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1. 发明申请

US20160102043A1 PROCESS FOR PRODUCTION OF METHACRYLIC ACID ESTERS 审中-公开
标题翻译：生产甲基丙烯酸酯的方法
公开(公告)号：US20160102043A1
公开(公告)日：2016-04-14
申请号：US14889554
申请日：2014-06-17
申请人： ROHM AND HAAS COMPANY
发明人： Andrew M. Lemonds , Jinsuo Xu
IPC分类号： C07C67/327 , C07C67/08 , B01J23/04 , C07C67/54 , C07C231/10 , C07C67/317 , C07C51/09
CPC分类号： C07C67/327 , B01J21/08 , B01J23/04 , C07C51/09 , C07C67/08 , C07C67/317 , C07C67/54 , C07C231/10 , C07C69/54
摘要： A method for producing α-, β-unsaturated carboxylic acid esters in high yield from acetone cyanohydrin and sulfuric acid through the separation and concurrent catalytic conversion of reaction side products to additional α-, β-unsaturated carboxylic acid ester product. The catalyst comprises at least one Group IA element, and boron as a promoter, on a porous support.
摘要翻译：通过将反应副产物分离并同时催化转化成另外的α-，β-不饱和羧酸酯产物，从丙酮氰醇和硫酸以高产率生产α-，β-不饱和羧酸酯的方法。在多孔载体上，催化剂包含至少一种IA族元素和硼作为助催化剂。

2. 发明授权

US10723685B2 Process for preparing methacrolein 有权
公开(公告)号：US10723685B2
公开(公告)日：2020-07-28
申请号：US16615841
申请日：2018-05-24
申请人： Rohm and Haas Company
发明人： Reetam Chakrabarti , Dmitry A. Krapchetov , Mark A. Silvano , Jinsuo Xu
IPC分类号： C07C45/82 , C07C47/22 , C07C45/75
摘要： Provided is a process for preparing methacrolein which maximizes capture of methanol. Also provided are processes for producing methacrylic acid and methyl methacrylate.

3. 发明申请

US20150141694A1 PROCESS FOR PRODUCTION OF METHACRYLIC ACID ESTERS 有权
标题翻译：生产甲基丙烯酸酯的方法
公开(公告)号：US20150141694A1
公开(公告)日：2015-05-21
申请号：US14398767
申请日：2013-05-21
申请人： Rohm and Haas Company
发明人： Andrew M. Lemonds , Jinsuo Xu
IPC分类号： C07C67/327
CPC分类号： C07C67/327 , B01J23/04 , B01J27/182 , B01J35/1019 , B01J35/1023 , B01J35/1038 , B01J35/1042 , B01J35/1047 , B01J35/1061 , B01J37/0236 , B01J37/28 , C07C69/54
摘要： A method for producing α-, β-unsaturated carboxylic acid esters in high yield from reaction by-product streams via the catalytic conversion of the by-products to additional α-, β-unsaturated carboxylic acid ester product. The catalyst comprises cesium, and phosphorous as a promoter, on a porous support.
摘要翻译：通过将副产物催化转化成另外的α-，β-不饱和羧酸酯产物，从反应副产物流中以高产率生产α-，β-不饱和羧酸酯的方法。在多孔载体上，催化剂包含铯和磷作为助催化剂。

4. 发明申请

US20180244597A1 METHOD OF DETERMINING THE INERTNESS OF MATERIALS FOR USE IN MONOMER PRODUCTION 审中-公开
公开(公告)号：US20180244597A1
公开(公告)日：2018-08-30
申请号：US15753381
申请日：2016-08-22
申请人： Rohm and Haas Company
发明人： Jinsuo Xu
IPC分类号： C07C45/35 , C07C51/25 , G01N33/22 , G01N30/86
CPC分类号： C07C45/35 , C07C51/252 , G01N30/8675 , G01N33/227 , G01N33/442 , C07C47/22 , C07C57/04
摘要： A process for selecting an inert material for use in monomer production regarding the formation of heavy by-products during the reaction of propylene to acrolein and acrylic acid.

5. 发明申请

US20180237373A1 METHOD OF DETERMINING THE INERTNESS OF MATERIALS FOR USE IN MONOMER PRODUCTION 审中-公开
公开(公告)号：US20180237373A1
公开(公告)日：2018-08-23
申请号：US15753379
申请日：2016-08-22
申请人： Rohm and Haas Company
发明人： Jinsuo Xu
IPC分类号： C07C51/25 , C07C45/35 , G01N30/86
CPC分类号： C07C51/252 , C07C45/35 , G01N30/8675 , G01N33/442 , C07C47/22 , C07C57/04
摘要： A method of determining the inertness of a material regarding the formation of heavy by-products during the reaction of propylene to acrolein and acrylic acid.

6. 发明申请

US20220274905A1 PRODUCTION OF ACROLEIN OR ACRYLIC ACID FROM ALLYL ALCOHOL WITH HIGH YIELD AND LOW IMPURITY 有权
公开(公告)号：US20220274905A1
公开(公告)日：2022-09-01
申请号：US17632653
申请日：2020-09-10
申请人： Rohm and Haas Company
发明人： Jinsuo Xu
IPC分类号： C07C45/38 , C07C51/25
摘要： Acrolein is produced by selectively oxidizing allyl alcohol over a first mixed metal oxide catalyst in the presence of oxygen in the vapor phase. The first mixed metal oxide catalyst comprises oxides of molybdenum and bismuth. Acrylic acid is produced by selectively oxidizing the acrolein over a second mixed metal oxide catalyst in the presence of oxygen in the vapor phase. The second mixed metal oxide catalyst has a different composition from the first mixed metal oxide catalyst.

7. 发明申请

US20220193640A1 ALDEHYDE BYPRODUCT REDUCTION IN ACRYLIC ACID PRODUCTION USING HIGHLY ACTIVE AND ELECTIVE CATALYSTS 有权
公开(公告)号：US20220193640A1
公开(公告)日：2022-06-23
申请号：US17601751
申请日：2020-04-20
申请人： Dow Global Technologies LLC , Rohm and Haas Company
发明人： Jinsuo Xu , Nelson I. Quiros , Daniel A. Bors , Joseph F. Dewilde
IPC分类号： B01J23/652 , B01J23/00 , B01J23/28 , C07C51/16 , C07C45/28
摘要： A catalyst composition comprises an acrolein-oxidizing catalyst comprising a mixed metal oxide catalyst of general formula (1): MoVaA1bA2cA3dOm (I) in which A1 comprises at least one element selected from the group consisting of W and Cu; A2 comprises at least one element selected from the group consisting of Sb, Fe, and Nb; A3 comprises at least one element selected from the group consisting of Y, Ti, Zr, Hf, Ta, Cr, Mn, Re, Ru, Co, Rh, Ir, Ni, Pd, Pt, Ag, Au, Zn, B, Al, Ga, In, Ge, Sn, Si, Te, Pb, P, As, Bi, Se, rare earth elements, alkaline elements, and alkaline earth elements; a ranges from 0.01 to 1.0; b ranges from 0.01 to 1.5; c ranges from 0 to 1.5; d ranges from 0 to 1.0; and m is dependent on the oxidation state of the other elements. The catalyst composition further comprises a finishing catalyst comprising a mixed metal oxide catalyst of general formula (II): MoVwNbxX1yX2zOn (II) in which X1 comprises at least one element selected from the group consisting of Te and Sb; X2 comprises at least one an element selected from the group consisting of Y, Ti, Zr, Hf, Nb, Ta, Cr, Mn, Re, Fe, Ru, Co, Rh, Ir, Ni, Pd, Pt, Ag, Au, Zn, B, Al, Ga, In, Ge, Sn, Pb, P, As, Bi, Se, rare earth elements and alkaline earth elements; w ranges from 0.01 to 1.0; x ranges from 0.01 to 1.0; y ranges from 0.01 to 1.0; z ranges from 0 to 1.0; and n is depended on the oxidation state of the other elements. The finishing catalyst does not contain W or Cu, and has an X-ray diffraction pattern showing an orthorhombic phase as the major crystal phase with main peaks with 2θ at 6.7°, 7.8°, 22.1°, and 27.2°. The acrolein-oxidizing catalyst has a different chemical composition than the finishing catalyst. A process for producing acrylic acid is also disclosed.

8. 发明授权

US11236034B2 Method for preparing acrylic acid 有权
公开(公告)号：US11236034B2
公开(公告)日：2022-02-01
申请号：US16980936
申请日：2019-02-21
申请人： Rohm and Haas Company
发明人： Donald A. Ebert , Timothy Allen Hale , Brian Robert Keyes , Justin Rose , Jinsuo Xu
IPC分类号： C07C51/25 , C07C57/04
摘要： Provided is a process for preparing acrylic acid comprising (1) preparing acrolein by catalytic gas phase oxidation comprising (a) providing a reaction gas comprising (i) 5 to 10 mol % propylene, (ii) 0.02 to 0.75 mol % propane, and (iii) 0.25 to 1.9 mol % of a fuel mixture comprising at least one of methane and ethane, wherein the molar ratio of the total amount of propane, methane, and ethane to the total amount of propylene is from 0.01:1 to 0.25:1, (b) contacting the reaction gas with a first mixed metal oxide catalyst to form a mixture comprising acrolein, wherein the first mixed metal oxide catalyst comprises one or more of molybdenum, bismuth, cobalt, and iron, and (2) contacting the acrolein mixture with a second mixed metal oxide catalyst to form a mixture comprising acrylic acid, wherein the second mixed metal oxide catalyst comprises one or more of molybdenum, vanadium, tungsten, copper, and antimony.

9. 发明授权

US10968158B2 Method of determining the inertness of materials for use in monomer production 有权
公开(公告)号：US10968158B2
公开(公告)日：2021-04-06
申请号：US15753379
申请日：2016-08-22
申请人： Rohm and Haas Company
发明人： Jinsuo Xu
IPC分类号： C07C51/25 , C07C45/35 , G01N30/66 , G01N33/44 , G01N31/10 , G01N30/86
摘要： A method of determining the inertness of a material regarding the formation of heavy by-products during the reaction of propylene to acrolein and acrylic acid.

10. 发明授权

US10577299B2 Methods for using macroporous inert materials in monomer production 有权
公开(公告)号：US10577299B2
公开(公告)日：2020-03-03
申请号：US16092094
申请日：2017-04-17
申请人： Rohm and Haas Company
发明人： Jinsuo Xu
IPC分类号： C07C51/25 , C07C47/22 , C07C57/04 , C07C45/33 , B01J23/31 , C07C45/34
摘要： The present invention provides methods for monomer production, for example, acrylic acid, wherein the methods comprise oxidizing one or more reactant gases, for example, propylene, in a fixed bed reactor, preferably, two fixed bed reactors, in the presence of oxygen and a mixed metal oxide catalyst to form an oxidized gaseous mixture and, at any point in the oxidizing, feeding or flowing the one or more reactant gases or the oxidized gaseous mixture through an inert macroporous material that has a pore volume of from 0.2 cm3/g to 2.0 cm3/g, a surface area of from 0.01 to 0.6 m2/g, and wherein from 30 to 98 wt. % of the total pore volume in the inert macroporous material has a pore diameter of at least 100 μm.

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