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1. 发明授权

US5194067A Recovery of hydrogen peroxide 失效
标题翻译：回收过氧化氢
公开(公告)号：US5194067A
公开(公告)日：1993-03-16
申请号：US905979
申请日：1992-06-29
申请人： Rajendra S. Albal , Robert N. Cochran , David W. Leyshon , Lawrence M. Candela
发明人： Rajendra S. Albal , Robert N. Cochran , David W. Leyshon , Lawrence M. Candela
IPC分类号： B01D11/04 , C01B15/013 , C01B15/026 , C07C45/39 , C07C45/80 , C07D20060101 , C07D265/32 , C07D279/12 , C07D413/04 , C07D413/06 , C07D413/14
CPC分类号： C07C45/39 , C01B15/013 , C01B15/026 , C07C45/80
摘要： A process is provided whereby the hydrogen peroxide-containing oxidate from methyl benzyl alcohol oxidation is extracted with water and with ethyl benzene extractive solvent and an aqueous hydrogen peroxide phase is separated from an ethyl benzene solvent phase which also contains methyl benzyl alcohol and acetophenone, the improvement being that ethyl benzene is introduced into the extraction zone below the point of introduction of the oxidate, thus avoiding the possibility of formation of an aqueous hydrogen peroxide phase concentrated to a hazardous degree in hydrogen peroxide in the extraction zone.

2. 发明授权

US4975266A Production of hydrogen peroxide 失效
标题翻译：生产过氧化氢
公开(公告)号：US4975266A
公开(公告)日：1990-12-04
申请号：US457662
申请日：1989-12-27
申请人： Rajendra S. Albal , Robert N. Cochran , Lawrence M. Candela
发明人： Rajendra S. Albal , Robert N. Cochran , Lawrence M. Candela
IPC分类号： C01B15/013 , C01B15/026 , C07C45/39
CPC分类号： C01B15/026 , C01B15/013 , C07C45/39
摘要： Hydrogen peroxide is produced by liquid phase molecular oxygen oxidation of methyl benzyl alcohol. Inhibiting impurities are removed prior to oxidation.
摘要翻译：过氧化氢通过甲基苄醇的液相分子氧氧化产生。在氧化之前除去杂质。

3. 发明授权

US4897252A Production of hydrogen peroxide 失效
标题翻译：生产过氧化氢
公开(公告)号：US4897252A
公开(公告)日：1990-01-30
申请号：US295409
申请日：1989-01-10
申请人： Robert N. Cochran , Lawrence M. Candela
发明人： Robert N. Cochran , Lawrence M. Candela
IPC分类号： A61K8/00 , A61K8/65 , A61K8/66 , A61K8/98 , A61K35/14 , A61K38/22 , A61Q5/00 , C01B15/013 , C01B15/026 , C07C45/39
CPC分类号： C01B15/026 , C01B15/013 , C07C45/39
摘要： Hydrogen peroxide is produced by liquid phase molecular oxygen oxidation of methyl benzyl alcohol, water concentration in the reaction mixture being maintained below 4% by weight, more preferably below 2% by weight, and most preferably below 1% by weight.

4. 发明授权

US5039508A Production of hydrogen peroxide 失效
标题翻译：生产过氧化氢
公开(公告)号：US5039508A
公开(公告)日：1991-08-13
申请号：US554770
申请日：1990-07-19
申请人： Robert N. Cochran , Lawrence M. Candela
发明人： Robert N. Cochran , Lawrence M. Candela
IPC分类号： C01B15/013 , C01B15/026 , C07C45/39
CPC分类号： C01B15/026 , C01B15/013 , C07C45/39
摘要： Hydrogen peroxide is produced by liquid phase molecular oxygen oxidation of methyl benzyl alcohol, the reaction being carried out such that the oxygen absorption rate is 90% or more of the maximum at the reaction conditions and the exit gas oxygen partial pressure is not greater than 3.0, the minimum necessary to establish the maximum oxygen absorption rate.
摘要翻译：过氧化氢是通过甲基苄醇的液相分子氧氧化制备的，反应进行为使得氧气吸收速率在反应条件下为最大值的90％以上，出口气体氧分压不大于3.0 ，建立最大氧吸收速率所需的最小值。

5. 发明授权

US4950794A Ethylbenzene oxidation 失效
标题翻译：乙苯氧化
公开(公告)号：US4950794A
公开(公告)日：1990-08-21
申请号：US356081
申请日：1989-05-24
申请人： Lawrence M. Candela , Robert N. Cochran , Scott H. Sandler
发明人： Lawrence M. Candela , Robert N. Cochran , Scott H. Sandler
IPC分类号： C07C407/00 , C07C27/12 , C07C45/36 , C07C49/78 , C07C409/08
CPC分类号： C07C409/08 , C07C407/00 , C07C45/36
摘要： The oxidation of ethylbenzene to products comprised of ethylbenzene hydroperoxide and acetophenone is modified in order to enhance acetophenone production by reducing the alkali content of the oxidation mixture below 0.1 ppm and by incorporation of 0.05 to 2 wt. % water in the oxidation mixture.

6. 发明授权

US4897085A Recovery of hydrogen peroxide 失效
标题翻译：回收过氧化氢
公开(公告)号：US4897085A
公开(公告)日：1990-01-30
申请号：US295411
申请日：1989-01-10
申请人： Robert N. Cochran , Lawrence M. Candela
发明人： Robert N. Cochran , Lawrence M. Candela
IPC分类号： C01B15/013 , C01B15/026 , C07C45/38 , C07C45/80 , C07C49/78
CPC分类号： C01B15/026 , C01B15/013 , C07C45/80
摘要： A process is provided whereby the hydrogen peroxide-containing oxidate from methyl benzyl alcohol oxidation is contacted with ethyl benzene extractive solvent and a hydrogen peroxide phase is separated from a solvent phase which also contains methyl benzyl alcohol and acetophenone.

7. 发明授权

US06770790B1 Purification of tertiary butyl alcohol 有权
标题翻译：叔丁醇的纯化
公开(公告)号：US06770790B1
公开(公告)日：2004-08-03
申请号：US10688410
申请日：2003-10-17
申请人： Xiangmin Li , Lawrence M. Candela , Yuan-Zhang Han , Andrew P. Kahn
发明人： Xiangmin Li , Lawrence M. Candela , Yuan-Zhang Han , Andrew P. Kahn
IPC分类号： C07C2734
CPC分类号： C07C29/76 , C07C31/10 , C07C31/12
摘要： The invention is a method to purify tertiary butyl alcohol by contact with at least two solid adsorbents comprising aluminum oxide and a large pore zeolite such as zeolite X. The purification method successfully improves product quality and reduces the amount of impurities in the tertiary butyl alcohol.
摘要翻译：本发明是通过与包含氧化铝和大孔沸石如沸石X的至少两种固体吸附剂接触来纯化叔丁醇的方法。纯化方法成功地提高了产品质量并减少了叔丁醇中的杂质量。

8. 发明申请

US20110207973A1 Process for producing allyl alcohol 有权
标题翻译：生产烯丙醇的方法
公开(公告)号：US20110207973A1
公开(公告)日：2011-08-25
申请号：US12660372
申请日：2010-02-25
申请人： Shaw-Chan Lin , Lawrence M. Candela , Andrew P. Kahn , Elizabeth I. Ross-Medgaarden , Gary A. Sawyer
发明人： Shaw-Chan Lin , Lawrence M. Candela , Andrew P. Kahn , Elizabeth I. Ross-Medgaarden , Gary A. Sawyer
IPC分类号： C07C27/02
CPC分类号： C07C29/095 , C07C45/82 , C07C33/03 , C07C47/22
摘要： A process for producing allyl alcohol is disclosed. The process comprises reacting propylene, acetic acid, and oxygen to produce a reaction mixture. The reaction mixture is distilled to produce a vapor stream comprising propylene and a liquid stream comprising allyl acetate, acetic acid, acrolein, and allyl diacetate. The liquid stream is distilled to produce a lights stream comprising acrolein; a side draw comprising allyl acetate, acetic acid, and water; and a bottoms stream comprising acetic acid and allyl diacetate. The bottoms stream is distilled to remove a heavies stream comprising allyl diacetate. The side draw is hydrolyzed to produce allyl alcohol.
摘要翻译：公开了一种生产烯丙醇的方法。该方法包括使丙烯，乙酸和氧气反应以产生反应混合物。将反应混合物蒸馏以产生包含丙烯和包含乙酸烯丙酯，乙酸，丙烯醛和二乙酸烯丙酯的液体料流的蒸气流。将液体流蒸馏以产生包含丙烯醛的光流; 包括乙酸烯丙酯，乙酸和水的侧面拉伸; 和包含乙酸和二乙酸烯丙酯的底部料流。将塔底物流蒸馏以除去包含二乙酸烯丙酯的重质物流。侧面水解产生烯丙醇。

9. 发明申请

US20090187049A1 Production of propylene glycol monoalkyl ether 有权
标题翻译：丙二醇单烷基醚的生产
公开(公告)号：US20090187049A1
公开(公告)日：2009-07-23
申请号：US12009212
申请日：2008-01-17
申请人： Xiangmin Li , Lawrence M. Candela , Mark A. Liepa
发明人： Xiangmin Li , Lawrence M. Candela , Mark A. Liepa
IPC分类号： C07C43/10
CPC分类号： C07C41/03 , C07C41/44 , C07C43/13
摘要： The invention is a process for producing a propylene glycol monoalkyl ether which comprises first reacting propylene oxide and an alcohol in the presence of an alkali or alkaline earth metal alkoxide catalyst to produce an alkoxylation mixture comprising propylene glycol monoalkyl ether; distilling the alkoxylation mixture to produce a first overhead stream comprising propylene oxide and alcohol and a first bottoms stream comprising propylene glycol monoalkyl ether; and then distilling the first bottoms stream to produce purified propylene glycol monoalkyl ether as a second overhead stream. The reaction and/or one or more of the distillation steps occur in the presence of an alkali metal borohydride. The process produces propylene glycol monoalkyl ether with low UV absorbance and reduced carbonyl impurities.
摘要翻译：本发明是一种生产丙二醇单烷基醚的方法，该方法包括首先在碱金属或碱土金属醇盐催化剂存在下使环氧丙烷与醇反应生成包含丙二醇单烷基醚的烷氧基化混合物; 蒸馏所述烷氧基化混合物以产生包含环氧丙烷和醇的第一塔顶物流和包含丙二醇单烷基醚的第一塔底物流; 然后蒸馏第一塔底物流以产生纯化的丙二醇单烷基醚作为第二塔顶馏出物。反应和/或一个或多个蒸馏步骤在碱金属硼氢化物的存在下进行。该方法生产具有低紫外吸收和降低的羰基杂质的丙二醇单烷基醚。

10. 发明授权

US5639928A Dehydration of 1-phenyl ethanol 失效
标题翻译： 1-苯基乙醇脱水
公开(公告)号：US5639928A
公开(公告)日：1997-06-17
申请号：US296769
申请日：1994-08-26
申请人： Walter S. Dubner , Lawrence M. Candela
发明人： Walter S. Dubner , Lawrence M. Candela
IPC分类号： C07C1/24 , C07C7/20 , C07C1/20
CPC分类号： C07C1/24 , C07C7/20
摘要： The present invention relates to the improved liquid phase dehydration of 1-phenyl ethanol to styrene monomer, the improvement comprising the use of a residue formation inhibiting agent during the liquid phase dehydration.
摘要翻译：本发明涉及改进的1-苯基乙醇对苯乙烯单体的液相脱水，其改进包括在液相脱水过程中使用残留物形成抑制剂。

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