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    • 7. 发明申请
    • 3D miniature preconcentrator and inlet sample heater
    • 3D微型预浓缩器和入口样品加热器
    • US20070084347A1
    • 2007-04-19
    • US11239367
    • 2005-09-30
    • Paul BoyleDavid Ruiz-AlonsoAndrew KoehlMartyn RushRussell ParrisAshley Wilks
    • Paul BoyleDavid Ruiz-AlonsoAndrew KoehlMartyn RushRussell ParrisAshley Wilks
    • B01D53/02
    • G01N1/405B01D53/02B01D53/0407G01N2030/085Y10T436/25375
    • The present invention relates to a three dimensional preconcentrator and inlet heater. The preconcentrator consists of a substrate with passageways, a conductive material coated to the top and the bottom of the substrate and an adsorbent coating covering the entire substrate. This substrate is suspended in a holding frame by a connecting bridge. The preconcentrator may also include a resistor and a proportional-integral-differential controller. The device may be used inline with a detector and can be retrofitted to existing devices. An array of preconcentrators may also be formed. The invention also relates to methods of use of the preconcentrator and methods of manufacture. A method of use includes contacting an analyte and a preconcentrator, allowing the analyte to adsorb to the preconcentrator and then desorbing the analyte. A method of manufacture involves applying the adsorbent coating by misted chemical deposition.
    • 本发明涉及一种三维预浓缩器和入口加热器。 预浓缩器由具有通道的基底,涂覆到基底的顶部和底部的导电材料和覆盖整个基底的吸附剂涂层组成。 该基板通过连接桥悬挂在保持框架中。 预浓缩器还可以包括电阻器和比例积分微分控制器。 该装置可以与检测器联合使用,并且可以被改装到现有装置。 还可以形成一组预浓缩器。 本发明还涉及预浓缩器的使用方法和制造方法。 一种使用方法包括使分析物和预浓缩器接触,允许分析物吸附到预浓缩器,然后解吸分析物。 制造方法包括通过雾化的化学沉积来施加吸附剂涂层。