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1. 发明授权

US09267028B2 Mixtures of crosslinking agents 有权
标题翻译：交联剂的混合物
公开(公告)号：US09267028B2
公开(公告)日：2016-02-23
申请号：US13876559
申请日：2011-09-23
申请人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
发明人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
IPC分类号： C08G12/36 , C08F283/06 , C08L61/24 , C08G8/10 , C08G12/10 , C08G12/12 , C08G12/30 , C08G12/40 , C08G16/02 , C08L61/06 , C08L61/22 , C08L61/26 , C08L61/30 , C08K5/29 , C08K5/34
CPC分类号： C08L61/24 , C08G8/10 , C08G12/10 , C08G12/12 , C08G12/30 , C08G12/40 , C08G16/0256 , C08G16/0268 , C08K5/29 , C08K5/34 , C08L61/06 , C08L61/22 , C08L61/26 , C08L61/30
摘要： The invention relates to a crosslinker composition comprising a reaction product of a cyclic urea U and a multifunctional aliphatic aldehyde A, and at least one crosslinker selected from the group consisting of reaction products of an aminotriazine and at least one aldehyde selected from the group consisting of aliphatic monoaldehydes and multifunctional aliphatic aldehydes having the structure Y(CHO)n, where Y is an n-functional aliphatic residue, and n is greater than 1; reaction products of urea and/or cyclic ureas and formaldehyde; alkoxycarbonyl-aminotriazines; multifunctional isocyanates which may be partially or completely blocked; reaction products of phenols and aliphatic monoaldehydes; multifunctional epoxides; multifunctional aziridines; and multifunctional carbodiimides, wherein any of the crosslinkers which have hydroxyl groups may be etherified with one or more linear, branched, or cyclic aliphatic alcohols.
摘要翻译：本发明涉及一种交联剂组合物，其包含环状脲U和多官能脂族醛A的反应产物和至少一种选自以下的交联剂：氨基三嗪和至少一种选自以下的醛的反应产物：具有结构Y（CHO）n的脂肪族单醛和多官能脂族醛，其中Y是N-官能脂族残基，n大于1; 脲和/或环脲和甲醛的反应产物; 烷氧基羰基 - 氨基三嗪; 可部分或完全封闭的多官能异氰酸酯; 苯酚和脂肪族单醛的反应产物; 多功能环氧化物; 多功能氮丙啶; 和多官能碳化二亚胺，其中任何具有羟基的交联剂可以与一种或多种直链，支链或环状脂族醇醚化。

2. 发明申请

US20130203929A1 REACTION PRODUCT OF A CYCLIC UREA AND A MULTIFUNCTIONAL ALDEHYDE 审中-公开
标题翻译：循环尿素和多官能二氢呋喃的反应产物
公开(公告)号：US20130203929A1
公开(公告)日：2013-08-08
申请号：US13823782
申请日：2011-09-23
申请人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
发明人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
IPC分类号： C08G12/28 , C09D161/26
CPC分类号： C08G12/28 , B32B21/02 , C08G12/12 , C08G12/36 , C08L61/30 , C09D161/24 , C09D161/26
摘要： The invention relates to a reaction product UA of at least one cyclic urea U and at least one multifunctional aldehyde A which reaction product has as substituents on the carbonyl carbon atoms of the aldehyde A at least one kind of functional groups selected from the group consisting of hydroxyl groups —OH and alkoxy groups —OR characterised in that the groups —OR comprise at least two kinds of alkoxy groups —OR1 and —OR2, where R1 and R2 are both selected from the group consisting of linear, branched or cyclic alkyl groups having from one to twelve carbon atoms, where R1 and R2 may be the same or may be different from each other, to a process of making these, and to a method of use as crosslinker in coating compositions.
摘要翻译：本发明涉及至少一种环脲U和至少一种多官能醛A的反应产物UA，该反应产物在醛A的羰基碳原子上具有取代基，至少一种选自以下的官能团：羟基-OH和烷氧基-OR，其特征在于基团-OR包含至少两种烷氧基-OR 1和-OR 2，其中R 1和R 2都选自直链，支链或环状烷基，其具有 1到12个碳原子，其中R 1和R 2可以相同或可以彼此不同，涉及制备它们的方法，以及用作涂料组合物中交联剂的方法。

3. 发明授权

US09193885B2 Process for the preparation of a reaction product of a cyclic urea and a multifunctional aldehyde 有权
标题翻译：制备环状脲和多官能醛的反应产物的方法
公开(公告)号：US09193885B2
公开(公告)日：2015-11-24
申请号：US13876556
申请日：2011-09-23
申请人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
发明人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
IPC分类号： C08G12/12 , C08G12/36 , C09D161/24
CPC分类号： C09D167/02 , C08G12/12 , C08G12/26 , C08G12/36 , C09D161/24
摘要： This invention relates to a process to make a reaction product UA of at least one multifunctional aldehyde A with at least one cyclic urea U, by mixing the at least one multifunctional aldehyde A with the at least one cyclic urea U in the presence of at least one alcohol R1—OH, and optionally, at least one solvent that has no reactive groups which may react with aldehyde groups, —CO—NH— groups, or hydroxyl groups, to effect an addition reaction to obtain a solution of a product UA, where R1 is selected from the group consisting of linear, branched or cyclic alkyl groups having from one to twelve carbon atoms, to the reaction product obtained by this process, and to a method of use thereof as crosslinker for coating compositions.
摘要翻译：本发明涉及通过在至少一种环状脲U的存在下将至少一种多官能醛A与至少一种环状脲U混合来制备至少一种多官能醛A与至少一种环状脲U的反应产物UA的方法一个醇R 1 -OH和任选的至少一种不具有可与醛基-CO-NH-基团或羟基反应的反应性基团的溶剂，以进行加成反应以获得产物UA，其中R1选自具有1至12个碳原子的直链，支链或环状烷基，通过该方法获得的反应产物，以及作为涂料组合物交联剂的使用方法。

4. 发明申请

US20130189442A1 PROCESS FOR THE PREPARATION OF A REACTION PRODUCT OF A CYCLIC UREA AND A MULTIFUNCTIONAL ALDEHYDE 有权
标题翻译：制备循环尿素和多功能阿片剂的反应产物的方法
公开(公告)号：US20130189442A1
公开(公告)日：2013-07-25
申请号：US13876556
申请日：2011-09-23
申请人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
发明人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
IPC分类号： C09D161/24 , C08G12/12
CPC分类号： C09D167/02 , C08G12/12 , C08G12/26 , C08G12/36 , C09D161/24
摘要： This invention relates to a process to make a reaction product UA of at least one multifunctional aldehyde A with at least one cyclic urea U, by mixing the at least one multifunctional aldehyde A with the at least one cyclic urea U in the presence of at least one alcohol R1—OH, and optionally, at least one solvent that has no reactive groups which may react with aldehyde groups, —CO—NH— groups, or hydroxyl groups, to effect an addition reaction to obtain a solution of a product UA, where R1 is selected from the group consisting of linear, branched or cyclic alkyl groups having from one to twelve carbon atoms, to the reaction product obtained by this process, and to a method of use thereof as crosslinker for coating compositions.
摘要翻译：本发明涉及通过在至少一种环状脲U的存在下将至少一种多官能醛A与至少一种环状脲U混合来制备至少一种多官能醛A与至少一种环状脲U的反应产物UA的方法一个醇R 1 -OH和任选的至少一种不具有可与醛基-CO-NH-基团或羟基反应的反应性基团的溶剂，以进行加成反应以获得产物UA，其中R1选自具有1至12个碳原子的直链，支链或环状烷基，通过该方法获得的反应产物，以及作为涂料组合物交联剂的使用方法。

5. 发明申请

US20130189438A1 MIXTURES OF CROSSLINKING AGENTS 有权
标题翻译：交联剂混合物
公开(公告)号：US20130189438A1
公开(公告)日：2013-07-25
申请号：US13876559
申请日：2011-09-23
申请人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
发明人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
IPC分类号： C08L61/24
CPC分类号： C08L61/24 , C08G8/10 , C08G12/10 , C08G12/12 , C08G12/30 , C08G12/40 , C08G16/0256 , C08G16/0268 , C08K5/29 , C08K5/34 , C08L61/06 , C08L61/22 , C08L61/26 , C08L61/30
摘要： The invention relates to a crosslinker composition comprising a reaction product of a cyclic urea U and a multi-functional aliphatic aldehyde A, and at least one crosslinker selected from the group consisting of reaction products of an amino-triazine and at least one aldehyde selected from the group consisting of aliphatic monoaldehydes and multifunctional aliphatic aldehydes having the structure Y(CHO)n, where Y is an n-functional aliphatic residue, and n is greater than 1; reaction products of urea and/or cyclic ureas and formaldehyde; alkoxycarbonyl-aminotriazines; multifunctional isocyanates which may be partially or completely blocked; reaction products of phenols and aliphatic monoaldehydes; multifunctional epoxides; multifunctional aziridines; and multifunctional carbodiimides, wherein any of the crosslinkers which have hydroxyl groups may be etherified with one or more linear, branched, or cyclic aliphatic alcohols.
摘要翻译：本发明涉及一种交联剂组合物，其包含环脲U和多官能脂族醛A的反应产物和至少一种交联剂，其选自氨基 - 三嗪和至少一种选自以下的醛的反应产物：由具有结构Y（CHO）n的脂肪族单醛和多官能脂族醛组成的组，其中Y为正官能脂肪族残基，n大于1; 脲和/或环脲和甲醛的反应产物; 烷氧基羰基 - 氨基三嗪; 可部分或完全封闭的多官能异氰酸酯; 苯酚和脂肪族单醛的反应产物; 多功能环氧化物; 多功能氮丙啶; 和多官能碳化二亚胺，其中任何具有羟基的交联剂可以与一种或多种直链，支链或环状脂族醇醚化。

6. 发明授权

US10155836B2 Reaction product of a cyclic urea and a multifunctional aldehyde 有权
公开(公告)号：US10155836B2
公开(公告)日：2018-12-18
申请号：US13823782
申请日：2011-09-23
申请人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
发明人： Ram B. Gupta , Lawrence A. Flood , Urvee Y. Treasurer , Barry A. Lawless , Colin Brogan
IPC分类号： C08G12/28 , B32B21/02 , C08G12/12 , C08G12/36 , C08L61/30 , C09D161/24 , C09D161/26
摘要： The invention relates to a reaction product UA of at least one cyclic urea U and at least one multifunctional aldehyde A which reaction product has as substituents on the carbonyl carbon atoms of the aldehyde A at least one kind of functional groups selected from the group consisting of hydroxyl groups —OH and alkoxy groups —OR characterised in that the groups —OR comprise at least two kinds of alkoxy groups —OR1 and —OR2, where R1 and R2 are both selected from the group consisting of linear, branched or cyclic alkyl groups having from one to twelve carbon atoms, where R1 and R2 may be the same or may be different from each other, to a process of making these, and to a method of use as crosslinker in coating compositions.

7. 发明授权

US6063922A Carbamate functional 1,3,5-triazines 失效
标题翻译：氨基甲酸酯官能1,3,5-三嗪
公开(公告)号：US6063922A
公开(公告)日：2000-05-16
申请号：US816583
申请日：1997-03-13
申请人： Lawrence A. Flood , Ram B. Gupta , Revathi Iyengar , David A. Ley , Vankatarao K. Pai
发明人： Lawrence A. Flood , Ram B. Gupta , Revathi Iyengar , David A. Ley , Vankatarao K. Pai
IPC分类号： C07D251/48 , C07C251/18 , C07C251/70 , C07D251/18 , C07D251/70
CPC分类号： C07C251/70 , C07C251/18 , C07D251/18 , C07D251/70
摘要： Provided is a novel carbamate functional 1,3,5-triazine of the general formula ##STR1## wherein Z' is selected from the group consisting of hydrogen, hydrocarbyl, and a group represented by the formula NHQ',each Q' is independently selected from the group consisting of a hydrocarbyl, a hydrocarbyloxy hydrocarbyl and a group represented by the formula COOY, with the proviso that at least two of the Q' groups are COOY, andeach Y is independently selected from the group consisting of a hydrocarbyl group and a hydrocarbyloxy hydrocarbyl ether group, with the proviso that at least one Y group is a hydrocarbyloxy hydrocarbyl ether group. These carbamate functional 1,3,5-triazines find use, for example, as crosslinkers or reactive modifiers in curable compositions.
摘要翻译：本发明提供了一种新的氨基甲酸酯官能的1,3,5-三嗪，其通式如下：其中Z'选自氢，烃基和由式NHQ'表示的基团，每个Q'独立地选自由烃基，烃氧基烃基和由式COOY表示的基团组成，条件是Q'基团中的至少两个为COOY，并且每个Y独立地选自烃基和烃氧基烃基醚基团，条件是至少一个Y基团是烃氧基烃基醚基团。这些氨基甲酸酯官能的1,3,5-三嗪可用于例如可固化组合物中的交联剂或反应性改性剂。

8. 发明授权

US5792866A Process for the preparation of 1,3,5-triazine carbamates from amino 1,3,5-triazines and organic carbonates 失效
标题翻译：从氨基1,3,5-三嗪和有机碳酸酯制备1,3,5-三嗪氨基甲酸酯的方法
公开(公告)号：US5792866A
公开(公告)日：1998-08-11
申请号：US450760
申请日：1995-05-25
申请人： Lawrence A. Flood , Ram B. Gupta , Revathi Iyengar , David A. Ley , Vankatarao K. Pai
发明人： Lawrence A. Flood , Ram B. Gupta , Revathi Iyengar , David A. Ley , Vankatarao K. Pai
IPC分类号： C07D251/48 , C07C251/18 , C07C251/70 , C07D251/18 , C07D251/70 , C07D251/54
CPC分类号： C07C251/70 , C07C251/18 , C07D251/18 , C07D251/70
摘要： Provided is a process for preparing an at least bis-carbamate functional 1,3,5-triazine by contacting an at least diamino-1,3,5-triazine, an acyclic organic carbonate and a base, as well as certain novel compositions producible thereby. Also provided are substantially halogen contamination free crosslinker compositions comprising the products obtainable by the process, and curable compositions based upon these crosslinkers.
摘要翻译：提供了通过使至少二氨基-1,3,5-三嗪，无环有机碳酸酯和碱与至少两个氨基甲酸酯官能的1,3,5-三嗪的制备方法，以及某些可生产的新型组合物从而。还提供了基本上无卤素污染的交联剂组合物，其包含可通过该方法获得的产物，以及基于这些交联剂的可固化组合物。

9. 发明授权

US08460758B2 Process for the preparation of a crosslinker composition 有权
标题翻译：制备交联剂组合物的方法
公开(公告)号：US08460758B2
公开(公告)日：2013-06-11
申请号：US12745996
申请日：2008-12-05
申请人： Lawrence A. Flood , Barry A. Lawless
发明人： Lawrence A. Flood , Barry A. Lawless
IPC分类号： B05D1/00
CPC分类号： C08G14/08 , C09D161/34 , C09D167/08 , C08L2666/16
摘要： This invention is directed to a process for the preparation of a crosslinker composition, comprising the steps of providing a mixture of an aliphatic alcohol A having at least one hydroxyl group and from 1 to 10 carbon atoms, with at least one multifunctional aldehyde C having at least two aldehyde groups —CHO to form a mixture AC, heating the mixture AC to convert at least a part of the multifunctional aldehyde C to its hemiacetal or to its acetal to form a mixture (AC)′, adding to the mixture (AC)′ least one cyclic urea U or the educts to produce the said cyclic urea U in situ, which cyclic urea U has at least one unsubstituted >NH group, and reacting the mixture thus obtained to form a chemical bond between the nitrogen atom of the at least one unsubstituted >NH group of the at least one cyclic urea U5 and the carbon atom of the least one aldehyde group —CHO of the multifunctional aldehyde C, and coating compositions comprising the said crosslinker composition.
摘要翻译：本发明涉及一种制备交联剂组合物的方法，包括以下步骤：提供具有至少一个羟基和1-10个碳原子的脂族醇A与至少一种多官能醛C的混合物，至少两个醛基-CHO以形成混合物AC，加热混合物AC以将至少一部分多官能醛C转化成其半缩醛或缩醛，形成混合物（AC）至少一个环状尿素U或离子以原位生成所述环状尿素U，该环状脲U具有至少一个未取代的NH基团，并使由此获得的混合物反应，以形成在至少一个环状脲U5的至少一个未取代的> NH基团和多官能醛C的至少一个醛基-CHO的碳原子，以及包含所述交联剂组合物的涂料组合物。

10. 发明申请

US20100297356A1 PROCESS FOR THE PREPARATION OF A CROSSLINKER COMPOSITION 有权
标题翻译：制备交联剂组合物的方法
公开(公告)号：US20100297356A1
公开(公告)日：2010-11-25
申请号：US12745996
申请日：2008-12-05
申请人： Lawrence A. Flood , Barry A. Lawless
发明人： Lawrence A. Flood , Barry A. Lawless
IPC分类号： B05D3/02 , C08L73/00 , C08L63/00 , C08L33/00 , C08L75/04 , B05D1/02 , B05D1/28 , B05D1/18 , C09K3/00
CPC分类号： C08G14/08 , C09D161/34 , C09D167/08 , C08L2666/16
摘要： This invention is directed to a process for the preparation of a crosslinker composition, comprising the steps of providing a mixture of an aliphatic alcohol A having at least one hydroxyl group and from 1 to 10 carbon atoms, with at least one multifunctional aldehyde C having at least two aldehyde groups —CHO to form a mixture AC, heating the mixture AC to convert at least a part of the multifunctional aldehyde C to its hemiacetal or to its acetal to form a mixture (AC)′, adding to the mixture (AC)′ least one cyclic urea U or the educts to produce the said cyclic urea U in situ, which cyclic urea U has at least one unsubstituted >NH group, and reacting the mixture thus obtained to form a chemical bond between the nitrogen atom of the at least one unsubstituted >NH group of the at least one cyclic urea U5 and the carbon atom of the least one aldehyde group —CHO of the multifunctional aldehyde C, and coating compositions comprising the said crosslinker composition.
摘要翻译：本发明涉及一种制备交联剂组合物的方法，包括以下步骤：提供具有至少一个羟基和1-10个碳原子的脂族醇A与至少一种多官能醛C的混合物，至少两个醛基-CHO以形成混合物AC，加热混合物AC以将至少一部分多官能醛C转化成其半缩醛或缩醛，形成混合物（AC）至少一个环状尿素U或离子以原位生成所述环状尿素U，该环状脲U具有至少一个未取代的NH基团，并使由此获得的混合物反应，以形成在至少一个环状脲U5的至少一个未取代的> NH基团和多官能醛C的至少一个醛基-CHO的碳原子，以及包含所述交联剂组合物的涂料组合物。

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