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1. 发明授权

US06830816B2 Highly filled, pasty, composition containing silicoorganic nanohybrid and/or microhybrid capsules for scratch-resistant and/or abrasion-resistant coatings 失效
标题翻译：含有硅胶有机纳米混合和/或微混合胶囊的高填充，糊状组合物，用于耐刮擦和/或耐磨涂层
公开(公告)号：US06830816B2
公开(公告)日：2004-12-14
申请号：US10112042
申请日：2002-04-01
申请人： Reiner Mehnert , Hans-Juergen Glaesel , Helmut Langguth , Jaroslaw Monkiewicz , Roland Edelmann , Bjoern Borup
发明人： Reiner Mehnert , Hans-Juergen Glaesel , Helmut Langguth , Jaroslaw Monkiewicz , Roland Edelmann , Bjoern Borup
IPC分类号： C08K320
CPC分类号： C09C1/3081 , C01P2004/88 , C08K9/06 , C09C3/12 , Y10T428/2995 , Y10T428/31551 , Y10T428/31663 , Y10T428/31786 , Y10T428/31935
摘要： The present invention relates to a composition containing silico-organic nanohybrid and/or microhybrid capsules for scratch-resistant and/or abrasion-resistant coatings, wherein the silico-organic nanohybrid and/or microhybrid system includes one or more small metal oxide cores A and a substantially complete, silico-organic shell B, and the composition can be obtained by a reaction performed in situ, in a synthetic resin or in a synthetic-resin precursor compound, between metal oxide particles (KA-O) and at least one organofunctional silicon compound which contains an organofunctional group and at least one hydrolyzable group or at least one hydroxy group. The present invention also relates to the use of such compositions as the base for lacquers for producing a scratch-resistant and abrasion-resistant coating on a substrate as well as articles provided with corresponding scratch-resistant as well as abrasion-resistant coatings.
摘要翻译：本发明涉及包含用于耐刮擦和/或耐磨涂层的硅 - 有机纳米混合和/或微混合胶囊的组合物，其中硅 - 有机纳米混合和/或微混合系统包括一个或多个小金属氧化物核心A和基本上完全的硅 - 有机壳B，并且组合物可以通过在合成树脂或合成树脂前体化合物中原位进行的金属氧化物颗粒（KA-O）与至少一种有机官能团含有有机官能团和至少一个可水解基团或至少一个羟基的硅化合物。本发明还涉及这样的组合物作为基底用于在基材上生产耐刮擦和耐磨涂层以及具有相应的耐刮擦和耐磨涂层的制品的用途。

2. 发明授权

US06720072B1 High-temperature resistant polymerizable metal oxide particles 失效
标题翻译：耐高温聚合金属氧化物颗粒
公开(公告)号：US06720072B1
公开(公告)日：2004-04-13
申请号：US09807008
申请日：2001-07-06
申请人： Rudolf Hinterwaldner , Hans-Juergen Glaesel , Eberhard Hartmann , Reiner Mehnert
发明人： Rudolf Hinterwaldner , Hans-Juergen Glaesel , Eberhard Hartmann , Reiner Mehnert
IPC分类号： B32B516
CPC分类号： A61K6/0008 , A61K6/0017 , A61K6/0023 , B22C1/00 , C08F292/00 , C09D151/10 , Y10T428/2991 , Y10T428/2995 , C08L83/08 , C08L51/085 , C08L83/12
摘要： High-temperature resistant polymerizable metal oxide particles having a glass transition temperature of the homopolymerizable ≧100° C. and a core A. The core includes an oxide of a metal or semimetal of the third to sixth main group, of the first to eighth subgroup of the periodic table, or of the lanthanides, and has at least one group —(B)w—X bound via the oxygen atom of the oxide or hydroxide, in which B represents a binding link, and X represents a reactive functional group, and w is equal to 0 or 1. The inventive particles are useful, in particular, for producing coating materials, molding materials and adhesives.
摘要翻译：具有均聚物> 100℃的玻璃化转变温度和芯A的耐高温聚合性金属氧化物颗粒。芯包括第一至第八主体的金属或半金属的氧化物，第三至第六主体的金属或半金属并且具有通过氧化物或氢氧化物的氧原子结合的至少一个基团 - （B）wX，其中B表示结合连接，X表示反应性官能团，并且 w等于0或1.本发明的颗粒特别用于生产涂料，模塑材料和粘合剂。

3. 发明授权

US08962138B2 Organically functionalized polysiloxane nanoparticles, method for the production thereof, and use thereof 有权
标题翻译：有机官能化聚硅氧烷纳米颗粒，其制备方法及其用途
公开(公告)号：US08962138B2
公开(公告)日：2015-02-24
申请号：US13377064
申请日：2010-06-10
申请人： Monika Bauer , Hans-Juergen Glaesel
发明人： Monika Bauer , Hans-Juergen Glaesel
IPC分类号： B32B5/16 , C08G77/04 , C08G77/06 , C08G77/20 , C08G77/54 , C08G77/62 , C08K5/544 , C08L33/18
CPC分类号： C08G77/04 , C08G77/54 , C08G77/62 , C08K5/544 , C08L33/18 , Y10T428/2982 , Y10T428/2991 , Y10T428/2998 , Y10T428/31663 , C08L2666/44
摘要： The present invention relates to polysiloxane nanoparticles having the following properties: an average particle size d50 (measured using REM recordings) in the range of 10-200 nm, a specific surface area Ao of at least 50 m2/g, a pore volume of at least 0.2 cm3/g, an average pore volume d50 of at least 0.8 nm, wherein the particles have groups that contain carbon, which groups are bonded to the silicon at least partially in the form of unsubstituted or substituted alkyl, alkenyl, aryl, arylalkyl, or alkylaryl groups. Said polysiloxane nanoparticles can be produced, among other things, in that either a silazane or a mixture of different silazanes having one or more —[Si(R)(R1)—NR2]— units and/or a silane or a mixture of different silanes having the formula R′x—SiX4-a or an oligosiloxane obtainable by means of hydrolytic condensation of said silane/said silanes or a mixture of such oligosiloxanes are provided in a solvent and brought in contact with a strongly alkaline medium in such a way that the pH is not below 13 after the addition thereof. In specific embodiments, synthesis in acid is also successful.
摘要翻译：本发明涉及具有以下特性的聚硅氧烷纳米粒子：10-200nm范围内的平均粒径d50（使用REM记录测定），比表面积Ao为至少50m 2 / g，孔体积为至少0.2cm 3 / g，平均孔体积d50至少为0.8nm，其中所述颗粒具有含有碳的基团，所述基团至少部分地以未取代或取代的烷基，烯基，芳基，芳烷基，或烷基芳基。可以制备所述聚硅氧烷纳米颗粒，其特征在于，硅氮烷或具有一个或多个 - [Si（R）（R 1）-NR 2] - 单元和/或硅烷或不同的混合物的不同硅氮烷的混合物具有式R'x-SiX4-a的硅烷或通过所述硅烷/所述硅烷或这种低聚硅氧烷的混合物的水解缩合得到的低聚硅氧烷在溶剂中提供，并以这种方式与强碱性介质接触加入后pH不低于13。在具体实施方案中，酸中的合成也是成功的。

4. 发明申请

US20120082850A1 ORGANICALLY FUNCTIONALIZED POLYSILOXANE NANOPARTICLES, METHOD FOR THE PRODUCTION THEREOF, AND USE THEREOF 有权
标题翻译：有机官能化的聚硅氧烷纳米材料，其生产方法及其用途
公开(公告)号：US20120082850A1
公开(公告)日：2012-04-05
申请号：US13377064
申请日：2010-06-10
申请人： Monika Bauer , Hans-Juergen Glaesel
发明人： Monika Bauer , Hans-Juergen Glaesel
IPC分类号： C08G77/04 , C08G77/06 , C08G77/20 , C08L83/04 , C08L83/07 , B32B5/16 , C08G77/62 , C08L83/16 , B82Y40/00 , B82Y30/00
CPC分类号： C08G77/04 , C08G77/54 , C08G77/62 , C08K5/544 , C08L33/18 , Y10T428/2982 , Y10T428/2991 , Y10T428/2998 , Y10T428/31663 , C08L2666/44
摘要： The present invention relates to polysiloxane nanoparticles have the following properties: an average particle size d50 (measured using REM recordings) in the range of 10-200 nm, a specific surface area Ao of at least 50 m2/g, a pore volume of at least 0.2 cm3/g, an average pore volume d50 of at least 0.8 mn, whereas the particles have groups that contain carbon, which groups are bonded to the silicon at least partially in the form of unsubstituted or substituted alkyl, alkenyl, aryl, arylalkyl, or alkylaryl groups. Said polysiloxane nanoparticles can be produced, among other things, in that either a silaxone or a mixture of different silazanes having one or more —[Si(R)(R1)—NR2]— units and/or a silane or a mixture of different silanes having the formula R′x-SiX4-a or an oligosiloxane obtainable by means of hydrolytic condensation of said silane said silanes or a mixture of such oligosiloxanes are provided in a solvent and brought in contact with a strongly alkaline medium in such a way that the pH is not below 13 alter the addition thereof. In specific embodiments, synthesis in acid is also successful.
摘要翻译：本发明涉及聚硅氧烷纳米粒子具有以下性质：平均粒径d 50（使用REM记录测量）在10-200nm的范围内，比表面积A o为至少50m 2 / g，孔体积为至少0.2cm 3 / g，平均孔体积d50至少为0.8mn，而颗粒具有含有碳的基团，该基团至少部分地以未取代或取代的烷基，烯基，芳基，芳烷基，或烷基芳基。可以生产所述聚硅氧烷纳米颗粒，其特征在于，硅沙星或具有一个或多个 - [Si（R）（R 1）-NR 2] - 单元和/或硅烷或不同的混合物的不同硅氮烷的混合物具有式R'x-SiX4-a的硅烷或通过所述硅烷的水解缩合获得的低聚硅氧烷，所述硅烷或这种低聚硅氧烷的混合物在溶剂中提供，并与强碱性介质接触，使得 pH值不低于13，加入时不能改变。在具体实施方案中，酸中的合成也是成功的。

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