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    • 2. 发明授权
    • Iron-based powder composition for powder metallurgy excellent in
flowability and compactibility and method
    • 用于粉末冶金的铁基粉末组合物具有流动性和紧凑性和方法优异
    • US5989304A
    • 1999-11-23
    • US973142
    • 1997-11-28
    • Yukiko OzakiSatoshi UenosonoKuniaki Ogura
    • Yukiko OzakiSatoshi UenosonoKuniaki Ogura
    • B22F1/00B22F1/02C22C33/02
    • B22F1/0062B22F1/0059B22F1/0077B22F1/0096B22F1/02C22C33/02C22C33/0207B22F2003/023B22F2003/145B22F2998/00
    • An iron-based powder composition for powder metallurgy excellent in flowability and compactibility is produced in accordance with a method comprising the steps of: adding to iron-based and alloying powders, for a primary mixing, a surface treatment agent, and in addition, for a secondary mixing, a fatty acid amide and at least one lubricant, wherein the lubricant has a melting point higher than that of the fatty acid amide and can be a thermoplastic resin, a thermoplastic elastomer, and inorganic or organic compounds having a layered crystal structure; heating and stirring up a mixture after the secondary mixing at a temperature above a melting point of the fatty acid amide to melt the fatty acid amide; cooling, while mixing, the mixture subjected to the heating and stirring process so that the alloying powder and a lubricant having a melting point higher than the fatty acid amide adhere to a surface of the iron base powder subjected to the surface treatment by an adhesive force of the melt; and adding at the time of the cooling, for a tertiary mixing, a metallic soap and at least one thermoplastic resin or thermoplastic elastomer powders and inorganic or organic compounds having layered crystal structure. The mixture is heated to about 423K and loaded into a die for compaction.
    • PCT No.PCT / JP97 / 00029 Sec。 371日期1997年11月28日 102(e)1997年11月28日日期PCT 1997年1月9日PCT PCT。 公开号WO98 / 05454 日期1998年12月2日根据包括以下步骤的方法制备粉末冶金用的粉末冶金用铁粉组合物:将铁基和合金粉末加入到初级混合表面处理剂中, 此外,对于二次混合,脂肪酸酰胺和至少一种润滑剂,其中润滑剂的熔点高于脂肪酸酰胺的熔点,并且可以是热塑性树脂,热塑性弹性体和无机或有机化合物 具有层状晶体结构; 在高于脂肪酸酰胺的熔点的温度下二次混合之后加热和搅拌混合物以熔化脂肪酸酰胺; 冷却,同时混合,将混合物进行加热和搅拌处理,使得合金粉末和熔点高于脂肪酸酰胺的润滑剂与通过粘合力进行表面处理的铁基粉末的表面粘附 的熔体; 在冷却时加入金属皂和至少一种热塑性树脂或热塑性弹性体粉末和具有层状晶体结构的无机或有机化合物。 将混合物加热至约423K并加载到模具中用于压实。
    • 3. 发明授权
    • Iron-based powder mixture for powder metallurgy, process for producing the same, and method of forming a molding from the same
    • 用于粉末冶金的铁基粉末混合物,其制备方法以及从其形成模塑方法
    • US06451082B1
    • 2002-09-17
    • US09749576
    • 2000-12-28
    • Yukiko OzakiSatoshi UenosonoKuniaki Ogura
    • Yukiko OzakiSatoshi UenosonoKuniaki Ogura
    • B22F102
    • B22F1/0062B22F1/0059B22F1/0077B22F1/0096B22F2003/145B22F2998/00C22C33/0207
    • An iron-based powder composition is provided that is greatly flowable and compactible and less dependent on temperature with respect to flowability and compactibility at room temperature or during warming. The iron-based powder composition includes an iron-based powder, a lubricant melted and fixed to the iron-based powder, an alloying powder bonded to the iron-based powder with the aid of the lubricant, and a free lubricant. One or more constituent members are coated with an organosiloxane layer in a coating ratio of greater than about 80%. The organosiloxane has phenyl groups as a functional group. The lubricant melted and fixed to the iron-based powder is a composite melt composed of a calcium soap and a lithium soap, or a composite melt composed of a calcium soap and an amide lubricant. The free lubricant is a mixed powder composed of an amide lubricant and a methyl polymethacrylate powder, or a lithium soap powder. A process for producing the iron-based powder composition is also provided.
    • 提供了一种铁基粉末组合物,其在流动性和在室温下或在加热过程中的紧密性方面具有极大的流动性和可压缩性,并且对温度的依赖性较小。 铁基粉末组合物包括铁基粉末,融化并固定在铁基粉末上的润滑剂,借助润滑剂粘合到铁基粉末上的合金粉末和游离润滑剂。 一个或多个构成部件以大于约80%的涂布比涂覆有机硅氧烷层。 有机硅氧烷具有苯基作为官能团。 熔融并固定在铁基粉末上的润滑剂是由钙皂和锂皂组成的复合熔体或由钙皂和酰胺润滑剂组成的复合熔体。 游离润滑剂是由酰胺润滑剂和聚甲基丙烯酸甲酯粉末或锂皂粉组成的混合粉末。 还提供了一种制备铁基粉末组合物的方法。
    • 4. 发明授权
    • Iron-based powder composition for powder metallurgy having higher flowability and higher compactibility and process for production thereof
    • 用于粉末冶金的铁基粉末组合物具有较高的流动性和更高的紧密度及其生产方法
    • US06503445B2
    • 2003-01-07
    • US09767111
    • 2001-01-22
    • Yukiko OzakiSatoshi UenosonoKuniaki Ogura
    • Yukiko OzakiSatoshi UenosonoKuniaki Ogura
    • B22F302
    • B22F1/0062B22F1/0059B22F1/0077B22F1/0096B22F2998/00C22C33/0207
    • A process for producing an iron-based powder composition for powder metallurgy having excellent flowability at room temperature and a warm compaction temperature, having improved compactibility enabling lowering ejection force in compaction, and to provide a process for producing a compact of a high density from the iron-based powder composition, wherein the iron-based powder composition comprises an iron-based powder, a lubricant, and an alloying powder, and at least one of the iron-based powder, the lubricant, and the alloying powder is coated with at least one surface treatment agent selected from the group of surface treatment agents of organoalkoxysilanes, organosilazanes, titanate coupling agents, fluorine-containing silicon silane coupling agents, and wherein the iron-based powder composition is compacted at a temperature not lower than the lowest melting point of the employed lubricants, but not higher than the highest melting point of the employed lubricants.
    • 一种粉末冶金用铁基粉末组合物的制造方法,其在室温下具有优异的流动性和温暖的压实温度,具有改善的压实性,从而能够降低压缩时的喷射力,并且提供了一种从 铁基粉末组合物,其中所述铁基粉末组合物包含铁基粉末,润滑剂和合金粉末,并且所述铁基粉末,所述润滑剂和所述合金粉末中的至少一种涂覆有 至少一种选自有机烷氧基硅烷的表面处理剂,有机硅氮烷,钛酸酯偶联剂,含氟硅烷偶联剂的表面处理剂,其中铁基粉末组合物在不低于最低熔点的温度下压实 的使用润滑剂,但不高于所用润滑剂的最高熔点。
    • 5. 发明授权
    • Iron base powder mixture for powder metallurgy excellent in fluidity and moldability, method of production thereof, and method of production of molded article by using the iron base powder mixture
    • 用于粉末冶金的铁基粉末混合物,其流动性和成型性优异,其制备方法,以及使用铁基粉末混合物制备成型制品的方法
    • US06235076B1
    • 2001-05-22
    • US09171911
    • 1998-10-28
    • Yukiko OzakiSatoshi UenosonoKuniaki Ogura
    • Yukiko OzakiSatoshi UenosonoKuniaki Ogura
    • B22F100
    • B22F1/0062B22F1/0059B22F1/0077B22F1/0096B22F2998/00C22C33/0207
    • The present invention intends to provide an iron-based powder composition for powder metallurgy having excellent flowability at room temperature and a warm compaction temperature, having improved compactibility enabling lowering ejection force in compaction, to provide a process for producing the iron-based powder composition, and to provide a process for producing a compact of a high density from the iron-based powder composition. The iron-based powder composition comprises an iron-based powder, a lubricant, and an alloying powder, and at least one of the iron-based powder, the lubricant, and the alloying powder is coated with at least one surface treatment agent selected from the group of surface treatment agents of organoalkoxysilanes, organosilazanes, titanate coupling agents, fluorine-containing silicon silane coupling agents. The iron-based powder composition is compacted at a temperature not lower than the lowest melting point of the employed lubricants, but not higher than the highest melting point of the employed lubricants.
    • 本发明提供一种粉末冶金用铁粉末组合物,其在室温下具有优异的流动性和温和的压实温度,其具有改善的压实性,从而能够降低压实时的喷射力,从而提供了制备铁基粉末组合物的方法, 并提供从铁基粉末组合物制造高密度的压块的方法。 铁基粉末组合物包含铁基粉末,润滑剂和合金粉末,并且至少一种铁基粉末,润滑剂和合金粉末涂覆有至少一种选自以下的表面处理剂: 有机烷氧基硅烷,有机硅氮烷,钛酸酯偶联剂,含氟硅烷偶联剂的表面处理剂组。 铁基粉末组合物在不低于所用润滑剂的最低熔点的温度下压实,但不高于所用润滑剂的最高熔点。
    • 6. 发明授权
    • Method of making iron-based powder composition for powder metallurgy
excellent in flow ability and compactibility
    • 制造粉末冶金用铁基粉末组合物的流动性和紧凑性优异的方法
    • US6139600A
    • 2000-10-31
    • US401841
    • 1999-09-22
    • Yukiko OzakiSatoshi UenosonoKuniaki Ogura
    • Yukiko OzakiSatoshi UenosonoKuniaki Ogura
    • B22F1/00B22F1/02C22C33/02
    • B22F1/0062B22F1/0059B22F1/0077B22F1/0096B22F1/02C22C33/02C22C33/0207B22F2003/023B22F2003/145B22F2998/00
    • An iron-based powder composition is produces in accordance with a method comprising the steps of: adding to iron-based and alloying powders, for a primary mixing, a surface treatment agent, and in addition, for a secondary mixing, a fatty acid amide and at least one lubricant, wherein the lubricant has a melting point higher than that of the fatty acid amide and can be, a thermoplastic resin, a thermoplastic elastomer, and inorganic or organic compounds having a layered crystal structure; heating and stirring up a mixture after the secondary mixing at a temperature above a melting point of the fatty acid amide to melt the fatty acid amide; cooling, while mixing, the mixture subjected to the heating and stirring process so that the alloying powder and a lubricant having a melting point higher than the fatty acid amide adhere to a surface of the iron base powder subjected to the surface treatment by an adhesive force of the melt; and adding at the time of the cooling, for a tertiary mixing, a metallic soap and at least one a thermoplastic resin or thermoplastic elastomer powders and inorganic or organic compounds having layered crystal structure. The mixture is heated to about 423K and loaded into a die for compaction.
    • 铁基粉末组合物根据包括以下步骤的方法生产:将铁基和合金粉末加入到初级混合表面处理剂中,并且另外加入脂肪酸酰胺 和至少一种润滑剂,其中所述润滑剂的熔点高于所述脂肪酸酰胺的熔点,并且可以是热塑性树脂,热塑性弹性体和具有层状晶体结构的无机或有机化合物; 在高于脂肪酸酰胺的熔点的温度下二次混合之后加热和搅拌混合物以熔化脂肪酸酰胺; 冷却,同时混合,将混合物进行加热和搅拌处理,使得合金粉末和熔点高于脂肪酸酰胺的润滑剂与通过粘合力进行表面处理的铁基粉末的表面粘附 的熔体; 在冷却时加入金属皂和至少一种热塑性树脂或热塑性弹性体粉末和具有层状晶体结构的无机或有机化合物。 将混合物加热至约423K并加载到模具中用于压实。
    • 7. 发明授权
    • Iron-based mixed powder for powder metallurgy and sintered body
    • 用于粉末冶金和烧结体的铁基混合粉末
    • US07300490B2
    • 2007-11-27
    • US11230714
    • 2005-09-20
    • Yukiko OzakiHiroshi SugiharaSatoshi Uenosono
    • Yukiko OzakiHiroshi SugiharaSatoshi Uenosono
    • B22F1/00
    • C22C33/0228B22F1/0059
    • An iron-based mixed powder for powder metallurgy having improved machinability, without degrading the mechanical property of a sintered body made by compacting the iron-based mixed power. The iron-based mixed powder comprises a mixture of an iron-based powder, a powder for an alloy, a powder for machinability improvement, and a lubricant. The powder for machinability improvement comprises a manganese sulfide powder, and at least one selected from the group consisting of a calcium phosphate powder and a hydroxy apatite powder. Alternatively the powder for machinability improvement has an average particle diameter of 1 to 60 micrometers and comprise manganese sulfide powder and calcium fluoride powder.
    • 一种用于粉末冶金的铁基混合粉末,其具有改善的机械加工性,而不降低通过压制铁基混合动力制成的烧结体的机械性能。 铁基混合粉末包括铁基粉末,合金粉末,用于机械加工性改进的粉末和润滑剂的混合物。 用于机械加工性改善的粉末包括硫化锰粉末和选自磷酸钙粉末和羟基磷灰石粉末中的至少一种。 或者,用于机械加工性改进的粉末具有1至60微米的平均粒径,并且包含硫化锰粉末和氟化钙粉末。