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1. 发明授权

US07584919B2 Compacting device 失效
标题翻译：压实装置
公开(公告)号：US07584919B2
公开(公告)日：2009-09-08
申请号：US11569783
申请日：2005-05-10
申请人： Peter Adler , Andreas Gölz , Holger Kirchner , Armin Müller , Torsten Sill , Raymund Sonnenschein
发明人： Peter Adler , Andreas Gölz , Holger Kirchner , Armin Müller , Torsten Sill , Raymund Sonnenschein
IPC分类号： B02C19/00
CPC分类号： B30B11/165 , B30B3/005 , B30B11/18
摘要： Compacting device for the low-metal compaction of a powder with a casing which at least in part surrounds a working chamber, with a feed arrangement arranged on the casing and feeding a powder, which is to be compacted, into the working chamber, with at least a compacting roller which is rotatably arranged in the working chamber, comprises a roller jacket and, together with an opposing wall, forms a compacting gap for compacting the powder therein, characterised in that the at least one compacting roller consists of ceramic, at least on the roller jacket.
摘要翻译：用于具有壳体的粉末的低金属压实的压实装置，其至少部分地围绕工作室，其中馈送装置布置在壳体上并将待压实的粉末供给到工作室中，其中在至少一个可旋转地布置在工作室中的压实辊包括一个辊套，并与相对的壁一起形成一个用于压实其中的粉末的压实间隙，其特征在于至少一个压实辊至少由陶瓷组成在夹克上。

2. 发明申请

US20080279748A1 Silicon and Method for Producing the Same 失效
标题翻译：硅及其制造方法
公开(公告)号：US20080279748A1
公开(公告)日：2008-11-13
申请号：US11569774
申请日：2005-05-10
申请人： Peter Adler , Andreas Gölz , Holger Kirchner , Armin Müller , Torsten Sill , Raymund Sonnenschein
发明人： Peter Adler , Andreas Gölz , Holger Kirchner , Armin Müller , Torsten Sill , Raymund Sonnenschein
IPC分类号： C01B33/029
CPC分类号： C01B33/02 , C01B33/027 , C01B33/029
摘要： Method for producing silicon which is suitable as a starting material for producing a silicon melt for the fabrication of silicon blocks or silicon crystals, comprising the following steps: introduction of a gaseous mixture of monosilane and hydrogen into a reactor, thermal degradation of the gaseous mixture with formation of silicon powder, separation of the silicon powder obtained from the gaseous mixture, and mechanical compacting of the separated silicon powder.
摘要翻译：制备硅的方法，其适合作为用于制造硅块或硅晶体的硅熔体的起始材料，包括以下步骤：将甲硅烷和氢气的气态混合物引入反应器中，气体混合物的热降解形成硅粉末，从气体混合物中分离得到的硅粉末，并分离硅粉末的机械压实。

3. 发明授权

US07758839B2 Silicon and method for producing the same 失效
标题翻译：硅及其制造方法
公开(公告)号：US07758839B2
公开(公告)日：2010-07-20
申请号：US11569774
申请日：2005-05-10
申请人： Peter Adler , Andreas Gölz , Holger Kirchner , Armin Müller , Torsten Sill , Raymund Sonnenschein
发明人： Peter Adler , Andreas Gölz , Holger Kirchner , Armin Müller , Torsten Sill , Raymund Sonnenschein
IPC分类号： C01B33/29 , C01B33/27 , C01B33/02 , F16C13/00
CPC分类号： C01B33/02 , C01B33/027 , C01B33/029
摘要： Method for producing silicon which is suitable as a starting material for producing a silicon melt for the fabrication of silicon blocks or silicon crystals, comprising the following steps: introducing a gaseous mixture of monosilane and hydrogen into a reactor, thermal degrading the gaseous mixture for forming silicon powder, separating the formed silicon powder produced from the gaseous mixture, and mechanical compacting the separated silicon powder with compacting rollers which having a roller jacket consisting of a ceramic material selected from graphite, glass and silicon nitride.
摘要翻译：制备硅的方法，其适合作为用于制造硅块或硅晶体的硅熔体的起始材料，其包括以下步骤：将甲硅烷和氢气的气态混合物引入反应器中，热降解用于形成的气体混合物硅粉末，分离由气态混合物生成的形成的硅粉末，并用具有由选自石墨，玻璃和氮化硅的陶瓷材料组成的辊套的压实辊机械压实分离的硅粉末。

4. 发明申请

US20070248438A1 Compacting Device 失效
标题翻译：压实装置
公开(公告)号：US20070248438A1
公开(公告)日：2007-10-25
申请号：US11569783
申请日：2005-05-10
申请人： Peter Adler , Andreas Golz , Holger Kirchner , Armin Muller , Torsten Sill , Raymund Sonnenschein
发明人： Peter Adler , Andreas Golz , Holger Kirchner , Armin Muller , Torsten Sill , Raymund Sonnenschein
IPC分类号： B65B1/00
CPC分类号： B30B11/165 , B30B3/005 , B30B11/18
摘要： Compacting device for the low-metal compaction of a powder with a casing which at least in part surrounds a working chamber, with a feed arrangement arranged on the casing and feeding a powder, which is to be compacted, into the working chamber, with at least a compacting roller which is rotatably arranged in the working chamber, comprises a roller jacket and, together with an opposing wall, forms a compacting gap for compacting the powder therein, characterised in that the at least one compacting roller consists of ceramic, at least on the roller jacket.
摘要翻译：用于具有壳体的粉末的低金属压实的压实装置，其至少部分地围绕工作室，其中馈送装置布置在壳体上并将待压实的粉末供给到工作室中，其中在至少一个可旋转地布置在工作室中的压实辊包括一个辊套，并与相对的壁一起形成一个用于压实其中的粉末的压实间隙，其特征在于至少一个压实辊至少由陶瓷组成在夹克上。

5. 发明申请

US20070251447A1 Reactor and Method for Manufacturing Silicon 审中-公开
标题翻译：反应器和硅制造方法
公开(公告)号：US20070251447A1
公开(公告)日：2007-11-01
申请号：US11573061
申请日：2005-07-26
申请人： Armin Muller , Torsten Sill , Raymund Sonnenschein , Peter Adler
发明人： Armin Muller , Torsten Sill , Raymund Sonnenschein , Peter Adler
IPC分类号： C01B33/035
CPC分类号： C01B33/035 , C30B29/06
摘要： A reactor for separating a gas containing silicon is provided with at least one electrically heatable deposition element of silicon to save costs, which element has a doping with at least one impurity to improve its electrical conductivity, the doping having a concentration in an initial state, such that the deposition element with the silicon deposited thereon in the final state is suitable for the manufacture of silicon melt for the production of polycrystalline silicon blocks or single silicon crystals for photovoltaics. A method for manufacturing silicon with the reactor according to the invention and the use of the manufactured silicon in photovoltaics are also described.
摘要翻译：用于分离含硅气体的反应器设置有至少一个可电镀硅的沉积元件以节省成本，该元件具有掺杂至少一种杂质以改善其导电性，该掺杂在初始状态下具有浓度，使得在最终状态下沉积有硅的沉积元件适于制造用于生产用于光伏的多晶硅块或单晶硅晶体的硅熔体。还描述了使用根据本发明的反应器制造硅的方法以及制造的硅在光伏中的用途。

6. 发明授权

US07799274B2 Device and process for the deposition of ultrafine particles from the gas phase 有权
标题翻译：从气相沉积超细颗粒的装置和工艺
公开(公告)号：US07799274B2
公开(公告)日：2010-09-21
申请号：US10581458
申请日：2004-10-13
申请人： Peter Adler , Wolfgang Pirzl , Raymund Sonnenschein
发明人： Peter Adler , Wolfgang Pirzl , Raymund Sonnenschein
IPC分类号： G01N31/12 , B01J10/00 , B01J10/02 , B01J12/00 , B01J12/02 , B01J14/00 , B01J15/00 , B01J16/00 , B01J19/00 , F27B15/08
CPC分类号： C01B33/029 , B01J19/087 , B01J2219/00085 , B01J2219/00135 , B01J2219/0875 , C01B21/068 , C01B33/183
摘要： A device for the thermal decomposition of a volatile compound, and for deposition of particles which are formed by the decomposition, includes (a) a pressure vessel, (b) at least one reaction tube located inside the pressure vessel such that, an open end of the reaction tube extends into the pressure vessel and an other end of the reaction tube is located outside the pressure vessel and is provided with a gas feed, wherein a longitudinal axis of the reaction tube is oriented in the direction of gravity and parallel to a longitudinal axis of the pressure vessel and wherein the reaction tube can be heated on a gas inlet side and cooled on a gas outlet side, wherein the pressure vessel, in its lower part, comprises a collection cone, wherein the open end of the at least one reaction tube extends into a gas space of the collection cone, wherein the collection cone is connected to an outlet lock for particles, and (c) a gas outlet unit located mainly inside the pressure vessel, the gas outlet unit comprising a gas guide, a gas inlet region, wherein the gas inlet region is in communication with the gas space of the collection cone, a filter system, and a gas outlet, which is located outside the pressure vessel.
摘要翻译：挥发性化合物的热分解装置和通过分解形成的颗粒的沉积装置包括（a）压力容器，（b）位于压力容器内部的至少一个反应管，使得开口端的反应管延伸到压力容器中，并且反应管的另一端位于压力容器外部并且设置有气体进料，其中反应管的纵向轴线沿重力方向定向并平行于压力容器的纵向轴线，并且其中反应管可以在气体入口侧被加热并在气体出口侧被冷却，其中压力容器在其下部包括收集锥体，其中至少该开口端一个反应管延伸到收集锥体的气体空间中，其中收集锥体连接到用于颗粒的出口锁，和（c）主要位于压力容器内部的气体出口单元，气体出口其包括气体引导件，气体入口区域，其中所述气体入口区域与所述收集锥体的气体空间，过滤器系统和气体出口连通，所述气体入口区域位于所述压力容器的外部。

7. 发明申请

US20070110619A1 Device and process for the deposition of ultrafine particles from the gas phase 有权
标题翻译：从气相沉积超细颗粒的装置和工艺
公开(公告)号：US20070110619A1
公开(公告)日：2007-05-17
申请号：US10581458
申请日：2004-10-13
申请人： Peter Adler , Wolfgang Pirzl , Raymund Sonnenschein
发明人： Peter Adler , Wolfgang Pirzl , Raymund Sonnenschein
IPC分类号： G01N31/12
CPC分类号： C01B33/029 , B01J19/087 , B01J2219/00085 , B01J2219/00135 , B01J2219/0875 , C01B21/068 , C01B33/183
摘要： The present invention relates to a device for the thermal decomposition of volatile compounds and deposition of particles which are then formed, which includes at least the following characteristic features a pressure vessel (1), at least one reaction tube (2), the open end (2e) of which extends-into the pressure vessel and the other end of which is located outside the pressure vessel and is provided with a gas feed (3), the longitudinal axis of the reaction tube is oriented in the direction of gravity and parallel to the longitudinal axis of the pressure vessel (1d), and the reaction tube can be heated (2a) on the gas inlet side and cooled (2b) on the gas outlet side, the pressure vessel (1), in its lower part, has a collection cone (1a), the open end of the reaction tube(s) (2c) extending into the gas space of the collection cone (1b), the collection cone (1a) is connected to an outlet lock (6) for powder (P), and a gas outlet unit (7), which is equipped with a gas guide (7a), the gas inlet region (7b) of which is in communication with the gas space (1b) of the collection cone (1a), a filter system (8) and a gas outlet (9), which is located outside the pressure vessel.
摘要翻译：本发明涉及一种用于热分解挥发性化合物和沉积颗粒的装置，其随后形成，其至少包括以下特征：压力容器（1），至少一个反应管（2），开口端（2e）延伸进入压力容器并且另一端位于压力容器外部并且设置有气体进料（3），反应管的纵向轴线沿重力方向定向，并且平行于压力容器（1d）的纵向轴线，并且反应管可以在气体入口侧被加热（2a）并在气体出口侧，压力容器（1）上冷却（2b）其下部具有收集锥体（1a），反应管的开口端（2c）延伸到收集锥体（1b）的气体空间中，收集锥体（1a）被连接到用于粉末（P）的出口锁（6）和装有w的气体出口单元（7）一个气体引导件（7a），其气体入口区域（7b）与收集锥体（1a）的气体空间（1b）连通，一个过滤系统（8）和一个气体出口 9），其位于压力容器外部。

8. 发明申请

US20110229398A1 FLUIDIZED BED REACTOR, THE USE THEREOF, AND A METHOD FOR THE ENERGY-INDEPENDENT HYDROGENATION OF CHLOROSILANES 审中-公开
标题翻译：流化床反应器及其使用方法，以及能量独立加氢氯化石蜡的方法
公开(公告)号：US20110229398A1
公开(公告)日：2011-09-22
申请号：US13062431
申请日：2009-07-10
申请人： Harald Troll , Peter Adler , Raymund Sonnenschein
发明人： Harald Troll , Peter Adler , Raymund Sonnenschein
IPC分类号： C01B33/107 , F27B15/14 , B01J8/18
CPC分类号： C01B33/1071 , B01J8/006 , B01J8/1809 , B01J8/1836 , B01J2208/00061 , B01J2208/00079 , B01J2208/00132 , B01J2208/00212 , B01J2208/00265 , Y02P20/129
摘要： The present invention relates to a device, to the use thereof, and to a method for the substantially energy-independent continuous production of chlorosilanes, particularly for the production of trichlorosilane as an intermediate product for yielding high-purity silicon.
摘要翻译：本发明涉及一种装置及其用途，以及用于基本上能量无关连续生产氯硅烷的方法，特别是用于生产作为产生高纯度硅的中间产物的三氯硅烷。

9. 发明申请

US20080095691A1 Apparatus and Process for Preparing Silanes 有权
标题翻译：硅烷制备装置及方法
公开(公告)号：US20080095691A1
公开(公告)日：2008-04-24
申请号：US11575226
申请日：2005-07-21
申请人： Raymund Sonnenschein , Peter Adler , Tim Popken , John Kahsnitz
发明人： Raymund Sonnenschein , Peter Adler , Tim Popken , John Kahsnitz
IPC分类号： B01D3/00 , B01J8/02 , C01B33/107
CPC分类号： C01B33/107 , B01D3/009 , B01J8/025 , C01B33/1071 , C01B33/10773 , Y02P20/127 , Y10S203/06
摘要： The invention relates to an apparatus, for preparing silanes of the general formula HnSiCl4-n where n=1, 2, 3 and/or 4 by dismutation of at least one relatively highly chlorinated silane in the presence of a catalyst, which is based on at least one distillation column (1) having a column bottom (1.1) and a column top (1.2), at least one side reactor (2) with catalyst bed (3), at least one feed inlet (1.3), a product offtake (1.4) and at least one further product offtake (1.5 or 1.8), where the distillation column (1) is provided with at least one chimney tray (4) and at least one side reactor (2) is connected to the distillation column (1) via at least three pipes (5, 6, 7) in such a way that the connection point of the line (5) to the distillation column (1) for the discharge of the condensate from the chimney tray (4, 4.1) is at a higher level than the upper edge of the catalyst bed (3, 3.1 or 3.2), the line (6) for the discharge of the liquid phase from the side reactor (2) opens (6.1) into the distillation column (1) below the chimney tray (4) and this opening (6, 6.1) is at a lower level than the upper edge of the catalyst bed (3, 3.1 or 3.2) and the line (7) for the discharge of the gas phase from the associated side reactor (2) opens (7.1) into the distillation column (1) above the level (4.1) of the chimney tray (4). Furthermore, the present invention provides a process for preparing said silanes in the apparatus of the invention.
摘要翻译：本发明涉及一种用于制备通式为其中n = 1,2,3和/或4的硅烷的硅烷的装置，其中n = 1,2,3和/或4通过在基于具有塔底（1.1）和塔顶（1.2）的至少一个蒸馏塔（1），至少一个具有催化剂的侧反应器（2）的催化剂存在下，至少一种相对高度氯化的硅烷床（3），至少一个进料入口（1.3），产品出口（1.4）和至少一个另外的出料产品（1.5或1.8），其中蒸馏塔（1）设置有至少一个烟囱托盘（4）），并且至少一个侧反应器（2）经由至少三个管（5,6,7）连接到蒸馏塔（1），使得管线（5）到蒸馏塔（用于排出来自烟囱式塔盘（4,4.1）的冷凝物的排放比催化剂床（3,3.1或3.2）的上边缘高的水平，排出管线（6）来自侧反应器（2）的液相的边界向烟囱盘（4）下方的蒸馏塔（1）打开（6.1），该开口（6,6.1）处于比催化剂的上边缘低的水平床（3,3.1或3.2）和用于从相关联的反应器（2）排出气相的管线（7）打开（7.1）进入烟囱式塔板（4.1）上方的蒸馏塔（1）（4）。此外，本发明提供了在本发明的装置中制备所述硅烷的方法。

10. 发明授权

US08105564B2 Process for producing monosilane 失效
标题翻译：生产甲硅烷的方法
公开(公告)号：US08105564B2
公开(公告)日：2012-01-31
申请号：US12088286
申请日：2006-06-19
申请人： Raymund Sonnenschein , Peter Adler , Yuriy Kasatkin , Adolf Petrik , Leonid Schwarzmann
发明人： Raymund Sonnenschein , Peter Adler , Yuriy Kasatkin , Adolf Petrik , Leonid Schwarzmann
IPC分类号： B01J8/02 , C01B33/08 , C01B33/04
CPC分类号： C01B33/043 , B01D3/009 , B01J8/0085 , B01J8/009 , B01J8/025 , B01J8/0285 , B01J8/0426 , B01J8/0438 , B01J8/0453 , B01J8/048 , B01J8/0484 , B01J8/0492 , B01J8/0496 , B01J8/065 , B01J8/067 , B01J19/30 , B01J19/32 , B01J2208/00176 , B01J2208/00212 , B01J2208/00221 , B01J2208/00247 , B01J2208/00274 , B01J2208/00283 , B01J2208/0053 , B01J2208/00884 , B01J2208/021 , B01J2219/30475 , B01J2219/32466 , B01J2219/3325 , C01B33/10773 , Y02P20/127 , Y10S203/06
摘要： Provided is a plant for the continuous production of monosilane and tetrachlorosilane by catalytic dismutation of trichlorosilane, wherein the plant contains: a countercurrent reactor having a double wall, a catalyst bed containing a catalyst which is located in the countercurrent reactor, a condenser at the top of the countercurrent reactor, a vaporizer unit at the bottom of the countercurrent reactor, a trichlorosilane feed line for the introduction of trichlorosilane into the countercurrent reactor, a heat exchanger, with the trichlorosilane conveyed by line via the heat exchanger and preheated there by a bottom product from the vaporizer unit and, for this purpose, the bottom product is fed by line via the heat exchanger into the double wall at a level in the lower part of the countercurrent reactor and discharged from the double wall at a level in the upper part of the countercurrent reactor, a condensation unit downstream of the condenser, and a distillation column having an outlet for monosilane.
摘要翻译：提供了通过三氯硅烷的催化歧化连续生产甲硅烷和四氯硅烷的设备，其中该装置包含：具有双壁的逆流反应器，含有位于逆流反应器中的催化剂的催化剂床，位于顶部的冷凝器逆流反应器底部的蒸发器单元，用于将三氯硅烷引入逆流反应器的三氯硅烷进料管线，热交换器，三氯硅烷通过热交换器通过管线输送并通过底部预热来自蒸发器单元的产品，并且为此目的，底部产物通过热交换器通过管线被供给到逆流反应堆的下部中的水平面处的双壁中，并且在双层壁的上部排出的逆流反应器，在冷凝器下游的冷凝单元和具有外部反应器的蒸馏塔甲硅烷。

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