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1. 发明授权

US5449463A Desalter wash water additive 失效
标题翻译：脱盐洗涤水添加剂
公开(公告)号：US5449463A
公开(公告)日：1995-09-12
申请号：US212455
申请日：1994-03-11
申请人： Phillip L. Elliott , Michael L. Braden , Donald J. Newman
发明人： Phillip L. Elliott , Michael L. Braden , Donald J. Newman
IPC分类号： B01D17/05 , C10G31/08
CPC分类号： C10G31/08
摘要： One aspect of the invention provides a method of preventing crude oil from becoming emulsified in desalter wash water. According to the method, the wash water is treated with an effective amount of a dispersion of a water-soluble cationic polymer.
摘要翻译：本发明的一个方面提供一种防止原油在脱盐洗涤水中乳化的方法。根据该方法，洗涤水用有效量的水溶性阳离子聚合物的分散体处理。

2. 发明授权

US5554298A Steel mill flume water treatment 失效
标题翻译：钢厂水槽水处理
公开(公告)号：US5554298A
公开(公告)日：1996-09-10
申请号：US376729
申请日：1995-01-20
申请人： Ronald D. Kochik , David A. Picco , Michael L. Braden , Kristine S. Salmen
发明人： Ronald D. Kochik , David A. Picco , Michael L. Braden , Kristine S. Salmen
IPC分类号： B01D17/04 , B01D17/05 , B21B45/02
CPC分类号： B01D17/047 , B21B45/0296 , Y02P70/135
摘要： The invention comprises a method of preventing deposition of oil on steel mill scale particles comprising adding from about 1 part per million to about 500 parts per million of an amine acrylate/acrylic acid copolymer to mill flume water. Once the copolymer is added, deposition of oil onto scale particles is prevented. The recovered mill scale has less than 2% oil by weight on the scale, making it suitable for recycle to the steelmaking process. Oil and water are subsequently separated with a greater percentage of oil being recovered.
摘要翻译：本发明包括一种防止油在钢厂颗粒上沉积的方法，其包括将约百万分之一至约百万分之一份的丙烯酸胺/丙烯酸共聚物加入到水槽中。一旦加入共聚物，就可以防止油垢沉积在鳞屑颗粒上。回收的轧机规模在规模上具有小于2％的油重量，使其适合回收到炼钢过程。随后，油和水随着回收的油的百分比的增加而分离。

3. 发明授权

US09790438B2 Method for removing metals and amines from crude oil 有权
公开(公告)号：US09790438B2
公开(公告)日：2017-10-17
申请号：US12563583
申请日：2009-09-21
申请人： Juan M. Garcia, III , Samuel A. Lordo , Michael L. Braden
发明人： Juan M. Garcia, III , Samuel A. Lordo , Michael L. Braden
IPC分类号： C10G17/04 , C10G17/09 , C10G33/02 , C10G33/04 , C10G17/02
CPC分类号： C10G17/04 , C10G17/02 , C10G17/09 , C10G33/02 , C10G33/04 , C10G2300/202 , C10G2300/205 , C10G2300/80 , C10G2300/805
摘要： A method of removing metals and amines from crude oil is provided. The method includes adding an effective metal removing amount of one or more hydroxycarboxylic acids selected from lactic acid and malic acid and salts thereof to the crude oil; adding wash water to the crude oil; mixing the crude oil, acid and wash water to form an emulsion; and resolving the emulsion into an aqueous phase and crude oil having a reduced metals content.

4. 发明申请

US20130043166A1 REMOVAL OF MERCURY AND MERCURIC COMPOUNDS FROM CRUDE OIL STREAMS 有权
公开(公告)号：US20130043166A1
公开(公告)日：2013-02-21
申请号：US13211418
申请日：2011-08-17
申请人： Michael L. Braden , Samuel A. Lordo
发明人： Michael L. Braden , Samuel A. Lordo
IPC分类号： C10G29/28
CPC分类号： C10G25/003 , C10G29/20 , C10G31/08 , C10G53/02 , C10G2300/1044 , C10G2300/201 , C10G2300/202 , C10G2300/205
摘要： The invention is directed towards a method of removing mercury bearing species from a hydrocarbon containing fluid. The method comprises the steps of: i) adding dithiocarbamate polymer to the fluid in an amount such that the number of mercury bonding sites on the polymer exceeds the amount of mercury atoms by at least 10% and ii) removing the mercury bearing dithiocarbamate polymer with a water/oil separation device. The invention relies upon an unexpected reversal in the solubility of dithiocarbamate polymer at very high concentrations. Because of the high solubility the polymer remains within the water phase of the hydrocarbon fluid and can be removed without the need for cumbersome precipitation methods and complicated solid liquid separation devices. As a result, the invention allows mercury contaminated crude oil to be easily rid of its mercury with easy to use equipment already present in a typical oil refinery.

5. 发明授权

US5552498A Preparation of amphoteric acrylic acid copolymers suitable as oil-in-water emulsion breakers 失效
标题翻译：适用于水包油乳液破乳剂的两性丙烯酸共聚物的制备
公开(公告)号：US5552498A
公开(公告)日：1996-09-03
申请号：US567761
申请日：1995-12-05
申请人： Michael L. Braden
发明人： Michael L. Braden
IPC分类号： B01D17/04 , C08F2/22 , C08F4/04 , C08F220/04 , C08F220/34 , C08F2/10 , C08F220/06
CPC分类号： C08F220/34 , B01D17/047 , C08F220/04
摘要： The invention comprise a composition for breaking oil-in-water emulsions comprising adding from about 1 part per million to about 500 parts per million of an amphoteric acrylic acid copolymer to the emulsion. Once the copolymer is added, the emulsion is subjected to agitation until the oil-in-water emulsion is resolved and the oil and water separates into two phases. The oil and water phases are then subjected to a separation technique to separate the phases. The invention further comprises a method of synthesizing the amphoteric polymers used in the emulsion breaking application.
摘要翻译：本发明包括一种用于破坏水包油乳液的组合物，其包括向乳液中加入约百万分之一至约百万分之500的两性丙烯酸共聚物。一旦加入共聚物，乳液就会受到搅拌，直到水包油乳液被分解，油和水分成两相。然后对油相和水相进行分离技术以分离相。本发明还包括合成在乳液破乳应用中使用的两性聚合物的方法。

6. 发明授权

US08524074B2 Removal of mercury and mercuric compounds from crude oil streams 有权
标题翻译：从原油流中去除汞和汞化合物
公开(公告)号：US08524074B2
公开(公告)日：2013-09-03
申请号：US13211418
申请日：2011-08-17
申请人： Michael L. Braden , Samuel A. Lordo
发明人： Michael L. Braden , Samuel A. Lordo
IPC分类号： C10G29/20 , C10G29/00
CPC分类号： C10G25/003 , C10G29/20 , C10G31/08 , C10G53/02 , C10G2300/1044 , C10G2300/201 , C10G2300/202 , C10G2300/205
摘要： The invention is directed towards a method of removing mercury bearing species from a hydrocarbon containing fluid. The method comprises the steps of: i) adding dithiocarbamate polymer to the fluid in an amount such that the number of mercury bonding sites on the polymer exceeds the amount of mercury atoms by at least 10% and ii) removing the mercury bearing dithiocarbamate polymer with a water/oil separation device. The invention relies upon an unexpected reversal in the solubility of dithiocarbamate polymer at very high concentrations. Because of the high solubility the polymer remains within the water phase of the hydrocarbon fluid and can be removed without the need for cumbersome precipitation methods and complicated solid liquid separation devices. As a result, the invention allows mercury contaminated crude oil to be easily rid of its mercury with easy to use equipment already present in a typical oil refinery.
摘要翻译：本发明涉及从含烃流体中除去含汞物质的方法。该方法包括以下步骤：i）向流体中加入二硫代氨基甲酸酯聚合物，其量使得聚合物上的汞结合位置的数量超过汞原子数量至少10％，和ii）除去带有二硫代氨基甲酸酯的聚合物与水/油分离装置。本发明依赖于二硫代氨基甲酸酯聚合物在非常高的浓度下的溶解度的意想不到的逆转。由于高溶解度，聚合物保留在烃流体的水相中，并且可以被除去，而不需要繁琐的沉淀方法和复杂的固体分液装置。因此，本发明允许汞污染的原油通过在典型的炼油厂中已经存在的易于使用的设备容易地除去其汞。

7. 发明申请

US20110068049A1 METHOD FOR REMOVING METALS AND AMINES FROM CRUDE OIL 有权
标题翻译：从原油中去除金属和氨基的方法
公开(公告)号：US20110068049A1
公开(公告)日：2011-03-24
申请号：US12563583
申请日：2009-09-21
申请人： Juan M. Garcia, III , Samuel A. Lordo , Michael L. Braden
发明人： Juan M. Garcia, III , Samuel A. Lordo , Michael L. Braden
IPC分类号： C10G17/04
CPC分类号： C10G17/04 , C10G17/02 , C10G17/09 , C10G33/02 , C10G33/04 , C10G2300/202 , C10G2300/205 , C10G2300/80 , C10G2300/805
摘要： A method of removing metals and amines from crude oil comprising adding an effective metal removing amount of one or more hydroxycarboxylic acids selected from lactic acid and malic acid and salts thereof to said crude oil; adding wash water to said crude oil; mixing said crude oil, acid and wash water to form an emulsion; and resolving said emulsion into an aqueous phase and crude oil having a reduced metals content.
摘要翻译：从原油中除去金属和胺的方法，包括向所述原油中加入有效金属去除量的一种或多种选自乳酸和苹果酸的羟基羧酸及其盐; 向所述原油中加入洗涤水; 混合所述原油，酸和洗涤水以形成乳液; 并将所述乳液分解成水相和具有降低的金属含量的原油。

8. 发明授权

US5104545A Process for removing water soluble organic compounds from produced water 失效
标题翻译：从生产水中除去水溶性有机化合物的方法
公开(公告)号：US5104545A
公开(公告)日：1992-04-14
申请号：US451219
申请日：1989-12-15
申请人： C. Mitchell Means , Michael L. Braden
发明人： C. Mitchell Means , Michael L. Braden
IPC分类号： B01D15/00 , B01D17/02 , C02F1/28 , E21B41/00 , E21B43/34
CPC分类号： E21B43/34 , B01D17/0202 , C02F1/28 , E21B41/0057
摘要： A process for the removal of water soluble organic compounds from produced water is provided. The process allows for the removal of water soluble organic compounds by passing the produced water through a column of adsorbing resin which is capable of removing the soluble organic compounds from the water and providing an environmentally acceptable effluent. The process further allows for the regeneration of the adsorbing resin by backwashing the resin with a solvent capable of eluting accumulated soluble organic compounds from the column. The process further allows for the treatment of the eluting solvent and soluble organic compound admixture in a manner to allow reuse of the solvent and to allow recovery of the soluble organic compounds or to allow direct injection of the soluble organic compound admixture into the oil stream. Thus, the invention provides a process for removal and recovery of water soluble organic compounds from produced water which creates no environmentally hazardous waste streams.
摘要翻译：提供了从生产的水中除去水溶性有机化合物的方法。该方法允许通过使所产生的水通过吸附树脂柱而去除水溶性有机化合物，所述吸附树脂能够从水中除去可溶性有机化合物并提供环境可接受的流出物。该方法还允许通过用能够从塔中洗脱累积的可溶性有机化合物的溶剂反洗树脂来再生吸附树脂。该方法还允许以允许溶剂再利用并允许回收可溶性有机化合物或允许可溶性有机化合物外加剂直接注入油流中的方式处理洗脱溶剂和可溶性有机化合物混合物。因此，本发明提供从产生的水中除去和回收水溶性有机化合物的方法，其不产生对环境有害的废物流。

9. 发明授权

US4931191A Method for separating solids from water using amine containing polymers 失效
标题翻译：使用含胺聚合物从水中分离固体的方法
公开(公告)号：US4931191A
公开(公告)日：1990-06-05
申请号：US296638
申请日：1989-01-13
申请人： Michael L. Braden , Stephen J. Allenson
发明人： Michael L. Braden , Stephen J. Allenson
IPC分类号： B01D21/01 , C02F1/54
CPC分类号： B01D21/01 , C02F1/54
摘要： A method for clarifying water by liquid/solid separation comprising dosing the water to be clarified with a copolymer produced by the emulsion polymerization of only hydrophobic monomers where at least one hydrophobic monomer is an amine containing monomer which is hydrophobic when the amine is neutral and hydrophilic when the amine is salified.
摘要翻译：一种通过液体/固体分离来澄清水的方法，包括用仅由疏水性单体乳液聚合制备的共聚物给予澄清的水，其中至少一种疏水性单体是当胺是中性和亲水时疏水的含胺单体当胺盐化时。

10. 发明授权

US5961838A Amphoteric polymer/polyamine combinations for color removal and clarification of paper mill waste water 失效
标题翻译：两性聚合物/多胺组合，用于脱色和澄清造纸废水
公开(公告)号：US5961838A
公开(公告)日：1999-10-05
申请号：US993229
申请日：1997-12-18
申请人： Michael L. Braden , Richard E. Metzgar , Jitendra T. Shah
发明人： Michael L. Braden , Richard E. Metzgar , Jitendra T. Shah
IPC分类号： B01D21/01 , C02F1/56 , C02F1/54
CPC分类号： C02F1/56 , Y10S210/917 , Y10S210/928
摘要： Processes for removing color from a paper mill waste effluent and for removing color from a textile plant waste effluent utilizing an amphoteric copolymer/polyamine combination are described. A preferred amphoteric copolymer is poly(dimethylaminoethylacrylate methyl chloride quaternary salt/acrylic acid) and a preferred polyamine is a polymeric reaction product of epichlorohydrin and dimethylamine.
摘要翻译：描述了使用两性共聚物/多胺组合从造纸厂废物流出物中除去颜色并从纺织厂废物流出物中除去颜色的方法。优选的两性共聚物是聚（二甲基氨基乙基丙烯酸酯甲基氯季铵盐/丙烯酸），优选的多胺是表氯醇和二甲胺的聚合反应产物。

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