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1. 发明申请

US20150119304A1 PROCESS FOR PREPARING AN OVERBASED SALT OF A SULFURIZED ALKYL-SUBSTITUTED HYDROXYAROMATIC COMPOSITION 有权
标题翻译：制备硫化烷基取代羟基芳族化合物的过硫酸盐的方法
公开(公告)号：US20150119304A1
公开(公告)日：2015-04-30
申请号：US14067121
申请日：2013-10-30
申请人： Ronald T.F. Jukes , Eugene E. Spala
发明人： Ronald T.F. Jukes , Eugene E. Spala
IPC分类号： C10M135/02 , C07C319/14
CPC分类号： C10M135/02 , C07C319/14 , C10M159/22 , C10M177/00 , C10M2203/1006 , C10M2203/1025 , C10M2219/089 , C10N2210/02 , C10N2230/02 , C10N2230/10 , C10N2240/10 , C10N2240/102
摘要： Disclosed herein is an overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition, which is prepared by the process comprising (a) providing an overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition having a total base number (TBN) greater than about 250; and (b) sparging the overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition with air at a temperature ranging from about 190° C. to about 250° C.
摘要翻译：本文公开了硫化烷基取代的羟基芳族组合物的高碱性盐，其通过以下方法制备，所述方法包括（a）提供总碱值（TBN）大于约250的硫化烷基取代的羟基芳族组合物的高碱性盐; 和（b）在约190℃至约250℃的温度下用空气喷射含硫烷基取代的羟基芳族组合物的高碱性盐。

2. 发明授权

US09434906B2 Marine diesel engine lubricating oil compositions 有权
标题翻译：船用柴油机润滑油组成
公开(公告)号：US09434906B2
公开(公告)日：2016-09-06
申请号：US13849884
申请日：2013-03-25
申请人： Ronald Theodorus Fake Jukes , Eugene E. Spala
发明人： Ronald Theodorus Fake Jukes , Eugene E. Spala
IPC分类号： C10M159/22 , C10M169/04
CPC分类号： C10M169/044 , C10M159/22 , C10M2203/1006 , C10M2207/262 , C10M2219/046 , C10M2219/089 , C10N2210/02 , C10N2220/022 , C10N2230/02 , C10N2230/04 , C10N2230/10 , C10N2230/52 , C10N2240/102 , C10N2260/10 , C10N2270/00
摘要： Disclosed herein are marine diesel engine lubricating oil compositions which comprises (a) a major amount of an oil of lubricating viscosity, and (b) about 3 wt. % to about 40 wt. %, based on the total weight of the marine diesel engine lubricating oil composition, of a sulfurized, alkaline earth metal alkylphenate detergent which is substantially free of polyol promoter oxidation products.
摘要翻译：本文公开了船用柴油发动机润滑油组合物，其包含（a）主要量的润滑粘度的油，和（b）约3重量％％至约40wt。基于船用柴油发动机润滑油组合物的总重量，基本上不含多元醇促进剂氧化产物的硫化碱土金属烷基酚盐洗涤剂。

3. 发明授权

US08933002B2 Lubricating oil compositions 有权
标题翻译：润滑油组成
公开(公告)号：US08933002B2
公开(公告)日：2015-01-13
申请号：US13293387
申请日：2011-11-10
申请人： Gilles Sinquin , Curt Campbell , Hélène Lecroq , Eugene E. Spala
发明人： Gilles Sinquin , Curt Campbell , Hélène Lecroq , Eugene E. Spala
IPC分类号： C10M135/02 , C10M159/22 , C07C37/66 , C07C39/00 , C07C381/00
CPC分类号： C07C381/00 , C10M135/02 , C10M159/22 , C10M2219/088 , C10M2219/089 , C10N2240/10 , C10N2270/00 , C10N2210/02
摘要： Disclosed herein is a neutral or overbased salt of a sulfurized alkylhydroxyaromatic compound obtained by the process comprising the steps of (a) sulfurizing an alkylhydroxyaromatic compound derived from alkylation of a hydroxyaromatic compound with one or more olefins comprising C9 to C18 oligomers of monomers selected from propylene, butylene or mixtures thereof to provide a sulfurized alkylhydroxyaromatic reaction product; (b) removing any unsulfurized alkylhydroxyaromatic compound from the sulfurized alkylhydroxyaromatic reaction product of step (a) to obtain a sulfurized alkylhydroxyaromatic compound substantially free of the unsulfurized alkylhydroxyaromatic compound; and (c) neutralizing the sulfurized alkylhydroxyaromatic compound of step (b) to provide a salt of the sulfurized alkylhydroxyaromatic compound, wherein the overbased salt of the sulfurized alkylhydroxyaromatic compound contains less than about 2% by combined mass of the unsulfurized alkylhydroxyaromatic compound and its unsulfurized metal salt.
摘要翻译：本文公开了一种中和或高碱性的硫化烷基羟基芳族化合物的盐，该方法包括以下步骤：（a）将衍生自羟基芳族化合物的烷基羟基芳族化合物硫化为一种或多种烯烃，所述烯烃包含选自丙烯的单体的C 9至C 18低聚物，丁烯或其混合物以提供硫化的烷基羟基芳族化合物反应产物; （b）从步骤（a）的硫化烷基羟基芳族化合物反应产物中除去任何未硫化的烷基羟基芳族化合物，得到基本上不含未硫化烷基羟基芳族化合物的硫化烷基羟基芳族化合物; 和（c）中和步骤（b）的硫化烷基羟基芳族化合物以提供硫化烷基羟基芳族化合物的盐，其中硫化烷基羟基芳族化合物的高碱性盐含有少于约2％的未硫化烷基羟基芳族化合物及其未硫化的金属盐。

4. 发明授权

US09062271B2 Process for preparing an overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition 有权
标题翻译：制备硫化烷基取代的羟基芳族组合物的高碱性盐的方法
公开(公告)号：US09062271B2
公开(公告)日：2015-06-23
申请号：US14067121
申请日：2013-10-30
申请人： Ronald T. F. Jukes , Eugene E. Spala
发明人： Ronald T. F. Jukes , Eugene E. Spala
IPC分类号： C10M159/22 , C10M135/02 , C07C319/14
CPC分类号： C10M135/02 , C07C319/14 , C10M159/22 , C10M177/00 , C10M2203/1006 , C10M2203/1025 , C10M2219/089 , C10N2210/02 , C10N2230/02 , C10N2230/10 , C10N2240/10 , C10N2240/102
摘要： Disclosed herein is an overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition, which is prepared by the process comprising (a) providing an overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition having a total base number (TBN) greater than about 250; and (b) sparging the overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition with air at a temperature ranging from about 190° C. to about 250° C.
摘要翻译：本文公开了硫化烷基取代的羟基芳族组合物的高碱性盐，其通过以下方法制备，所述方法包括（a）提供总碱值（TBN）大于约250的硫化烷基取代的羟基芳族组合物的高碱性盐; 和（b）在约190℃至约250℃的温度下用空气喷射含硫烷基取代的羟基芳族组合物的高碱性盐。

5. 发明授权

US08603956B2 Super overbased polyalkenyl sulfonate and alkylaryl sulfonate composition and process for making the same 有权
标题翻译：超高分子聚链烯基磺酸盐和烷基芳基磺酸盐组合物及其制备方法
公开(公告)号：US08603956B2
公开(公告)日：2013-12-10
申请号：US11279505
申请日：2006-04-12
申请人： Eugene E. Spala
发明人： Eugene E. Spala
IPC分类号： C10M159/12
CPC分类号： C10M159/24 , C10M2205/026 , C10M2219/046 , C10N2210/01 , C10N2210/02 , C10N2230/02 , C10N2230/52
摘要： The present invention is directed to super overbased polyalkenyl sulfonate and alkylaryl sulfonate composition comprising (a) one or more super overbased polyalkenyl sulfonates and (b) one or more super overbased alkylaryl sulfonates wherein the total base number (TBN) of the sulfonate composition is greater than 400. The present invention is also directed to a process for preparing such super overbased polyalkenyl sulfonate and alkylaryl sulfonate composition.
摘要翻译：本发明涉及超高碱性聚链烯基磺酸盐和烷基芳基磺酸盐组合物，其包含（a）一种或多种超高碱性聚链烯基磺酸盐和（b）一种或多种超高碱性烷基芳基磺酸盐，其中磺酸盐组合物的总碱值（TBN）较大本发明还涉及制备这种超高碱性聚链烯基磺酸盐和烷基芳基磺酸盐组合物的方法。

6. 发明授权

US08993499B2 Low temperature performance lubricating oil detergents and method of making the same 有权
标题翻译：低温性能润滑油清洁剂及其制造方法
公开(公告)号：US08993499B2
公开(公告)日：2015-03-31
申请号：US12339894
申请日：2008-12-19
申请人： Curt B. Campbell , Gilles P. Sinquin , Eugene E. Spala , Gilbert R. Chapon
发明人： Curt B. Campbell , Gilles P. Sinquin , Eugene E. Spala , Gilbert R. Chapon
IPC分类号： C10M159/20 , C10M159/22
CPC分类号： C10M159/20 , C10M159/22 , C10M2203/1025 , C10M2207/262 , C10M2215/28 , C10M2219/044 , C10M2223/045 , C10N2210/06 , C10N2220/028 , C10N2230/02 , C10N2230/04 , C10N2240/02 , C10N2240/04 , C10N2270/00 , C10N2220/022 , C10N2260/00 , C10N2260/14 , C10N2210/02
摘要： A carboxylate detergent prepared by the process comprising (a) alkylating a hydroxyaromatic compound with at least one normal alpha olefin having from about 12 to about 30 carbon atoms per molecule that has been isomerized to obtain an isomerized alpha olefin having 15-98 wt % branching and a residual alpha olefin content of between from about 0.1 to about 30 wt %, thereby producing an alkylated hydroxyaromatic compound; (b) neutralizing the resulting alkylated hydroxyaromatic compound with an alkali metal base; (c) carbonating the alkali metal salt from step (b) with carbon dioxide; (d) acidifying the salt produced in step (c); and (e) overbasing the resulting alkylated hydroxyaromatic carboxylic acid.
摘要翻译：通过该方法制备的羧酸盐洗涤剂包括（a）使羟基芳族化合物与至少一种正构的α-烯烃在每分子中具有约12至约30个碳原子进行烷基化，所述α-烯烃已被异构化，以获得具有15-98重量％支化的异构化α-烯烃和约0.1至约30重量％之间的残余α-烯烃含量，从而产生烷基化羟基芳族化合物; （b）用碱金属碱中和得到的烷基化羟基芳族化合物; （c）用二氧化碳将步骤（b）的碱金属盐碳化; （d）酸化步骤（c）中产生的盐; 和（e）使得到的烷基化羟基芳族羧酸过碱化。

7. 发明申请

US20140081043A1 Method For The Preparation of Low Overbased Alkyltoluene Sulfonate 有权
标题翻译：低碱性烷基甲苯磺酸盐的制备方法
公开(公告)号：US20140081043A1
公开(公告)日：2014-03-20
申请号：US14001346
申请日：2011-03-30
申请人： Pierre Téqui , Curt B. Campbell , Gilles P. Sinquin , Christine Boemare Gandon , Kyle J. Frederic , Eugene E. Spala
发明人： Pierre Téqui , Curt B. Campbell , Gilles P. Sinquin , Christine Boemare Gandon , Kyle J. Frederic , Eugene E. Spala
IPC分类号： C07C303/06
CPC分类号： C07C303/06 , B01J8/02 , B01J19/0013 , B01J19/0033 , B01J2219/00166 , B01J2219/00186 , B01J2219/00202 , B01J2219/00231 , C07C2/66 , C07C303/14 , C07C303/32 , C07C2529/08 , C07C2529/70 , C10M159/24 , C10M177/00 , C10M2219/044 , C10M2219/046 , C10N2210/02 , C10N2230/70 , C10N2270/00 , C10N2270/02 , C07C15/107 , C07C309/31
摘要： Disclosed is a method for improving filtration in the preparation of an alkaline earth metal alkyltoluene sulfonate concentrate by selectively controlling the meta, ortho, para isomer distribution of the alkyl group of the alkyltoluene produced by the process comprising alkylating toluene with at least one isomerized normal alpha olefin, having from about 18 to about 30 carbon atoms and having from 20% to 100% branching in an alkylation process which includes monitoring % isomer formation and adjusting an alkylation process parameter in order to provide a target specified isomer content of less than 38% meta-isomer content; and thereafter sulfonating and neutralizing to produce a low base number sulfonated alkyltoluene concentrate having a Base Number of about 2 to 60 (ASTM D 2896).
摘要翻译：公开了一种通过选择性地控制烷基甲苯的烷基的间位，邻位，对位异构体分布来制备碱土金属烷基甲苯磺酸盐浓缩物的方法，该方法包括使甲苯与至少一种异构化的正常α 烯烃，其具有约18至约30个碳原子并且在烷基化方法中具有20％至100％的支化，其包括监测％异构体形成和调节烷基化方法参数，以提供小于38％的目标特异异构体含量，间 - 异构体含量; 然后磺化和中和以产生碱值为约2至60（ASTM D 2896）的低碱值磺化烷基甲苯浓缩物。

8. 发明申请

US20130123157A1 LUBRICATING OIL COMPOSITIONS 有权
标题翻译：润滑油组合物
公开(公告)号：US20130123157A1
公开(公告)日：2013-05-16
申请号：US13293387
申请日：2011-11-10
申请人： Gilles Sinquin , Curt Campbell , Hélène Lecroq , Eugene E. Spala
发明人： Gilles Sinquin , Curt Campbell , Hélène Lecroq , Eugene E. Spala
IPC分类号： C10M135/02 , C07C381/00
CPC分类号： C07C381/00 , C10M135/02 , C10M159/22 , C10M2219/088 , C10M2219/089 , C10N2240/10 , C10N2270/00 , C10N2210/02
摘要： Disclosed herein is a neutral or overbased salt of a sulfurized alkylhydroxyaromatic compound obtained by the process comprising the steps of (a) sulfurizing an alkylhydroxyaromatic compound derived from alkylation of a hydroxyaromatic compound with one or more olefins comprising C9 to C18 oligomers of monomers selected from propylene, butylene or mixtures thereof to provide a sulfurized alkylhydroxyaromatic reaction product; (b) removing any unsulfurized alkylhydroxyaromatic compound from the sulfurized alkylhydroxyaromatic reaction product of step (a) to obtain a sulfurized alkylhydroxyaromatic compound substantially free of the unsulfurized alkylhydroxyaromatic compound; and (c) neutralizing the sulfurized alkylhydroxyaromatic compound of step (b) to provide a salt of the sulfurized alkylhydroxyaromatic compound, wherein the overbased salt of the sulfurized alkylhydroxyaromatic compound contains less than about 2% by combined mass of the unsulfurized alkylhydroxyaromatic compound and its unsulfurized metal salt.
摘要翻译：本文公开了一种中和或高碱性的硫化烷基羟基芳族化合物的盐，该方法包括以下步骤：（a）将衍生自羟基芳族化合物的烷基羟基芳族化合物硫化为一种或多种烯烃，所述烯烃包含选自丙烯的单体的C 9至C 18低聚物，丁烯或其混合物以提供硫化的烷基羟基芳族化合物反应产物; （b）从步骤（a）的硫化烷基羟基芳族化合物反应产物中除去任何未硫化的烷基羟基芳族化合物，得到基本上不含未硫化烷基羟基芳族化合物的硫化烷基羟基芳族化合物; 和（c）中和步骤（b）的硫化烷基羟基芳族化合物以提供硫化烷基羟基芳族化合物的盐，其中硫化烷基羟基芳族化合物的高碱性盐含有少于约2％的未硫化烷基羟基芳族化合物及其未硫化的金属盐。

9. 发明授权

US08188020B2 Lubricating oil composition containing an alkali metal detergent 有权
标题翻译：含有碱金属洗涤剂的润滑油组合物
公开(公告)号：US08188020B2
公开(公告)日：2012-05-29
申请号：US10744871
申请日：2003-12-22
申请人： Jean-Louis Le Coent , Amedee Guellec , Eugene E. Spala
发明人： Jean-Louis Le Coent , Amedee Guellec , Eugene E. Spala
IPC分类号： C07C51/15 , C10M131/00
CPC分类号： C10M159/22 , C10M129/44 , C10M129/93 , C10M159/20 , C10M169/04 , C10M169/045 , C10M2207/128 , C10M2207/129 , C10M2207/262 , C10M2215/28 , C10M2219/046 , C10M2223/045 , C10N2230/04 , C10N2230/10 , C10N2240/102
摘要： The present invention provides overbased detergents as lubricating additives effective for the lubrication of mechanical components in land and marine engines, such as, for example, hydraulic systems, transmissions, two-stroke and four-stroke vehicular engines, and trunk piston and two-stroke crosshead marine engines.
摘要翻译：本发明提供了高碱性清洁剂作为润滑添加剂，其有效用于陆地和船用发动机中的机械部件的润滑，例如液压系统，变速器，二冲程和四冲程车辆发动机，以及行李箱活塞和二冲程十字头船用发动机。

10. 发明申请

US20090170737A1 LOW TEMPERATURE PERFORMANCE LUBRICATING OIL DETERGENTS AND METHOD OF MAKING THE SAME 有权
标题翻译：低温性能润滑油清洗剂及其制备方法
公开(公告)号：US20090170737A1
公开(公告)日：2009-07-02
申请号：US12339894
申请日：2008-12-19
申请人： Curt B. Campbell , Gilles P. Sinquin , Eugene E. Spala , Gilbert R. Chapon
发明人： Curt B. Campbell , Gilles P. Sinquin , Eugene E. Spala , Gilbert R. Chapon
IPC分类号： C10M159/22 , C07C65/03 , C07C39/06
CPC分类号： C10M159/20 , C10M159/22 , C10M2203/1025 , C10M2207/262 , C10M2215/28 , C10M2219/044 , C10M2223/045 , C10N2210/06 , C10N2220/028 , C10N2230/02 , C10N2230/04 , C10N2240/02 , C10N2240/04 , C10N2270/00 , C10N2220/022 , C10N2260/00 , C10N2260/14 , C10N2210/02
摘要： A carboxylate detergent prepared by the process comprising (a) alkylating a hydroxyaromatic compound with at least one normal alpha olefin having from about 12 to about 30 carbon atoms per molecule that has been isomerized to obtain an isomerized alpha olefin having 15-98 wt % branching and a residual alpha olefin content of between from about 0.1 to about 30 wt %, thereby producing an alkylated hydroxyaromatic compound; (b) neutralizing the resulting alkylated hydroxyaromatic compound with an alkali metal base; (c) carbonating the alkali metal salt from step (b) with carbon dioxide; (d) acidifying the salt produced in step (c); and (e) overbasing the resulting alkylated hydroxyaromatic carboxylic acid.
摘要翻译：通过该方法制备的羧酸盐洗涤剂包括（a）使羟基芳族化合物与至少一种正构的α-烯烃在每分子中具有约12至约30个碳原子进行烷基化，所述α-烯烃已被异构化，以获得具有15-98重量％支化的异构化α-烯烃和约0.1至约30重量％之间的残余α-烯烃含量，从而产生烷基化羟基芳族化合物; （b）用碱金属碱中和得到的烷基化羟基芳族化合物; （c）用二氧化碳将步骤（b）的碱金属盐碳化; （d）酸化步骤（c）中产生的盐; 和（e）使得到的烷基化羟基芳族羧酸过碱化。

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