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1. 发明申请

US20110256197A1 Preparation of Metal Nanowire Decorated Carbon Allotropes 失效
标题翻译：金属纳米线装饰碳同素异形体的制备
公开(公告)号：US20110256197A1
公开(公告)日：2011-10-20
申请号：US13082734
申请日：2011-04-08
申请人： Robin E. Southward , Donavon Mark Delozier , Kent A. Watson , Joseph G. Smith , Sayata Ghose , John W. Connell
发明人： Robin E. Southward , Donavon Mark Delozier , Kent A. Watson , Joseph G. Smith , Sayata Ghose , John W. Connell
IPC分类号： B05D5/00 , H01B1/12 , H01B1/20 , B01J21/18 , B01J37/02 , B01J31/06 , A01N25/00 , A01N59/16 , C09K5/00 , B01J37/16 , B82Y40/00 , B82Y30/00
CPC分类号： C09K5/14 , B22F1/0025 , B22F9/24 , B22F2998/00 , B22F2999/00 , B82Y30/00 , B82Y40/00 , C01B32/15 , C01B32/152 , C01B32/158 , C01B32/20 , C01B32/225 , C08J5/005 , C22C1/058 , C22C1/1084 , C22C26/00 , C22C2026/001 , C22C2026/002 , B22F1/025
摘要： In the method of embodiments of the invention, the metal seeded carbon allotropes are reacted in solution forming zero valent metallic nanowires at the seeded sites. A polymeric passivating reagent, which selects for anisotropic growth is also used in the reaction to facilitate nanowire formation. The resulting structure resembles a porcupine, where carbon allotropes have metallic wires of nanometer dimensions that emanate from the seed sites on the carbon allotrope. These sites are populated by nanowires having approximately the same diameter as the starting nanoparticle diameter.
摘要翻译：在本发明实施方案的方法中，金属接种碳同素异形体在形成零价金属纳米线的溶液中在接种部位反应。用于各向异性生长的聚合物钝化试剂也用于反应以促进纳米线形成。所得结构类似于豪猪，其中碳同素异形体具有从碳同素异形体上的种子位点发出的具有纳米尺寸的金属线。这些位点由具有与起始纳米颗粒直径大致相同直径的纳米线填充。

2. 发明授权

US08703235B2 Preparation of metal nanowire decorated carbon allotropes 失效
标题翻译：金属纳米线装饰碳同素异形体的制备
公开(公告)号：US08703235B2
公开(公告)日：2014-04-22
申请号：US13082734
申请日：2011-04-08
申请人： Robin E. Southward , Donavon Mark Delozier , Kent A. Watson , Joseph G. Smith , Sayata Ghose , John W. Connell
发明人： Robin E. Southward , Donavon Mark Delozier , Kent A. Watson , Joseph G. Smith , Sayata Ghose , John W. Connell
IPC分类号： B05D7/00 , B32B5/16
CPC分类号： C09K5/14 , B22F1/0025 , B22F9/24 , B22F2998/00 , B22F2999/00 , B82Y30/00 , B82Y40/00 , C01B32/15 , C01B32/152 , C01B32/158 , C01B32/20 , C01B32/225 , C08J5/005 , C22C1/058 , C22C1/1084 , C22C26/00 , C22C2026/001 , C22C2026/002 , B22F1/025
摘要： In the method of embodiments of the invention, the metal seeded carbon allotropes are reacted in solution forming zero valent metallic nanowires at the seeded sites. A polymeric passivating reagent, which selects for anisotropic growth is also used in the reaction to facilitate nanowire formation. The resulting structure resembles a porcupine, where carbon allotropes have metallic wires of nanometer dimensions that emanate from the seed sites on the carbon allotrope. These sites are populated by nanowires having approximately the same diameter as the starting nanoparticle diameter.
摘要翻译：在本发明实施方案的方法中，金属接种碳同素异形体在形成零价金属纳米线的溶液中在接种部位反应。用于各向异性生长的聚合物钝化试剂也用于反应以促进纳米线形成。所得结构类似于豪猪，其中碳同素异形体具有从碳同素异形体上的种子位点发出的具有纳米尺寸的金属线。这些位点由具有与起始纳米颗粒直径大致相同直径的纳米线填充。

3. 发明授权

US08790773B2 Tailorable dielectric material with complex permittivity characteristics 有权
标题翻译：具有复介电常数特性的可调电介质材料
公开(公告)号：US08790773B2
公开(公告)日：2014-07-29
申请号：US12174360
申请日：2008-07-16
申请人： Kenneth L. Dudley , Holly A Elliott , John W. Connell , Joseph G. Smith , Sayata Ghose , Kent A. Watson , Donavon Mark Delozier
发明人： Kenneth L. Dudley , Holly A Elliott , John W. Connell , Joseph G. Smith , Sayata Ghose , Kent A. Watson , Donavon Mark Delozier
IPC分类号： B32B5/16 , C08K3/08
CPC分类号： C08K3/08 , B82Y30/00 , C08K2201/011
摘要： A dielectric material includes a network of nanosubstrates, such as but not limited to nanotubes, nanosheets, or other nanomaterials or nanostructures, a polymer base material or matrix, and nanoparticles constructed at least partially of an elemental metal. The network has a predetermined nanosubstrate loading percentage by weight with respect to a total weight of the dielectric material, and a preferential or predetermined longitudinal alignment with respect to an orientation of an incident electrical field. A method of forming the dielectric material includes depositing the metal-based nanoparticles onto the nanosubstrates and subsequently mixing these with a polymer matrix. Once mixed, alignment can be achieved by melt extrusion or a similar mechanical shearing process. Alignment of the nanosubstrate may be in horizontal or vertical direction with respect to the orientation of an incident electrical field.
摘要翻译：电介质材料包括纳米基层网络，例如但不限于纳米管，纳米片或其它纳米材料或纳米结构，聚合物基材或基体，以及至少部分由元素金属构成的纳米颗粒。网络具有相对于电介质材料的总重量的预定的纳米基质载荷百分比，以及相对于入射电场的取向的优选或预定的纵向对准。形成电介质材料的方法包括将金属基纳米颗粒沉积到纳米基板上，随后将其与聚合物基体混合。一旦混合，可以通过熔体挤出或类似的机械剪切工艺来实现对准。纳米基板的对准可以相对于入射电场的取向在水平或垂直方向上。

4. 发明申请

US20090022977A1 Combination structural support and thermal protection system 有权
标题翻译：组合结构支撑和热保护系统
公开(公告)号：US20090022977A1
公开(公告)日：2009-01-22
申请号：US12174360
申请日：2008-07-16
申请人： Kenneth L. Dudley , Holly A. Elliott , John W. Connell , Joseph G. Smith , Sayata Ghose , Kent A. Watson , Donavon Mark Delozier
发明人： Kenneth L. Dudley , Holly A. Elliott , John W. Connell , Joseph G. Smith , Sayata Ghose , Kent A. Watson , Donavon Mark Delozier
IPC分类号： B32B5/16 , C08K3/08
CPC分类号： C08K3/08 , B82Y30/00 , C08K2201/011
摘要： A dielectric material includes a network of nanosubstrates, such as but not limited to nanotubes, nanosheets, or other nanomaterials or nanostructures, a polymer base material or matrix, and nanoparticles constructed at least partially of an elemental metal. The network has a predetermined nanosubstrate loading percentage by weight with respect to a total weight of the dielectric material, and a preferential or predetermined longitudinal alignment with respect to an orientation of an incident electrical field. A method of forming the dielectric material includes depositing the metal-based nanoparticles onto the nanosubstrates and subsequently mixing these with a polymer matrix. Once mixed, alignment can be achieved by melt extrusion or a similar mechanical shearing process. Alignment of the nanosubstrate may be in horizontal or vertical direction with respect to the orientation of an incident electrical field.
摘要翻译：电介质材料包括纳米基层网络，例如但不限于纳米管，纳米片或其它纳米材料或纳米结构，聚合物基材或基体，以及至少部分由元素金属构成的纳米颗粒。网络具有相对于电介质材料的总重量的预定的纳米基质载荷百分比，以及相对于入射电场的取向的优选或预定的纵向对准。形成电介质材料的方法包括将金属基纳米颗粒沉积到纳米基板上，随后将其与聚合物基体混合。一旦混合，可以通过熔体挤出或类似的机械剪切工艺来实现对准。纳米基板的对准可以相对于入射电场的取向在水平或垂直方向上。

5. 发明授权

US07704553B2 Depositing nanometer-sized particles of metals onto carbon allotropes 有权
标题翻译：将纳米尺寸的金属颗粒沉积在碳同素异形体上
公开(公告)号：US07704553B2
公开(公告)日：2010-04-27
申请号：US11710386
申请日：2007-02-23
申请人： Kent A. Watson , Michael J. Fallbach , Sayata Ghose , Joseph G. Smith , Donavon M. Delozier , John W. Connell
发明人： Kent A. Watson , Michael J. Fallbach , Sayata Ghose , Joseph G. Smith , Donavon M. Delozier , John W. Connell
IPC分类号： B05D7/00 , B05D3/02
CPC分类号： C08J5/005 , B22F1/0018 , B22F9/20 , B22F2999/00 , B82Y30/00 , B82Y40/00 , C01B32/05 , C01B32/152 , C01B32/168 , C01B32/20 , C01B32/25 , C01B2202/02 , C01B2202/06 , C22C2026/001 , C22C2026/002 , Y10T428/31678 , B22F9/04 , B22F2203/11
摘要： A process for depositing nanometer-sized metal particles onto a substrate in the absence of aqueous solvents, organic solvents, and reducing agents, and without any required pre-treatment of the substrate, includes preparing an admixture of a metal compound and a substrate by dry mixing a chosen amount of the metal compound with a chosen amount of the substrate; and supplying energy to the admixture in an amount sufficient to deposit zero valance metal particles onto the substrate. This process gives rise to a number of deposited metallic particle sizes which may be controlled. The compositions prepared by this process are used to produce polymer composites by combining them with readily available commodity and engineering plastics. The polymer composites are used as coatings, or they are used to fabricate articles, such as free-standing films, fibers, fabrics, foams, molded and laminated articles, tubes, adhesives, and fiber reinforced articles. These articles are well-suited for many applications requiring thermal conductivity, electrical conductivity, antibacterial activity, catalytic activity, and combinations thereof.
摘要翻译：在不含水溶剂，有机溶剂和还原剂的情况下将纳米尺寸金属颗粒沉积到基底上的方法，并且不需要对基底进行任何必要的预处理，包括通过干燥制备金属化合物和基底的混合物将选定量的金属化合物与选定量的底物混合; 并且以足以将零价金属颗粒沉积到基底上的量向混合物供应能量。该方法产生可以控制的多个沉积的金属颗粒尺寸。通过该方法制备的组合物用于通过将它们与容易获得的商品和工程塑料组合来生产聚合物复合材料。聚合物复合材料用作涂层，或者它们用于制造制品，例如自立膜，纤维，织物，泡沫，模制和层压制品，管，粘合剂和纤维增强制品。这些制品非常适用于需要导热性，导电性，抗菌活性，催化活性及其组合的许多应用。

6. 发明授权

US08508413B2 Antenna with dielectric having geometric patterns 有权
标题翻译：具有几何图案的电介质天线
公开(公告)号：US08508413B2
公开(公告)日：2013-08-13
申请号：US13082839
申请日：2011-04-08
申请人： Kenneth L. Dudley , Holly A. Elliott , Robin L. Cravey , John W. Connell , Sayata Ghose , Kent A. Watson , Joseph G. Smith, Jr.
发明人： Kenneth L. Dudley , Holly A. Elliott , Robin L. Cravey , John W. Connell , Sayata Ghose , Kent A. Watson , Joseph G. Smith, Jr.
IPC分类号： H01Q1/38
CPC分类号： H01Q1/28 , H01Q1/38 , H01Q1/422
摘要： An antenna includes a ground plane, a dielectric disposed on the ground plane, and an electrically-conductive radiator disposed on the dielectric. The dielectric includes at least one layer of a first dielectric material and a second dielectric material that collectively define a dielectric geometric pattern, which may comprise a fractal geometry. The radiator defines a radiator geometric pattern, and the dielectric geometric pattern is geometrically identical, or substantially geometrically identical, to the radiator geometric pattern.
摘要翻译：天线包括接地平面，设置在接地平面上的电介质和设置在电介质上的导电散热器。电介质包括至少一层第一电介质材料和第二电介质材料，它们共同限定电介质几何图形，其可以包括分形几何形状。散热器限定散热器几何图案，电介质几何图案在几何上与散热器几何图案相同或基本上几何相同。

7. 发明授权

US07723464B2 Aromatic/aliphatic diamine derivatives for advanced compositions and polymers 有权
标题翻译：用于先进组合物和聚合物的芳族/脂族二胺衍生物
公开(公告)号：US07723464B2
公开(公告)日：2010-05-25
申请号：US11674321
申请日：2007-02-13
申请人： Donovan M. Delozier , Kent A. Watson , John W. Connell , Joseph G. Smith, Jr.
发明人： Donovan M. Delozier , Kent A. Watson , John W. Connell , Joseph G. Smith, Jr.
IPC分类号： C08G59/10 , H01L51/00
CPC分类号： C07C211/61 , C07C2603/18
摘要： Novel compositions of matter comprise certain derivatives of 9,9-dialkyl fluorene diamine (AFDA). The resultant compositions, whether compositions of matter or monomers that are subsequently incorporated into a polymer, are unique and useful in a variety of applications. Useful applications of AFDA-based material include heavy ion radiation shielding components and components of optical and electronic devices.
摘要翻译：物质的新型组合物包含9,9-二烷基芴二胺（AFDA）的某些衍生物。所得组合物，无论是随后掺入聚合物中的物质或单体的组合物在各种应用中是独特的和有用的。 AFDA材料的有用应用包括重离子辐射屏蔽组件和光学和电子设备的组件。

8. 发明申请

US20100078600A1 Electrically Conductive, Optically Transparent Polymer/Carbon Nanotube Composites And Process For Preparation Thereof 有权
标题翻译：导电，光学透明聚合物/碳纳米管复合材料及其制备方法
公开(公告)号：US20100078600A1
公开(公告)日：2010-04-01
申请号：US12550431
申请日：2009-08-31
申请人： John W. Connell , Joseph G. Smith , Joycelyn S. Harrison , Cheol Park , Kent A. Watson , Zoubeida Ounaies
发明人： John W. Connell , Joseph G. Smith , Joycelyn S. Harrison , Cheol Park , Kent A. Watson , Zoubeida Ounaies
IPC分类号： H01B1/24
CPC分类号： B82Y10/00 , B82Y30/00 , C08F2/44 , C08G73/10 , C08G73/1039 , C08G73/1071 , C08K5/00 , C08K7/24 , C08K2201/011 , C08L71/123 , C09J11/04 , H01B1/24 , Y10T428/25 , Y10T428/29 , Y10T428/2904 , Y10T428/2913 , Y10T428/2918 , Y10T428/2975 , C08L71/12
摘要： The present invention is directed to the effective dispersion of carbon nanotubes (CNTs) into polymer matrices. The nanocomposites are prepared using polymer matrices and exhibit a unique combination of properties, most notably, high retention of optical transparency in the visible range (i.e., 400-800 nm), electrical conductivity, and high thermal stability. By appropriate selection of the matrix resin, additional properties such as vacuum ultraviolet radiation resistance, atomic oxygen resistance, high glass transition (Tg) temperatures, and excellent toughness can be attained. The resulting nanocomposites can be used to fabricate or formulate a variety of articles such as coatings on a variety of substrates, films, foams, fibers, threads, adhesives and fiber coated prepreg. The properties of the nanocomposites can be adjusted by selection of the polymer matrix and CNT to fabricate articles that possess high optical transparency and antistatic behavior.
摘要翻译：本发明涉及碳纳米管（CNT）在聚合物基质中的有效分散。使用聚合物基质制备纳米复合材料，并且表现出独特的性质组合，最显着的是在可见光范围（即400-800nm）中高保留光学透明度，导电性和高热稳定性。通过适当选择基体树脂，可以获得诸如真空紫外线辐射电阻，原子氧电阻，高玻璃化转变温度（Tg）等优异的韧性等附加特性。所得的纳米复合材料可用于制造或配制各种制品，例如各种基材，薄膜，泡沫，纤维，线，粘合剂和纤维涂层预浸料上的涂层。可以通过选择聚合物基质和CNT来调节具有高光学透明度和抗静电性能的制品来调节纳米复合材料的性能。

9. 发明授权

US07109287B2 Space environmentally durable polyimides and copolyimides 失效
标题翻译：空间环保的聚酰亚胺和共聚酰亚胺
公开(公告)号：US07109287B2
公开(公告)日：2006-09-19
申请号：US10988407
申请日：2004-11-08
申请人： John W. Connell , Joseph G. Smith, Jr. , Paul M. Hergenrother , Kent A. Watson , Craig M. Thompson
发明人： John W. Connell , Joseph G. Smith, Jr. , Paul M. Hergenrother , Kent A. Watson , Craig M. Thompson
IPC分类号： C08G69/26
CPC分类号： C08G73/1071 , C08G73/10 , C08G73/1014 , C08G73/1039 , C08G73/1057 , C08G73/1067
摘要： Polyimides displaying low color in thin films, atomic oxygen resistance, vacuum ultraviolet radiation resistance, solubility in organic solvents in the imide form, high glass transition (Tg) temperatures, and high thermal stability are provided. The poly(amide acid)s, copoly(amide acid)s, polyimides and copolyimides are prepared by the reaction of stoichiometric ratios of an aromatic dianhydride with diamines which contain phenylphosphine oxide groups in polar aprotic solvents. Controlled molecular weight oligomeric (amide acid)s and imides can be prepared by offsetting the stoichiometry according to the Carothers equation using excess diamine and endcapping with aromatic anhydrides. The polyimide materials can be processed into various material forms such as thin films, fibers, foams, threads, adhesive film, coatings, dry powders, and fiber coated prepreg, and uses include thin film membranes on antennas, second-surface mirrors, thermal optical coatings, and multi-layer thermal insulation (MLI) blanket materials.
摘要翻译：提供在薄膜中显示低色的聚酰亚胺，原子氧电阻，真空紫外线辐射抗性，在酰亚胺形式的有机溶剂中的溶解度，高玻璃化转变温度和高热稳定性。聚（酰胺酸），共聚（酰胺酸），聚酰亚胺和共聚酰亚胺通过芳族二酐与极性非质子溶剂中含有苯基氧化膦基团的二胺的化学计量比的反应来制备。控制分子量的低聚（酰胺酸）和酰亚胺可以通过使用过量的二胺和用芳族酸酐封端根据Carothers方程来抵消化学计量来制备。聚酰亚胺材料可以加工成各种材料形式，如薄膜，纤维，泡沫，线，粘合膜，涂料，干粉和纤维涂层预浸料，其中包括天线薄膜，第二面反光镜，热光学涂层和多层保温（MLI）覆层材料。

10. 发明授权

US07906043B2 Electrically conductive, optically transparent polymer/carbon nanotube composites and process for preparation thereof 有权
标题翻译：导电，光学透明的聚合物/碳纳米管复合材料及其制备方法
公开(公告)号：US07906043B2
公开(公告)日：2011-03-15
申请号：US12550431
申请日：2009-08-31
申请人： John W. Connell , Joseph G. Smith , Joycelyn S. Harrison , Cheol Park , Kent A. Watson , Zoubeida Ounaies
发明人： John W. Connell , Joseph G. Smith , Joycelyn S. Harrison , Cheol Park , Kent A. Watson , Zoubeida Ounaies
IPC分类号： H01B1/04 , H01B1/24 , C08K3/04 , B32B9/00
CPC分类号： B82Y10/00 , B82Y30/00 , C08F2/44 , C08G73/10 , C08G73/1039 , C08G73/1071 , C08K5/00 , C08K7/24 , C08K2201/011 , C08L71/123 , C09J11/04 , H01B1/24 , Y10T428/25 , Y10T428/29 , Y10T428/2904 , Y10T428/2913 , Y10T428/2918 , Y10T428/2975 , C08L71/12
摘要： The present invention is directed to the effective dispersion of carbon nanotubes (CNTs) into polymer matrices. The nanocomposites are prepared using polymer matrices and exhibit a unique combination of properties, most notably, high retention of optical transparency in the visible range (i.e., 400-800 nm), electrical conductivity, and high thermal stability. By appropriate selection of the matrix resin, additional properties such as vacuum ultraviolet radiation resistance, atomic oxygen resistance, high glass transition (Tg) temperatures, and excellent toughness can be attained. The resulting nanocomposites can be used to fabricate or formulate a variety of articles such as coatings on a variety of substrates, films, foams, fibers, threads, adhesives and fiber coated prepreg. The properties of the nanocomposites can be adjusted by selection of the polymer matrix and CNT to fabricate articles that possess high optical transparency and antistatic behavior.
摘要翻译：本发明涉及碳纳米管（CNT）在聚合物基质中的有效分散。使用聚合物基质制备纳米复合材料，并且表现出独特的性能组合，最显着的是在可见光范围（即400-800nm）中的高保留光学透明度，导电性和高热稳定性。通过适当选择基体树脂，可以获得诸如真空紫外线辐射电阻，原子氧电阻，高玻璃化转变温度（Tg）等优异的韧性等附加特性。所得的纳米复合材料可用于制造或配制各种制品，例如各种基材，薄膜，泡沫，纤维，线，粘合剂和纤维涂层预浸料上的涂层。可以通过选择聚合物基质和CNT来调节具有高光学透明度和抗静电性能的制品来调节纳米复合材料的性能。

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