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1. 发明申请

US20200148828A1 SUCCINIMIDE-BASED COPOLYMERS AND USE AS HYDRATE INHIBITORS 审中-公开
公开(公告)号：US20200148828A1
公开(公告)日：2020-05-14
申请号：US16728245
申请日：2019-12-27
申请人： Saudi Arabian Oil Company , King Fahd University of Petroleum and Minerals
发明人： Mohamed Elanany , Khalid Majnouni , Rashed Alessa , Abdullah Al-Malki , Hassan Al-Ajwad , Mohammed Al-Daous , Shaikh Asrof Ali
IPC分类号： C08G73/10 , C10L3/10 , C08G73/02 , C08K5/01 , C08K5/04 , C08K5/07 , C08K5/16 , C08K5/34 , C08K5/36
摘要： Copolymers having General Formula (I): in which R1 is chosen from divalent C4-C7 aliphatic groups and divalent C4-C7 heteroaliphatic groups, optionally substituted with one or more C1-C6 aliphatic groups, heteroatoms independently chosen from O, N, and S, or combinations thereof, where: the divalent C4-C7 heteroaliphatic groups include one or two heteroatoms independently chosen from O, N, and S, and the maximum number of heteroatoms in R1 is two; x is a molar fraction range chosen from 0.05 to 0.95; and y is a molar fraction range chosen from 0.05 to 0.95, where the summation of x and y equals 1. Methods for inhibiting formation of clathrate hydrates in a fluid capable of forming the clathrate hydrates. The methods include contacting the fluid with at least one copolymer of General Formula (I) under conditions suitable for forming the clathrate hydrates.

2. 发明授权

US11060042B2 Succinimide-based copolymers and use as hydrate inhibitors 有权
公开(公告)号：US11060042B2
公开(公告)日：2021-07-13
申请号：US16728245
申请日：2019-12-27
申请人： Saudi Arabian Oil Company , King Fahd University of Petroleum and Minerals
发明人： Mohamed Elanany , Khalid Majnouni , Rashed Alessa , Abdullah Al-Malki , Hassan Al-Ajwad , Mohammed Al-Daous , Shaikh Asrof Ali
IPC分类号： C10L1/10 , C10L3/10 , C08G73/02 , C08G73/10 , C08K5/01 , C08K5/04 , C08K5/07 , C08K5/16 , C08K5/34 , C08K5/36
摘要： Copolymers having General Formula (I): in which R1 is chosen from divalent C4-C7 aliphatic groups and divalent C4-C7 heteroaliphatic groups, optionally substituted with one or more C1-C6 aliphatic groups, heteroatoms independently chosen from O, N, and S, or combinations thereof, where: the divalent C4-C7 heteroaliphatic groups include one or two heteroatoms independently chosen from O, N, and S, and the maximum number of heteroatoms in R1 is two; x is a molar fraction range chosen from 0.05 to 0.95; and y is a molar fraction range chosen from 0.05 to 0.95, where the summation of x and y equals 1. Methods for inhibiting formation of clathrate hydrates in a fluid capable of forming the clathrate hydrates. The methods include contacting the fluid with at least one copolymer of General Formula (I) under conditions suitable for forming the clathrate hydrates.

3. 发明申请

US20170321012A1 SUCCINIMIDE-BASED COPOLYMERS AND USE AS HYDRATE INHIBITORS 审中-公开
公开(公告)号：US20170321012A1
公开(公告)日：2017-11-09
申请号：US15584389
申请日：2017-05-02
申请人： Saudi Arabian Oil Company , King Fahd University of Petroleum and Minerals
发明人： Mohamed Elanany , Khalid Majnouni , Rashed Alessa , Abdullah Al-Malki , Hassan Al-Ajwad , Mohammed Al-Daous , Shaikh Asrof Ali
IPC分类号： C08G73/10 , C08K5/34 , C08K5/07 , C08G73/02 , C08K5/04 , C08K5/01 , C08K5/36 , C08K5/16
CPC分类号： C08G73/1092 , C08G73/02 , C08K5/01 , C08K5/04 , C08K5/07 , C08K5/16 , C08K5/34 , C08K5/36 , C10L3/107
摘要： Copolymers having General Formula (I): in which R1 is chosen from divalent C4-C7 aliphatic groups and divalent C4-C7 heteroaliphatic groups, optionally substituted with one or more C1-C6 aliphatic groups, heteroatoms independently chosen from O, N, and S, or combinations thereof, where: the divalent C4-C7 heteroaliphatic groups include one or two heteroatoms independently chosen from O, N, and S, and the maximum number of heteroatoms in R1 is two; x is a molar fraction range chosen from 0.05 to 0.95; and y is a molar fraction range chosen from 0.05 to 0.95, where the summation of x and y equals 1. Methods for inhibiting formation of clathrate hydrates in a fluid capable of forming the clathrate hydrates. The methods include contacting the fluid with at least one copolymer of General Formula (I) under conditions suitable for forming the clathrate hydrates.

4. 发明申请

US20170320985A1 METHODS FOR SYNTHESIZING ACRYLOYL-BASED COPOLYMERS, TERPOLYMERS 审中-公开
公开(公告)号：US20170320985A1
公开(公告)日：2017-11-09
申请号：US15585558
申请日：2017-05-03
申请人： Saudi Arabian Oil Company , King Fahd University of Petroleum and Minerals
发明人： Sameer A. Al-Ghamdi , Abdullah Al-Malki , Manal Al-Eid , Mohamed Elanany , Shaikh Asrof Ali
IPC分类号： C08F226/06 , C10L3/10
CPC分类号： C08F226/06 , C08F220/54 , C08F220/58 , C09K8/52 , C09K2208/22 , C09K2208/32 , C10L3/107
摘要： Methods for synthesizing acryloyl-based copolymers. The methods include providing a free radical initiator with a solution including monomeric repeating units, a chain transfer agent, and an organic solvent to form a reaction mixture, in which the monomeric repeating units include a first monomeric repeating unit having formula (1a), a second monomeric repeating unit having formula (1b) or (1d), and optionally a third monomeric repeating unit having formula (1c): in which the organic solvent is chosen from monoethylene glycol, ethanol, toluene, or combination thereof; and (B) initiating a polymerization reaction in the reaction mixture to polymerize the monomeric repeating units, thereby synthesizing the acryloyl-based copolymer. Methods for inhibiting formation of clathrate hydrates include contacting a fluid with the acryloyl-based copolymer synthesized in the reaction mixture.

5. 发明授权

US09890228B1 Quaternary ammonium solvated tetrapolymers and methods of removing CR(III) from solution using the tetrapolymer 有权
公开(公告)号：US09890228B1
公开(公告)日：2018-02-13
申请号：US15696760
申请日：2017-09-06
申请人： KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
发明人： Shamsuddeen Abdullahi Haladu , Shaikh Asrof Ali , Tawfik Abdo Saleh
IPC分类号： C08F26/06 , C02F1/28 , C02F101/22
CPC分类号： C08F26/06 , C02F1/285 , C02F2101/22
摘要： Cross-linked tetrapolymers made up of different diallyl zwitterionic diallyl quaternary ammonium salt monomers, with one of them functioning as a cross-linking monomer. The cross-linked terpolymers include a repeating unit with multiple ligand centers that different metal ions can bind to. The cross-linked tetrapolymers are cationic, zwitterionic and anionic, and can be in either an acidic form or a basic form. A method of removing metal ions from an aqueous solution with these cross-linked tetrapolymers is also described.

6. 发明授权

US09782768B2 Method for removing heavy metals from an aqueous solution with cross-linked copolymers 有权
公开(公告)号：US09782768B2
公开(公告)日：2017-10-10
申请号：US15282405
申请日：2016-09-30
申请人： KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
发明人： Zakariyah Abdulkareem Jamiu , Tawfik Abdo Saleh , Shaikh Asrof Ali
IPC分类号： B01J39/18 , B01J39/04 , C08G75/20 , C02F1/68 , C02F1/28 , C02F101/20 , C02F103/06
CPC分类号： B01J31/0222 , B01D61/02 , B01D65/02 , B01J31/0215 , B01J39/07 , B01J39/19 , B01J43/00 , B01J49/00 , C02F1/285 , C02F1/683 , C02F2101/20 , C02F2103/06 , C08G75/20 , C08J11/04 , H01M8/10
摘要： Cross-linked cyclocopolymers made up of one or more quaternary ammonium salts and sulfur dioxide as monomers. One of the quaternary ammonium salts is also an aspartic acid derivative. The cross-linked copolymers include a repeating unit with multiple chelating centers that different metal ions can bind to. The cross-linked copolymers are zwitterionic or anionic, and can be in either an acidic form or a basic form. A method for removing metal ions from an aqueous sample with these cross-linked copolymers is also described.

7. 发明授权

US09580521B1 Process for making a poly(zwitterion/dianion) 有权
标题翻译：制造聚（两性离子/二阴离子）
公开(公告)号：US09580521B1
公开(公告)日：2017-02-28
申请号：US15282175
申请日：2016-09-30
申请人： King Fahd University of Petroleum and Minerals , King Abdulaziz City for Science and Technology
发明人： Shaikh Asrof Ali , Shamsuddeen Abdullahi Haladu
IPC分类号： C08F8/44 , C08F226/04 , C08F8/12 , C08G75/22 , C08G75/20 , C08F26/06 , C08F226/06 , C08F26/04
CPC分类号： C08G75/22 , B01D65/02 , B01D2321/168 , C08F8/12 , C08F8/44 , C08F26/04 , C08F26/06 , C08F226/04 , C08F226/06 , C08G75/20 , C08G75/205
摘要： A zwitterionic monomer and corresponding cyclopolymerized polyzwitterion (±) (PZ) (i.e. poly(Z-alt-SO2). Phosophonate ester hydroloysis in PZ gave a pH-responsive polyzwitterionic acid (±) (PZA). The PZA under pH-induced transformation was converted into polyzwitterion/anion (±−) (PZAN) and polyzwitterion/dianion (±=) (PZDAN).
摘要翻译：两性离子单体和相应的环化聚合的两性离子（±）（PZ）（即聚（Z-alt-SO2）），PZ中的磷酸酯酯水解得到pH响应的两性离子酸（±）（PZA），pH诱导转化转化为聚两性离子/阴离子（± - ）（PZAN）和聚两性离子/二阴离子（±）（PZDAN）。

8. 发明授权

US08895633B2 Cross-linked polyaminocarboxylates for the removal of metal ions from aqueous solutions 有权
标题翻译：用于从水溶液中除去金属离子的交联聚氨基羧酸盐
公开(公告)号：US08895633B2
公开(公告)日：2014-11-25
申请号：US13784750
申请日：2013-03-04
申请人： King Fahd University of Petroleum and Minerals
发明人： Othman Charles Sadeq Othman Al Hamouz , Shaikh Asrof Ali , Nouri Mohammed Hassan
IPC分类号： C08F226/04 , C08F226/06 , C08F26/06
CPC分类号： C08F26/06
摘要： The cross-linked polyaminocarboxylates for the removal of metal ions from aqueous solutions of the present invention are cross-linked anionic polyelectrolytes CAPE 6 and CAPE 9, containing pH-responsive amino acid residues. The cross-linked anionic polyelectrolytes have been synthesized via cycloco-polymerization and ter-polymerization of a diallylammonioethanoate monomer (90 mol %) and a cross-linker, 1,1,4,4-tetraallylpiperazinium dichloride (10 mol %) in the absence of SO2 (CAPE 6) and in the presence of SO2 (CAPE 9), respectively. For the sorbents CAPE 6 and CAPE 9, the efficiency of Cu2+ removal at an initial metal concentration of 200 ppb was found to be 77.5% and 99.4%, respectively. Treatment of real wastewater samples spiked with Cu2+ ions showed the excellent ability of the cross-linked anionic polyelectrolytes to adsorb metal ions.
摘要翻译：用于从本发明的水溶液中除去金属离子的交联聚氨基羧酸盐是含有pH响应性氨基酸残基的交联阴离子聚电解质CAPE 6和CAPE 9。交联的阴离子聚电解质是通过二烯丙基氨基乙酸酯单体（90mol％）和交联剂1,1,4,4-四烯丙基哌嗪二氯化物（10mol％）在不存在的情况下的环共聚合和三元共聚合成的的SO2（CAPE 6）和SO 2（CAPE 9）的存在下。对于吸附剂CAPE 6和CAPE 9，初始金属浓度为200 ppb时Cu2 +去除效率分别为77.5％和99.4％。处理掺有Cu2 +离子的真实废水样品显示出交联阴离子聚电解质吸附金属离子的优异能力。

9. 发明授权

US09816024B2 2-(p-alkoxyphenyl)-2-imidazolines and their use as corrosion inhibitors 有权
公开(公告)号：US09816024B2
公开(公告)日：2017-11-14
申请号：US14727393
申请日：2015-06-01
申请人： King Fahd University of Petroleum and Minerals
发明人： Mohammad Abu Jafar Mazumder , Shaikh Asrof Ali , Hasan Ali Al-Muallem
IPC分类号： C09K8/54 , C23F11/14
CPC分类号： C09K8/54 , C09K2208/32 , C23F11/149
摘要： An aminoalkyl imidazolines of the formula: having p-octyloxy-, p-dodecyloxy-, or p-octadecyloxy-phenyl pendants as hydrophobes, for use to mitigate mild steel corrosion. An electron-rich aromatic ring, in conjugation with an amidine motif, imparts increasing corrosion inhibition efficiencies with an increasing hydrophobe chain length. X-ray photoelectron spectroscopy confirms the formation of an aminoalkyl imidazoline film on a metal surface prior to reaching a critical molar concentration.

10. 发明授权

US09790296B2 Cross-linked diallyl quaternary ammonium salt tetrapolymers and methods thereof 有权
公开(公告)号：US09790296B2
公开(公告)日：2017-10-17
申请号：US14644822
申请日：2015-03-11
申请人： King Fahd University of Petroleum and Minerals
发明人： Shamsuddeen Abdullahi Haladu , Shaikh Asrof Ali , Tawfik Abdo Saleh
IPC分类号： C08F26/06 , C02F1/28 , C02F101/22
CPC分类号： C08F26/06 , C02F1/285 , C02F2101/22
摘要： Cross-linked tetrapolymers made up of different diallyl zwitterionic diallyl quaternary ammonium salt monomers, with one of them functioning as a cross-linking monomer. The cross-linked terpolymers include a repeating unit with multiple ligand centers that different metal ions can bind to. The cross-linked tetrapolymers are cationic, zwitterionic and anionic, and can be in either an acidic form or a basic form. A method of removing metal ions from an aqueous solution with these cross-linked tetrapolymers is also described.

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