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    • 3. 发明申请
    • Method for Producing Chlorinated Aromatic Compound
    • 生产氯化芳香化合物的方法
    • US20100168484A1
    • 2010-07-01
    • US11990075
    • 2006-08-03
    • Susumu KyotaniNaoki Furukawa
    • Susumu KyotaniNaoki Furukawa
    • C07C17/08
    • C07C17/08C07C22/04C08F110/10C08F4/00C08F2500/03
    • [PROBLEMS] To provide a simpler method for producing a high-quality chlorinated aromatic hydrocarbon (e.g., cumylchloride), which can be used as a cationic polymerization initiator.[MEANS FOR SOLVING PROBLEMS] A chlorinated aromatic hydrocarbon can be produced by repeating both (a) the step of performing chlorination reaction by stirring an organic solution containing a compound represented by Ar(R1C═CH2)n with an aqueous hydrochloric acid solution having a hydrochloric acid concentration of 30% by weight or higher and (b) the step of removing the water phase in part or whole from the reaction solution produced in the step (a), and then adding an aqueous hydrochloric acid solution having a hydrochloric acid concentration of 30% by weight or higher to the reaction solution, until the chlorination reaction rate of the compound reaches a predetermined level.
    • 为了提供可以用作阳离子聚合引发剂的高质量氯化芳烃(例如氯化亚铜)的制备方法。 解决问题的手段氯化芳烃可以通过重复(a)通过搅拌含有由Ar(R 1 = CH 2)n表示的化合物的有机溶液的有机溶液与(a)的盐酸水溶液 盐酸浓度为30重量%以上,(b)从步骤(a)中制备的反应溶液中部分或全部除去水相的步骤,然后加入盐酸浓度的盐酸水溶液 相对于反应溶液为30重量%以上,直到化合物的氯化反应速度达到预定水平。
    • 4. 发明申请
    • Process for Producing Spherical Polymer Powder and Spherical Powder Comprising (Meth)Acrylic Block Copolymer
    • 制备(甲基)丙烯酸嵌段共聚物的球形聚合物粉末和球形粉末的方法
    • US20080152909A1
    • 2008-06-26
    • US11884035
    • 2006-02-09
    • Susumu KyotaniNaoki FurukawaTakeshi Chiba
    • Susumu KyotaniNaoki FurukawaTakeshi Chiba
    • C08J3/12B32B5/16C08F20/06
    • C08J3/14C08J2333/04Y10T428/2982
    • A process for spherical-polymer-powder production by which polymer particles which are nearly spherical, small in particle diameter, and suitable for use as a molding material can be easily obtained. The spherical polymer powder has excellent powder flowability, is safe, and can form, e.g., a high-quality molding, skin material, or coating film which is excellent in weather-ability, flexibility, rubber elasticity, low-temperature characteristics, adhesion to polar resins, texture, appearance, etc. The process for spherical-polymer-powder production is characterized by comprising a step in which an aqueous dispersion comprising a solvent solution of a polymer, water, and a dispersant is heated with stirring under such conditions that the power per unit volume of the dispersion, P/V, is 0.2 kW/m3 or more to remove the solvent from the aqueous dispersion.
    • 可以容易地获得球状聚合物粉末生产方法,通过该方法可以容易地获得几乎球形,粒径小,适合用作成型材料的聚合物颗粒。 球形聚合物粉末具有优异的粉末流动性,安全性,并且可以形成例如耐候性,柔韧性,橡胶弹性,低温特性,粘合性等优异的高品质成型,表皮材料或涂膜 极性树脂,质地,外观等。球形聚合物 - 粉末生产方法的特征在于包括以下步骤:将包含聚合物,水和分散剂的溶剂溶液的水性分散体在搅拌下加热的步骤, 每分散体积的功率P / V为0.2kW / m 3以上以从水性分散体中除去溶剂。