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1. 发明申请

US20220272982A1 METAL ORGANIC FRAMEWORKS COMPRISING COPPER IONS AND PROCESSES FOR PREPARING SAME 有权
公开(公告)号：US20220272982A1
公开(公告)日：2022-09-01
申请号：US17651205
申请日：2022-02-15
申请人： RJ Lee Group, Inc. , UT-BATTELLE, LLC , IOWA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
发明人： Steven J. Monaco , Richard J. Lee , Alan M. Levine , Jonathan Lyle Wistrom , Mariappan Parans Paranthaman , Merlin Theodore , Bryan Howard Bellaire , Nathan Drew Peroutka-Bigus
IPC分类号： A01N59/20 , C07F1/08 , A01N25/10 , A01N25/34 , A01P1/00
摘要： Provided is a metal organic framework (MOF) comprising copper ions. Also provided are resin powders, granules or pellets comprising the MOF. In some embodiments, the resin powders, granules or pellets are antimicrobial. Also provided are fibers or sheets comprising the MOF. In some embodiments, the fibers or sheets are antimicrobial. Processes for preparing the MOF are also provided.

2. 发明授权

US09920262B1 Methods of separation of pyrolysis oils 有权
公开(公告)号：US09920262B1
公开(公告)日：2018-03-20
申请号：US15358201
申请日：2016-11-22
申请人： RJ LEE GROUP, INC.
发明人： Jonathan Lyle Wistrom , Earl Richard Beaver , Skyler Linn Wistrom , Alan M. Levine , Richard J. Lee
IPC分类号： C10G53/14
CPC分类号： C10G53/14 , C10G2400/30
摘要： Methods for processing pyrolysis oil employs two or more of the following steps: A first separation creates (a) a lighter fraction and heavier fraction, (b) subjecting the lighter fraction to distillation and (c) subjecting the heavy fraction to removal of at least one of sulfur and nitrogen.

3. 发明授权

US10577540B2 Method and apparatus for steam separation of pyrolysis oils 有权
公开(公告)号：US10577540B2
公开(公告)日：2020-03-03
申请号：US16001580
申请日：2018-06-06
申请人： RJ LEE GROUP, INC.
发明人： Steven J. Monaco , Alan M. Levine , Richard J. Lee
IPC分类号： C10G7/00 , B01D3/38 , B01D3/42 , C10B53/07 , B01L3/14
摘要： Method and apparatus for processing pyrolysis oil from vehicular tires and effecting a steam distillation for separation of the pyrolysis oil to create a lighter fraction which may be subjected to fractional distillation and a heavy fraction which is usable as a fuel oil.

4. 发明申请

US20220324780A1 METHODS FOR ISOLATION AND PURIFICATION OF CANNABIDIOL (CBD) AND TERPENES FROM HEMP 有权
公开(公告)号：US20220324780A1
公开(公告)日：2022-10-13
申请号：US17657553
申请日：2022-03-31
申请人： RJ Lee Group, Inc.
发明人： Alan M. Levine , Steven J. Monaco , Richard J. Lee , Duane M. Erickson
IPC分类号： C07C37/50 , C07D311/80
摘要： The invention provides a plurality of methods which may be employed as a single method or a plurality of sequential method steps in the isolation and purification of Cannabidiol from Hemp plants. It also provides methods for having a terpene-rich fraction as a byproduct of the method. Depending upon the ultimate objective, the individual method components may be used separately or combined with one or more method steps to accomplish the objectives.

5. 发明授权

US10596487B2 Methods and apparatus for clarification of pyrolysis oils 有权
公开(公告)号：US10596487B2
公开(公告)日：2020-03-24
申请号：US15717264
申请日：2017-09-27
申请人： RJ LEE GROUP, INC.
发明人： Alan M. Levine , Steven J. Monaco , Richard J. Lee
IPC分类号： B01D1/00 , B01D3/14 , B01D5/00 , B01D15/00 , B01D17/02 , B01J20/12 , B01J20/34 , C10G21/00 , C10G21/14 , C10G21/28 , C10G25/00 , C10G25/12 , C10G53/04 , C10G53/08
摘要： The present invention provides a method and apparatus for processing to improve the properties of pyrolysis oil and, as a result, the commercial value of the same. The net result is creation of an oil with a much lighter color in lieu of the black color, reducing or elimination the undesired sulfury/amine aroma and reducing the amount of PAH which is believed to be a carcinogen.

6. 发明授权

US09291611B2 Methods for quantitative analysis of asbestos in vermiculite-containing materials 有权
标题翻译：用于含蛭石材料中石棉的定量分析方法
公开(公告)号：US09291611B2
公开(公告)日：2016-03-22
申请号：US13918071
申请日：2013-06-14
申请人： RJ LEE GROUP, INC.
发明人： Richard J. Lee , Matthew Spencer Sanchez , Alan M. Levine
IPC分类号： G01N33/38 , G01N1/34
CPC分类号： G01N33/38 , G01N1/34
摘要： A method for quantitative analysis of asbestos in vermiculite-containing materials includes a first embodiment which includes washing the sample with water or treating the sample with a low concentration acid to digest gypsum and carbonates, ashing the sample at a low temperature to remove cellulose, therefrom and analyzing the sample. Digestion may be effected before or after ashing. Subsequently, a second subsample may be ashed at low temperature to remove cellulose and refluxed with a concentrated acid followed by refluxing with a base and rinsing with deionized water to wash away gypsum, vermiculite and other soluble components. This is followed by analysis to determine asbestos concentration. In a further embodiment, the residue of the first embodiment may be employed as the second subsample.
摘要翻译：用于含蛭石的材料中的石棉的定量分析方法包括第一实施方案，其包括用水洗涤样品或用低浓度酸处理样品以消化石膏和碳酸盐，在低温下灰化样品以除去纤维素并分析样品。消化可能在灰化之前或之后进行。随后，可以在低温下将第二子样品灰化以除去纤维素并与浓缩酸回流，然后与碱回流并用去离子水冲洗以洗去石膏，蛭石和其它可溶组分。随后分析确定石棉浓度。在另一实施例中，第一实施例的残留物可以用作第二子样品。

7. 发明申请

US20140370610A1 METHODS FOR QUANTITATIVE ANALYSIS OF ASBESTOS IN VERMICULITE-CONTAINING MATERIALS 有权
标题翻译：含有矿物质的材料中ASBESTOS的定量分析方法
公开(公告)号：US20140370610A1
公开(公告)日：2014-12-18
申请号：US13918071
申请日：2013-06-14
申请人： RJ LEE GROUP, INC.
发明人： RICHARD J. LEE , Matthew Spencer Sanchez , Alan M. Levine
IPC分类号： G01N33/38 , G01N1/34
CPC分类号： G01N33/38 , G01N1/34
摘要： A method for quantitative analysis of asbestos in vermiculite-containing materials includes a first embodiment which includes washing the sample with water or treating the sample with a low concentration acid to digest gypsum and carbonates, ashing the sample at a low temperature to remove cellulose, therefrom and analyzing the sample. Digestion may be effected before or after ashing. Subsequently, a second subsample may be ashed at low temperature to remove cellulose and refluxed with a concentrated acid followed by refluxing with a base and rinsing with deionized water to wash away gypsum, vermiculite and other soluble components. This is followed by analysis to determine asbestos concentration. In a further embodiment, the residue if the first embodiment may be employed as the second subsample.
摘要翻译：用于含蛭石的材料中的石棉的定量分析方法包括第一实施方案，其包括用水洗涤样品或用低浓度酸处理样品以消化石膏和碳酸盐，在低温下灰化样品以除去纤维素并分析样品。消化可能在灰化之前或之后进行。随后，可以在低温下将第二子样品灰化以除去纤维素并用浓酸回流，然后与碱回流并用去离子水冲洗以洗去石膏，蛭石和其它可溶组分。随后分析确定石棉浓度。在另一个实施例中，如果第一实施例可以用作第二子样本，则残留物。

8. 发明授权

US11220634B2 Method and apparatus for steam separation of pyrolysis oils 有权
公开(公告)号：US11220634B2
公开(公告)日：2022-01-11
申请号：US16744275
申请日：2020-01-16
申请人： RJ LEE GROUP, INC.
发明人： Steven J. Monaco , Alan M. Levine , Richard J. Lee
IPC分类号： C10G7/00 , B01D3/38 , B01D3/42 , C10B53/07 , B01D3/14
摘要： Method and apparatus for processing pyrolysis oil from vehicular tires and effecting a steam distillation for separation of the pyrolysis oil to create a lighter fraction which may be subjected to fractional distillation and a heavy fraction which is usable as a fuel oil.

9. 发明授权

US10767115B2 Methods and apparatus for clarification of pyrolysis oils 有权
公开(公告)号：US10767115B2
公开(公告)日：2020-09-08
申请号：US16041010
申请日：2018-07-20
申请人： RJ LEE GROUP, INC.
发明人： Alan M. Levine , Steven J. Monaco , Richard J. Lee
IPC分类号： B01D5/00 , B01D17/02 , B01J20/12 , B01J20/34 , C10B53/07 , C10G21/14 , C10G21/28 , C10G25/00 , C10G25/12 , C10G53/04 , C10G53/08 , B01D3/00 , B01D3/40 , B01D3/14 , C10G21/00
摘要： The present invention provides a method and apparatus for processing to improve the properties of pyrolysis oil and, as a result, the commercial value of the same. The net result is creation of an oil with a much lighter color in lieu of the black color, reducing or elimination the undesired sulfury/amine aroma and reducing the amount of PAH which is believed to be a carcinogen.

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