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1. 发明授权

US06297378B1 Process for making 2-(2-hydroxy-4-alkoxyphenyl)-4,6-bisaryl-1,3,5-triazines 失效
标题翻译：制备2-（2-羟基-4-烷氧基苯基）-4,6-二芳基-1,3,5-三嗪的方法
公开(公告)号：US06297378B1
公开(公告)日：2001-10-02
申请号：US09389067
申请日：1999-09-02
申请人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
发明人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
IPC分类号： C07D25116
CPC分类号： C07D251/24
摘要： The invention relates to a novel process for making 2-(2-hydroxy-4-alkoxyphenyl)-4,6-bisaryl-1,3,5-triazine and 2-(2,4-dialkoxyphenyl)-4,6-bisaryl-1,3,5-triazine compounds directly from 2-chloro-4,6-bisaryl-1,3,5-triazine compounds with 3-alkoxyphenol, 1,3-dialkoxylbenzene compounds or mixtures thereof. The reaction step to prepare 2-chloro-4,6-bisaryl-1,3,5-triazines from the reaction of cyanuric chloride with substituted aromatic compounds can be combined with the addition reaction of 3-alkoxyphenol or 1,3-dialkoxylbenzene in a two-step, one-pot process. The 2-(2-hydroxyl-4-alkoxyphenyl)-4,6-bisaryl-1,3,5-triazine, and 2-(2,4-dialkoxyphenyl)-4,6-bisaryl-1,3,5-triazine compounds, are useful to stabilize materials against damage by light, heat, and oxygen, and as stabilizers for organic material, or mixtures thereof.
摘要翻译：本发明涉及制备2-（2-羟基-4-烷氧基苯基）-4,6-二芳基-1,3,5-三嗪和2-（2,4-二烷氧基苯基）-4,6-二芳基 -1,3,5-三嗪化合物直接由2-氯-4,6-二芳基-1,3,5-三嗪化合物与3-烷氧基苯酚，1,3-二烷氧基苯化合物或其混合物组成。从氰尿酰氯与取代的芳族化合物的反应制备2-氯-4,6-二芳基-1,3,5-三嗪的反应步骤可以与3-烷氧基苯酚或1,3-二烷氧基苯的加成反应一个两步一锅的过程。 2-（2-羟基-4-烷氧基苯基）-4,6-二芳基-1,3,5-三嗪和2-（2,4-二烷氧基苯基）-4,6-二芳基-1,3,5-三嗪，三嗪化合物可用于稳定材料以防止光，热和氧的损伤，以及用作有机材料的稳定剂或其混合物。

2. 发明授权

US06486317B1 Process for making 2-hydroxy-4-alkoxyphenyl or 2,4-dihydroxyphenyl substituted 1,3,5-triazine UV absorbers 失效
标题翻译：制备2-羟基-4-烷氧基苯基或2,4-二羟基苯基取代的1,3,5-三嗪UV吸收剂的方法
公开(公告)号：US06486317B1
公开(公告)日：2002-11-26
申请号：US09691502
申请日：2000-10-18
申请人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
发明人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
IPC分类号： C07D25124
CPC分类号： C07D251/22 , C07D251/20 , C07D251/24
摘要： The invention provides new processes for preparing compositions containing at least one triazine compound, including new compounds for use in these processes to form the compositions and the new compositions that are formed.
摘要翻译：本发明提供了用于制备含有至少一种三嗪化合物的组合物的新方法，包括用于这些方法的新化合物以形成组合物和形成的新组合物。

3. 发明授权

US06710177B2 Process for making triazine UV absorbers using Lewis acids and reaction promoters 有权
标题翻译：使用路易斯酸和反应促进剂制备三嗪紫外线吸收剂的方法
公开(公告)号：US06710177B2
公开(公告)日：2004-03-23
申请号：US09779604
申请日：2001-02-09
申请人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
发明人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
IPC分类号： C07D25124
CPC分类号： C07D251/24 , C07D251/22
摘要： It has been now surprisingly discovered after extensive research that 2-halo-4,6-bisaryl-1,3,5-triazine can be prepared with unprecedented selectivity, efficiency, mild conditions, and in high yield by the reaction of cyanuric halide with aromatics in the presence of at least one Lewis acid and at least one reaction promoter. This reaction is also unprecedently general as a variety of aromatics can be used to produce a wide selection of 2-halo-4,6-bisaryl-1,3,5-triazines. The novel approach includes the use of the reaction promoters in combination with at least one Lewis acid under certain reaction conditions to promote the formation of 2-halo-4,6-bisaryl-1,3,5-triazine compounds from cyanuric halide. Preferably, the Lewis acids and reaction promoters are combined to form a complex. 2-Halo-4,6-bisaryl-1,3,5-triazines are key intermediates for making 2-(2-oxyaryl)-4,6-bisaryl-1,3,5-triazine class of UV absorbers.
摘要翻译：现在已经广泛研究出人意料地发现，2-卤代-4,6-二芳基-1,3,5-三嗪可以以前所未有的选择性，效率，温和条件制备，并且通过氰尿酰卤与芳族化合物在至少一种路易斯酸和至少一种反应促进剂的存在下进行。该反应也是前所未有的，因为各种芳族化合物可用于产生广泛选择的2-卤代-4,6-二芳基-1,3,5-三嗪。该新方法包括在某些反应条件下使用反应促进剂与至少一种路易斯酸组合以促进由氰尿酰卤形成2-卤代-4,6-二芳基-1,3,5-三嗪化合物。优选将路易斯酸和反应促进剂组合以形成络合物。 2-卤代-4,6-二芳基-1,3,5-三嗪是制备2-（2-氧芳基）-4,6-双芳基-1,3,5-三嗪类UV吸收剂的关键中间体。

4. 发明授权

US07485723B2 Process for making trisaryl triazine UV absorbers using Lewis acids and reaction promoters 有权
标题翻译：使用路易斯酸和反应促进剂制备三芳基三嗪紫外线吸收剂的方法
公开(公告)号：US07485723B2
公开(公告)日：2009-02-03
申请号：US11531932
申请日：2006-09-14
申请人： Ram B. Gupta , Dennis J Jakiela , Sampath Venimadhavan , Russell C Cappadona , Venkatrao K. Pai
发明人： Ram B. Gupta , Dennis J Jakiela , Sampath Venimadhavan , Russell C Cappadona , Venkatrao K. Pai
IPC分类号： C07D251/24
CPC分类号： C07D251/24 , C07D251/22
摘要： It has been now surprisingly discovered after extensive research that 2-halo-4,6-bisaryl-1,3,5-triazine can be prepared with unprecedented selectivity, efficiency, mild conditions, and in high yield by the reaction of cyanuric halide with aromatics in the presence of at least one Lewis acid and at least one reaction promoter. This reaction is also unprecedently general as a variety of aromatics can be used to produce a wide selection of 2-halo-4,6-bisaryl-1,3,5-triazines. The novel approach includes the use of the reaction promoters in combination with at least one Lewis acid under certain reaction conditions to promote the formation of 2-halo-4,6-bisaryl-1,3,5-triazine compounds from cyanuric halide. Preferably, the Lewis acids and reaction promoters are combined to form a complex 2-Halo-4,6-bisaryl-1,3,5-triazines are key intermediates for making 2-(2-oxyaryl)-4,6-bisaryl-1,3,5-triazine class of UV absorbers.
摘要翻译：现在已经广泛研究出人意料地发现，2-卤代-4,6-二芳基-1,3,5-三嗪可以以前所未有的选择性，效率，温和条件制备，并且通过氰尿酰卤与芳族化合物在至少一种路易斯酸和至少一种反应促进剂的存在下进行。该反应也是前所未有的，因为各种芳族化合物可用于产生广泛选择的2-卤代-4,6-二芳基-1,3,5-三嗪。该新方法包括在某些反应条件下使用反应促进剂与至少一种路易斯酸组合以促进由氰尿酰卤形成2-卤代-4,6-二芳基-1,3,5-三嗪化合物。优选地，将路易斯酸和反应促进剂组合以形成络合物2-卤代-4,6-二芳基-1,3,5-三嗪是制备2-（2-氧芳基）-4,6-二芳基-1,3,5-三嗪的关键中间体， 1,3,5-三嗪类紫外线吸收剂。

5. 发明授权

US06486316B1 Process for making triazine UV absorbers using Lewis acids and reaction promoters 有权
标题翻译：使用路易斯酸和反应促进剂制备三嗪紫外线吸收剂的方法
公开(公告)号：US06486316B1
公开(公告)日：2002-11-26
申请号：US09442000
申请日：1999-11-17
申请人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
发明人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
IPC分类号： C07D25124
CPC分类号： C07D251/24 , C07D251/22
摘要： It has been now surprisingly discovered after extensive research that 2-halo-4,6-bisaryl-1,3,5-triazine can be prepared with unprecedented selectivity, efficiency, mild conditions, and in high yield by the reaction of cyanuric halide with aromatics in the presence of at least one Lewis acid and at least one reaction promoter. This reaction is also unprecedently general as a variety of aromatics can be used to produce a wide selection of 2-halo-4,6-bisaryl-1,3,5-triazines. The novel approach includes the use of the reaction promoters in combination with at least one Lewis acid under certain reaction conditions to promote the formation of 2-halo-4,6-bisaryl-1,3,5-triazine compounds from cyanuric halide. Preferably, the Lewis acids and reaction promoters are combined to form a complex. 2-Halo-4,6-bisaryl-1,3,5-triazines are key intermediates for making 2-(2-oxyaryl)-4,6-bisaryl-1,3,5-triazine class of UV absorbers.
摘要翻译：现在已经广泛研究出人意料地发现，2-卤代-4,6-二芳基-1,3,5-三嗪可以以前所未有的选择性，效率，温和条件制备，并且通过氰尿酰卤与芳族化合物在至少一种路易斯酸和至少一种反应促进剂的存在下进行。该反应也是前所未有的，因为各种芳族化合物可用于产生广泛选择的2-卤代-4,6-二芳基-1,3,5-三嗪。该新方法包括在某些反应条件下使用反应促进剂与至少一种路易斯酸组合以促进由氰尿酰卤形成2-卤代-4,6-二芳基-1,3,5-三嗪化合物。优选将路易斯酸和反应促进剂组合以形成络合物。 2-卤代-4,6-二芳基-1,3,5-三嗪是制备2-（2-氧芳基）-4,6-双芳基-1,3,5-三嗪类UV吸收剂的关键中间体。

6. 发明授权

US06900314B2 Process for making triazine UV absorbers using lewis acids and reaction promoters 有权
标题翻译：使用路易斯酸和反应促进剂制备三嗪紫外线吸收剂的方法
公开(公告)号：US06900314B2
公开(公告)日：2005-05-31
申请号：US10835731
申请日：2004-04-30
申请人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
发明人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
IPC分类号： C07D251/14 , C07B61/00 , C07D251/22 , C07D251/24
CPC分类号： C07D251/24 , C07D251/22
摘要： It has been now surprisingly discovered after extensive research that 2-halo-4,6-bisaryl-1,3,5-triazine can be prepared with unprecedented selectivity, efficiency, mild conditions, and in high yield by the reaction of cyanuric halide with aromatics in the presence of at least one Lewis acid and at least one reaction promoter. This reaction is also unprecedently general as a variety of aromatics can be used to produce a wide selection of 2-halo-4,6-bisaryl-1,3,5-triazines. The novel approach includes the use of the reaction promoters in combination with at least one Lewis acid under certain reaction conditions to promote the formation of 2-halo-4,6-bisaryl-1,3,5-triazine compounds from cyanuric halide. Preferably, the Lewis acids and reaction promoters are combined to form a complex. 2-Halo-4,6-bisaryl-1,3,5-triazines are key intermediates for making 2-(2-oxyaryl)-4,6-bisaryl-1,3,5-triazine class of UV absorbers.
摘要翻译：现在已经广泛研究出人意料地发现，2-卤代-4,6-二芳基-1,3,5-三嗪可以以前所未有的选择性，效率，温和条件制备，并且通过氰尿酰卤与芳族化合物在至少一种路易斯酸和至少一种反应促进剂的存在下进行。该反应也是前所未有的，因为各种芳族化合物可用于产生广泛选择的2-卤代-4,6-二芳基-1,3,5-三嗪。该新方法包括在某些反应条件下使用反应促进剂与至少一种路易斯酸组合以促进由氰尿酰卤形成2-卤代-4,6-二芳基-1,3,5-三嗪化合物。优选将路易斯酸和反应促进剂组合以形成络合物。 2-卤代-4,6-二芳基-1,3,5-三嗪是制备2-（2-氧芳基）-4,6-双芳基-1,3,5-三嗪类UV吸收剂的关键中间体。

7. 发明授权

US06730785B2 Process for making triazine UV absorbers using lewis acids and reaction promoters 有权
公开(公告)号：US06730785B2
公开(公告)日：2004-05-04
申请号：US09779597
申请日：2001-02-09
申请人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
发明人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
IPC分类号： C07D25124
CPC分类号： C07D251/24 , C07D251/22
摘要： It has been now surprisingly discovered after extensive research that 2-halo-4,6-bisaryl-1,3,5-triazine can be prepared with unprecedented selectivity, efficiency, mild conditions, and in high yield by the reaction of cyanuric halide with aromatics in the presence of at least one Lewis acid and at least one reaction promoter. This reaction is also unprecedently general as a variety of aromatics can be used to produce a wide selection of 2-halo-4,6-bisaryl-1,3,5-triazines. The novel approach includes the use of the reaction promoters in combination with at least one Lewis acid under certain reaction conditions to promote the formation of 2-halo-4,6-bisaryl-1,3,5-triazine compounds from cyanuric halide. Preferably, the Lewis acids and reaction promoters are combined to form a complex. 2-Halo-4,6-bisaryl-1,3,5-triazines are key intermediates for making 2-(2-oxyaryl)-4,6-bisaryl-1,3,5-triazine class of UV absorbers.

8. 发明授权

US06225468B1 Process for making 2-(2,4,-dihydroxyphenyl) or 2-(2,4-dialkoxyphenyl)-4,6-bisaryl-1,3,5-triazines 有权
标题翻译：制备2-（2,4'-二羟基苯基）或2-（2,4-二烷氧基苯基）-4,6-双芳基-1,3,5-三嗪的方法
公开(公告)号：US06225468B1
公开(公告)日：2001-05-01
申请号：US09388644
申请日：1999-09-02
申请人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
发明人： Ram B. Gupta , Dennis J. Jakiela , Sampath Venimadhavan , Russell C. Cappadona , Venkatrao K. Pai
IPC分类号： C07D25124
CPC分类号： C07D251/24
摘要： Provided is a new process for the preparation of compositions containing at least one triazine ultraviolet light absorber.
摘要翻译：提供了用于制备含有至少一种三嗪紫外光吸收剂的组合物的新方法。

9. 发明授权

US4293692A Continuous process for manufacturing substantially fully methylated substantially fully methylolated melamine compositions 失效
标题翻译：用于制造基本上完全甲基化的基本上完全羟甲基化的三聚氰胺组合物的连续方法
公开(公告)号：US4293692A
公开(公告)日：1981-10-06
申请号：US852380
申请日：1977-11-17
申请人： Venkatrao K. Pai , Joseph F. Skrivan
发明人： Venkatrao K. Pai , Joseph F. Skrivan
IPC分类号： C08G12/00 , C07D251/64 , C08G12/30 , C08G12/32 , C07D251/70
CPC分类号： C07D251/64
摘要： The manufacture of a substantially fully methylated, substantially fully methylolated melamine composition is carried out by a continuous process in which the methylolation of melamine is conducted in two stages, the first stage being effected at an acidic pH and the second stage being effected at an alkaline pH. The reaction mixture is then concentrated and reacted with methanol after which all of the unreacted volatiles and precipitated salts are removed to provide the product composition.
摘要翻译：基本完全甲基化的，基本上完全羟甲基化的三聚氰胺组合物的制造通过连续方法进行，其中三聚氰胺的羟甲基化在两个阶段中进行，第一阶段在酸性pH下进行，第二阶段在碱性条件下进行 pH值。然后将反应混合物浓缩并与甲醇反应，然后除去所有未反应的挥发物和沉淀的盐以提供产物组合物。

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