 1. 发明授权
    • Process for making a high density detergent composition from a sufactant
paste containing a non-aqueous binder
    • 从含有非水性粘合剂的表面活性剂糊料制造高密度洗涤剂组合物的方法
    • US5733862A
    • 1998-03-31
    • US819840
    • 1997-03-17
    • Scott William CapeciDavid Robert Nassano
    • Scott William CapeciDavid Robert Nassano
    • C11D3/10C11D3/12C11D3/37C11D11/00C11D17/06
    • C11D11/0082C11D17/065C11D3/10C11D3/1233C11D3/3707
    • A process for preparing high density detergent agglomerates having a density of at least 650 g/l is provided. The process comprises the steps of: (a) continuously mixing a detergent surfactant paste and dry starting detergent material into a high speed mixer/densifier to obtain detergent agglomerates, wherein said surfactant paste includes, by weight of said surfactant paste, from about 0.1% to about 50% of a non-aqueous binder, from about 70% to about 95% of a detersive surfactant, and the balance water; (b) mixing the detergent agglomerates in a moderate speed mixer/densifier to further density and agglomerate the detergent agglomerates; and (c) drying said detergent agglomerates so as to form the high density detergent composition. The process may include one or more additional processing steps such as adding a coating agent after the moderate speed mixer/densifier to facilitate and control agglomeration.
    • 提供了一种制备密度至少为650g / l的高密度洗涤剂附聚物的方法。 该方法包括以下步骤:(a)将洗涤剂表面活性剂浆料和干燥的起始洗涤剂材料连续混合到高速混合器/致密器中以获得洗涤剂附聚物,其中所述表面活性剂浆料包含按表面活性剂浆料重量计约0.1% 至约50%的非水性粘合剂,约70%至约95%的去污表面活性剂和余量的水; (b)在中速混合器/增密器中混合洗涤剂附聚物以进一步密度并附聚洗涤剂附聚物; 和(c)干燥所述洗涤剂附聚物以形成高密度洗涤剂组合物。 该方法可以包括一个或多个另外的处理步骤,例如在中等速度混合器/增密器之后添加涂覆剂以促进和控制附聚。
    • 2. 发明授权
    • Process for making a high density detergent composition by controlling
agglomeration within a dispersion index
    • 通过控制分散指数内的附聚来制备高密度洗涤剂组合物的方法
    • US5691297A
    • 1997-11-25
    • US530545
    • 1995-09-19
    • David Robert NassanoScott William Capeci
    • David Robert NassanoScott William Capeci
    • C11D11/00C11D17/06
    • C11D11/0082C11D17/065
    • A process for continuously preparing high density detergent composition is provided. The process comprises the steps of: (a) agglomerating a detergent surfactant paste and dry starting detergent material in a high speed mixer/densifier to obtain agglomerates having a Dispersion Index in a range of from about 1 to about 6, wherein Dispersion Index=A/B A is the surfactant level in the agglomerates having a particle size of at least 1100 microns, and B is the surfactant level in the agglomerates having a particle size less than about 150 microns; (b) mixing the agglomerates in a moderate speed mixer/densifier to further densify, build-up and agglomerate the agglomerates; and (c) conditioning the agglomerates such that the flow properties of the agglomerates are improved, thereby forming the high density detergent composition.
    • 提供连续制备高密度洗涤剂组合物的方法。 该方法包括以下步骤:(a)在高速混合器/致密器中将洗涤剂表面活性剂浆料和干燥的起始洗涤剂料料凝聚,以获得分散指数在约1至约6范围内的附聚物,其中分散指数= A / BA是颗粒尺寸至少为1100微米的附聚物中的表面活性剂水平,B是颗粒尺寸小于约150微米的附聚物中的表面活性剂水平; (b)在中速混合器/增密器中混合附聚物以进一步致密化,聚集和附聚附聚物; 和(c)调节附聚物,使得附聚物的流动性能得到改善,从而形成高密度洗涤剂组合物。
    • 9. 发明授权
    • Processes for making a granular detergent composition containing a
crystalline builder
    • 制备含有结晶助洗剂的颗粒洗涤剂组合物的方法
    • US5707959A
    • 1998-01-13
    • US596883
    • 1996-03-13
    • Eugene Joseph PancheriScott William CapeciRichard Thomas Owen
    • Eugene Joseph PancheriScott William CapeciRichard Thomas Owen
    • C11D3/12C11D11/00C11D17/06C11D11/02
    • C11D3/128C11D11/0082C11D17/065C11D3/1233
    • A process for preparing high density detergent compositions is provided. The process comprises the steps of: (a) continuously mixing a detergent surfactant paste and dry starting detergent material into a high speed mixer/densifier to obtain detergent agglomerates, wherein the ratio of the surfactant paste to the dry detergent material is from about 1:10 to about 10:1; (b) mixing the detergent agglomerates in a moderate speed mixer/densifier to further densify and agglomerate the detergent agglomerates; and (c) drying said detergent agglomerates so as to form the high density detergent composition. The dry detergent material may contain a builder material including a crystalline microstructure in which a carbonate anion, a calcium cation and at least one water-soluble cation are contained. The process may include one or more additional processing steps such as adding a coating agent such as the builder material described herein after the moderate speed mixer/densifier to facilitate and control agglomeration.
    • 提供了制备高密度洗涤剂组合物的方法。 该方法包括以下步骤:(a)将洗涤剂表面活性剂浆料和干燥起始洗涤剂材料连续混合到高速混合器/增密器中以获得洗涤剂附聚物,其中表面活性剂浆料与干洗涤剂材料的比例为约1: 10至10:1; (b)在中速混合器/增密器中混合洗涤剂附聚物以进一步致密化并附聚洗涤剂附聚物; 和(c)干燥所述洗涤剂附聚物以形成高密度洗涤剂组合物。 干燥的洗涤剂材料可以含有包含其中含有碳酸根阴离子,钙阳离子和至少一种水溶性阳离子的结晶微结构的助洗剂材料。 该方法可以包括一个或多个另外的加工步骤,例如在中速混合器/增密器之后添加涂覆剂,例如本文所述的助洗剂材料,以促进和控制附聚。