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1. 发明申请

US20050176977A1 Method for producing conjugated linoleic acid glycerides 有权
标题翻译：共轭亚油酸甘油酯的制备方法
公开(公告)号：US20050176977A1
公开(公告)日：2005-08-11
申请号：US10513314
申请日：2003-04-25
申请人： Peter Horlacher , Franz Timmermann , Juergen Gierke , Karl-Heinz Ruf
发明人： Peter Horlacher , Franz Timmermann , Juergen Gierke , Karl-Heinz Ruf
IPC分类号： C07C67/03 , C07C67/333 , C11C3/06 , C11C3/14 , C07C51/347
CPC分类号： C11C3/14 , C07B2200/09 , C07C67/03 , C07C67/333 , C11C3/06 , C07C69/587
摘要： Processes for preparing conjugated fatty acid glycerides comprising: (a) isomerizing a fatty acid lower alkyl ester corresponding to the general formula (I) in the presence of a basic catalyst at a temperature of from 100 to 160° C., to form a conjugated fatty acid lower alkyl ester: R1CO—OR2 (I) wherein R1CO represents an acyl radical having from 16 to 22 carbon atoms and at least two carbon-carbon unsaturations and R2 represents an alkyl radical having from 1 to 4 carbon atoms; and (b) transesterifying the conjugated fatty acid lower alkyl ester with glycerol to form a conjugated fatty acid glyceride, wherein a lower alkanol corresponding to the general formula R2OH is formed, wherein R2 is as defined above, and the lower alkanol is continuously removed from the transesterification reaction; are described.
摘要翻译：制备共轭脂肪酸甘油酯的方法，包括：（a）在碱性催化剂存在下，在100至160℃的温度下，使通式（I）的脂肪酸低级烷基酯异构化，形成共轭脂肪酸低级烷基酯：<？in-line-formula description =“In-line formula”end =“lead”？> R 1 CO 2或I 2 ）<？in-line-formula description =“In-line formula”end =“tail”？>其中R 1 CO表示具有16至22个碳原子和至少两个碳原子的酰基碳不饱和度和R 2表示具有1至4个碳原子的烷基; 和（b）用甘油酯交换共轭脂肪酸低级烷基酯以形成共轭脂肪酸甘油酯，其中形成对应于通式R 2 OH的低级链烷醇，其中R 2 如上所定义，低级烷醇从酯交换反应中连续除去; 被描述。

2. 发明授权

US07179929B2 Method for producing conjugated linoleic acid glycerides 有权
标题翻译：共轭亚油酸甘油酯的制备方法
公开(公告)号：US07179929B2
公开(公告)日：2007-02-20
申请号：US10513314
申请日：2003-04-25
申请人： Peter Horlacher , Franz Timmermann , Juergen Gierke , Karl-Heinz Ruf
发明人： Peter Horlacher , Franz Timmermann , Juergen Gierke , Karl-Heinz Ruf
IPC分类号： C07C51/00
CPC分类号： C11C3/14 , C07B2200/09 , C07C67/03 , C07C67/333 , C11C3/06 , C07C69/587
摘要： Processes for preparing conjugated fatty acid glycerides comprising: (a) isomerizing a fatty acid lower alkyl ester corresponding to the general formula (I) in the presence of a basic catalyst at a temperature of from 100 to 160° C., to form a conjugated fatty acid lower alkyl ester: R1CO—OR2 (I) wherein R1CO represents an acyl radical having from 16 to 22 carbon atoms and at least two carbon-carbon unsaturations and R2 represents an alkyl radical having from 1 to 4 carbon atoms; and (b) transesterifying the conjugated fatty acid lower alkyl ester with glycerol to form a conjugated fatty acid glyceride, wherein a lower alkanol corresponding to the general formula R2OH is formed, wherein R2 is as defined above, and the lower alkanol is continuously removed from the transesterification reaction; are described.
摘要翻译：制备共轭脂肪酸甘油酯的方法，包括：（a）在碱性催化剂存在下，在100至160℃的温度下，使通式（I）的脂肪酸低级烷基酯异构化，形成共轭脂肪酸低级烷基酯：<？in-line-formula description =“In-line formula”end =“lead”？> R 1 CO 2或I 2 ）<？in-line-formula description =“In-line formula”end =“tail”？>其中R 1 CO表示具有16至22个碳原子和至少两个碳原子的酰基碳不饱和度和R 2表示具有1至4个碳原子的烷基; 和（b）用甘油酯交换共轭脂肪酸低级烷基酯以形成共轭脂肪酸甘油酯，其中形成对应于通式R 2 OH的低级链烷醇，其中R 2 如上所定义，低级烷醇从酯交换反应中连续除去; 被描述。

3. 发明申请

US20060189817A1 Method for producing conjugated linoleic acid 审中-公开
标题翻译：共轭亚油酸的制备方法
公开(公告)号：US20060189817A1
公开(公告)日：2006-08-24
申请号：US10538383
申请日：2003-12-09
申请人： Peter Horlacher , Karl-Heinz Ruf , Franz Timmermann , Wolfgang Adams , Rainer Kries
发明人： Peter Horlacher , Karl-Heinz Ruf , Franz Timmermann , Wolfgang Adams , Rainer Kries
IPC分类号： C07C51/347
CPC分类号： C11C3/14 , C07C51/09 , C07C51/353 , C07C51/43 , C07C57/12
摘要： The present invention relates to a process for the production of conjugated linoleic acid, in which (a) linoleic acid lower alkyl esters containing 1 to 5 carbon atoms in a linear or branched alkyl chain are isomerized in the presence of alkali metal alcoholates, (b) the then conjugated linoleic acids are released from the ester after saponification, and (c) the free linoleic acids are subjected to crystallization. The crystallization step of said method provides a cost-effective option for producing conjugated linoleic acids with a high purity and excellent storage stability, in particular in low temperatures.
摘要翻译：本发明涉及生产共轭亚油酸的方法，其中（a）在直链或支链烷基链中含有1至5个碳原子的亚油酸低级烷基酯在碱金属醇化物存在下异构化，（b ）然后皂化后从酯中释放出共轭亚油酸，（c）游离亚油酸进行结晶。所述方法的结晶步骤提供了用于生产具有高纯度和优异的储存稳定性的共轭亚油酸的成本有效的选择，特别是在低温下。

4. 发明授权

US06177580B1 Conjugated linolenic acid-based synthetic triglycerides 失效
标题翻译：共轭亚麻酸基合成甘油三酯
公开(公告)号：US06177580B1
公开(公告)日：2001-01-23
申请号：US09423054
申请日：1999-10-29
申请人： Franz Timmermann , Rolf Gaupp , Juergen Gierke , Rainer Von Kries , Wolfgang Adams , Andreas Sander
发明人： Franz Timmermann , Rolf Gaupp , Juergen Gierke , Rainer Von Kries , Wolfgang Adams , Andreas Sander
IPC分类号： C07C5100
CPC分类号： C11C3/08 , A23D9/00 , C07C67/08 , C11C3/02 , C07C69/587
摘要： A process for making synthetic triglycerides involving: (a) providing a reaction component selected from the group consisting of glycerol, a triglyceride, and mixtures thereof; (b) providing a fatty acid mixture containing at least 50% by weight, based on the weight of the fatty acid mixture, of conjugated linoleic acid; (c) providing an inert gas atmosphere; (d) combining the reaction component with the fatty acid mixture, in the inert atmosphere, to form a reaction mixture; and (e) heating the reaction mixture to a temperature of from 180 to 240° C., at a heating rate of from 0.5 to 3 K per minute, thus forming the synthetic triglyceride.
摘要翻译：制备合成甘油三酸酯的方法，其涉及：（a）提供选自甘油，甘油三酯及其混合物的反应组分; （b）提供含有至少50重量％脂肪酸混合物的共轭亚油酸的脂肪酸混合物; （c）提供惰性气体气氛; （d）在惰性气氛中将反应组分与脂肪酸混合物混合以形成反应混合物; 和（e）将反应混合物加热至180-240℃的温度，每分钟加热速率为0.5-3KK，从而形成合成甘油三酯。

5. 发明授权

US09144545B2 Sterol ester powder 有权
标题翻译：甾醇酯粉末
公开(公告)号：US09144545B2
公开(公告)日：2015-09-29
申请号：US12064651
申请日：2006-08-12
申请人： Peter Horlacher , Jürgen Gierke , Franz Timmermann , Wolfgang Albiez , Alois Hofmann
发明人： Peter Horlacher , Jürgen Gierke , Franz Timmermann , Wolfgang Albiez , Alois Hofmann
IPC分类号： A23C9/18 , A61K9/16 , A23L1/30 , A23L1/305
CPC分类号： A61K9/1658 , A23L33/11 , A23L33/17 , A23L33/19 , A61K9/1623
摘要： Compositions in powder form of sterols or stanol esters, and milk powder and/or proteins are disclosed. A process of making the compositions is also disclosed. The suitability of incorporation of the compositions in powder form in food products, for example beverages and milk products, is also disclosed.
摘要翻译：公开了甾醇或甾烷醇酯的粉末形式的组合物，以及奶粉和/或蛋白质。还公开了制备组合物的方法。还公开了将组合物以粉末形式并入食品，例如饮料和奶制品的适用性。

6. 发明申请

US20100055190A1 Sterol-Containing Compositions 审中-公开
标题翻译：含甾醇的成分
公开(公告)号：US20100055190A1
公开(公告)日：2010-03-04
申请号：US12282171
申请日：2007-02-27
申请人： Peter Horlacher , Dieter Hietsch , Wolfgang Albiez , Franz Timmermann , Katja Beck
发明人： Peter Horlacher , Dieter Hietsch , Wolfgang Albiez , Franz Timmermann , Katja Beck
IPC分类号： A61K9/14 , A61K31/56 , A61P9/10
CPC分类号： A23D7/0056 , A23D7/013 , A23L33/11 , C07J9/005
摘要： The invention relates to a powder formulation containing sterol in the form of a super-cooled melt from sterols and sterol esters, provided that the sterol ester content is at least 30 wt % in relation to the content of the powder. The introduced sterol ester is a fatty acid ester having a chain length of 2 to 24, preferably 8 to 12 carbon atoms. As the sterol preparations are wettable and melt easily without the use of complex equipment, they can easily be incorporated into food, and produce, in particular, good organoleptic and sensory properties, in particular, in drinks.
摘要翻译：本发明涉及一种粉末制剂，其含有来自甾醇和甾醇酯的过冷却熔体形式的固醇，条件是相对于粉末含量，甾醇酯含量至少为30重量％。引入的甾醇酯是链长为2至24，优选8至12个碳原子的脂肪酸酯。由于甾醇制剂在不使用复杂设备的情况下易于润湿和熔化，因此它们可以容易地并入食物中，特别是特别是在饮料中产生良好的感官和感官特性。

7. 发明申请

US20090099146A1 Compositions Containing Sterol-derived Esters 审中-公开
标题翻译：含有甾醇衍生酯的组合物
公开(公告)号：US20090099146A1
公开(公告)日：2009-04-16
申请号：US12282172
申请日：2007-02-27
申请人： Peter Horlacher , Dieter Hietsch , Wolfgang Albiez , Franz Timmermann , Katja Beck
发明人： Peter Horlacher , Dieter Hietsch , Wolfgang Albiez , Franz Timmermann , Katja Beck
IPC分类号： A61K31/56 , A61P3/06
CPC分类号： A23C9/1315 , A23C9/1528 , A23D7/011 , A23D7/013 , A23D9/013 , A23L33/11 , A23L33/12 , C07J9/005 , C11C3/003
摘要： The invention relates to sterol fatty acid esters of average chained fatty acids, having a chain length of 8 and 10 carbon atoms in a fatty acid distribution C8 to C10 (weight ratio) from 95:5 to 5:95, preferably, fatty acid distributions of C8 to C10 (weight ratio) from 90:10 to 20:80 and in particular, distributions of the fatty acids C8 to C10 (weight ratio) from 64:36 to 50:50 or from 78:22 to 65:35, are used. Preferably, capric and/or caprylic acids are used as fatty acids. Said sterol compounds can be easily incorporated into food, in particular, into drinks and milk products based on their wettability and easy to melt properties at low temperatures without using complex equipment, and have good organolepetic and sensory properties, and improved stability in relation to commercial sterol esters having long-chained and unsaturated fatty acids.
摘要翻译：本发明涉及脂肪酸分布C8〜C10（重量比）为95:5〜5:95的链长为8〜10个碳原子的平均链状脂肪酸的甾醇脂肪酸酯，优选为脂肪酸分布 C8〜C10（重量比）为90:10〜20:80，特别是脂肪酸C8〜C10（重量比）为64:36〜50:50或78:22〜65:35的分布，被使用。优选地，癸酸和/或辛酸用作脂肪酸。所述甾醇化合物可以容易地结合到食品中，特别是基于它们的润湿性和在低温下容易熔融的性质而不使用复杂的设备，并且具有良好的有机物和感官特性以及改进的与商业相关的稳定性具有长链和不饱和脂肪酸的甾醇酯。

8. 发明申请

US20080187643A1 Sterol Ester Powder 有权
标题翻译：甾醇酯粉末
公开(公告)号：US20080187643A1
公开(公告)日：2008-08-07
申请号：US12064651
申请日：2006-08-12
申请人： Peter Horlacher , Jurgen Gierke , Franz Timmermann , Wolfgang Albiez , Alois Hofmann
发明人： Peter Horlacher , Jurgen Gierke , Franz Timmermann , Wolfgang Albiez , Alois Hofmann
IPC分类号： A23C9/18 , A23C9/16
CPC分类号： A61K9/1658 , A23L33/11 , A23L33/17 , A23L33/19 , A61K9/1623
摘要： Compositions in powder form of sterols or stanol esters, and milk powder and/or proteins are disclosed. A process of making the compositions is also disclosed. The suitability of incorporation of the compositions in powder form in food products, for example beverages and milk products, is also disclosed.
摘要翻译：公开了甾醇或甾烷醇酯的粉末形式的组合物，以及奶粉和/或蛋白质。还公开了制备组合物的方法。还公开了将组合物以粉末形式并入食品，例如饮料和奶制品的适用性。

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