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1. 发明授权

US5879607A Method of making a protective coating material 失效
标题翻译：制作保护涂层材料的方法
公开(公告)号：US5879607A
公开(公告)日：1999-03-09
申请号：US625503
申请日：1996-03-29
申请人： Paul Klocek , William J. MacKnight , Richard J. Farris , Christian Lietzau
发明人： Paul Klocek , William J. MacKnight , Richard J. Farris , Christian Lietzau
IPC分类号： B29C70/22 , B29C70/34 , B29C70/46 , B32B27/02 , B32B27/04 , B32B27/36 , B29C61/00
CPC分类号： B29C70/22 , B29C70/34 , B29C70/46 , B32B27/02 , B32B27/04 , B29K2995/0026 , B29L2031/3456 , Y10S428/911 , Y10S428/918 , Y10T428/24124 , Y10T428/24132 , Y10T428/24364 , Y10T442/2615
摘要： A protective, impact resistant material and method which includes a fabric of thermoplastic polymeric fibers having a strength of at least 0.5 GPa and an elastic modulus of at least 25 GPa and a matrix of polymeric material disposed in the interstices between the fibers having an elastic modulus of 0.2 to 3.times.10.sup.6 psi. The polymeric fibers can be gel spun, polyethylene, polypropylene, nylon, polyvinyl alcohol and polyethylene terephthalate. In a second embodiment, the matrix is derived from the fabric. The method includes the steps of providing a matrix of melted polymeric material transparent to energy of a predetermined type and having a predetermined melting temperature, placing a fabric of polymeric fibers having a melting temperature higher than that of the matrix in the matrix, applying a pressure of 1000 to 2000 psi to the fabric in the matrix, then raising the temperature to the melting temperature of the fabric for the time required to cause consolidation of the fabric and the matrix and rapidly cooling the consolidated fabric and matrix to a temperature below the melting temperature of the fabric. In accordance with the second embodiment there is provided a fabric of polymeric fibers as in the first embodiment which is operated upon as in the first embodiment to cause melting of a sufficient portion of the fabric to fill the interstices between the fibers of the fabric. The fabric is then rapidly cooled to a temperature below the melting temperature of the fabric.
摘要翻译：一种保护性，耐冲击的材料和方法，其包括具有至少0.5GPa的强度和至少25GPa的弹性模量的热塑性聚合物纤维的织物和设置在纤维之间的间隙中的聚合物材料的基体，其具有弹性模量为0.2至3×10 6 psi。聚合物纤维可以是凝胶纺丝，聚乙烯，聚丙烯，尼龙，聚乙烯醇和聚对苯二甲酸乙二醇酯。在第二实施例中，矩阵是从织物得到的。该方法包括以下步骤：提供对预定类型的能量透明并具有预定熔融温度的熔融聚合物材料的基体，将具有高于基质的熔解温度的聚合物纤维的织物放置在基质中，施加压力在基质中的织物为1000至2000psi，然后将织物和基质固化所需的时间升高至织物的熔融温度，并迅速将固化织物和基体冷却至低于熔化温度织物的温度。根据第二实施例，提供如第一实施例中的聚合物纤维织物，其如第一实施例中那样操作，以使足够部分的织物熔化以填充织物纤维之间的间隙。然后将织物快速冷却至低于织物的熔融温度的温度。

2. 发明授权

US6077381A Method of making a high strength, high modulus continous polymeric material for durable, impact resistant applications 失效
标题翻译：制造高强度，高模量连续聚合物材料的方法，用于耐用，耐冲击的应用
公开(公告)号：US6077381A
公开(公告)日：2000-06-20
申请号：US487818
申请日：1995-06-07
申请人： Paul Klocek , William J. MacKnight , Richard J. Farris , Christian Lietzau
发明人： Paul Klocek , William J. MacKnight , Richard J. Farris , Christian Lietzau
IPC分类号： B29C70/22 , B29C70/34 , B29C70/46 , B32B27/02 , B32B27/04 , B32B27/36 , C09J5/00
CPC分类号： B29C70/22 , B29C70/34 , B29C70/46 , B32B27/02 , B32B27/04 , B29K2995/0026 , B29L2031/3456 , Y10S428/911 , Y10S428/918 , Y10T428/24124 , Y10T428/24132 , Y10T428/24364
摘要： A method of making a protective coating material wherein there is provided a matrix of melted polymeric material transparent to energy of a predetermined type and having a predetermined melting temperature. A fabric of polymeric fibers having a melting temperature higher than the melting temperature of the matrix is placed in the matrix. The fibers are thermoplastic and have a strength of at least about 0.5 GPa (70,000 psi) and an elastic (Young's) modulus of at least about 25 GPa (3.6.times.10.sup.6 psi) and said matrix has an elastic modulus in the range from about 0.2 to about 3.times.10.sup.6 psi. A pressure of from about 1000 to about 2000 psi is applied to the fabric disposed in the matrix and then the temperature is raised to about and at least the melting temperature of the fabric for about the minimum time required to cause consolidation of the fabric and the matrix. The consolidated fabric and matrix are then rapidly cooled to a temperature below the melting temperature of the fabric.
摘要翻译：一种制备保护涂层材料的方法，其中提供了对预定类型的能量透明并且具有预定熔融温度的熔融聚合材料的基体。将具有高于基体的熔融温度的熔融温度的聚合物纤维织物放置在基质中。纤维是热塑性的，并且具有至少约0.5GPa（70,000psi）的强度和至少约25GPa（3.6×10 6 psi）的弹性（杨氏）模量，并且所述基体的弹性模量在约0.2至约3×10 6 psi。将约1000至约2000psi的压力施加到布置在基质中的织物上，然后将织物的温度升高至大约至少并且至少达到织物的熔化温度约为使织物固结所需的最短时间矩阵。然后将固结织物和基质快速冷却至低于织物熔融温度的温度。

3. 发明授权

US6083583A High strength, high modulus continuous polymeric material for impact resistant applications 有权
标题翻译：高强度，高模量连续聚合物材料，用于耐用的耐冲击应用
公开(公告)号：US6083583A
公开(公告)日：2000-07-04
申请号：US174303
申请日：1998-10-15
申请人： Paul Klocek , William J. MacKnight , Richard J. Farris , Christian Lietzau
发明人： Paul Klocek , William J. MacKnight , Richard J. Farris , Christian Lietzau
IPC分类号： B29C70/22 , B29C70/34 , B29C70/46 , B32B27/02 , B32B27/04 , B32B27/36
CPC分类号： B29C70/22 , B29C70/34 , B29C70/46 , B32B27/02 , B32B27/04 , B29K2995/0026 , B29L2031/3456 , Y10S428/911 , Y10S428/918 , Y10T428/24124 , Y10T428/24132 , Y10T428/24364 , Y10T428/24694
摘要： A protective, impact resistant material and method, the material comprising a fabric of thermoplastic polymeric fibers having a strength of at least 0.4 GPa and an elastic modulus of at least 5 GPa and a matrix of polymeric material disposed in the interstices between the fibers, the matrix having an elastic modulus in the range 0.2 to 3.times.10.sup.6 psi. The polymeric fibers can be gel spun polyethylene, polypropylene, nylon, polyvinyl alcohol and polyethylene terephthalate. In a second embodiment, the matrix is derived from the fabric. The method of making the material comprises providing a matrix of melted polymeric material transparent to energy of a predetermined type and having a predetermined melting temperature, placing a fabric of polymeric fibers having a melting temperature higher than the melting temperature of the matrix in the matrix, applying a pressure of 1000 to 6000 psi to the fabric disposed in the matrix, then raising the temperature to the melting temperature of the fabric for the minimum time required to cause consolidation of the fabric and the matrix and rapidly cooling the consolidated fabric and matrix to a temperature below the melting temperature of the fabric. In accordance with a second embodiment there is provided a fabric of polymeric fibers as in the first embodiment which is operated upon as in the first embodiment to cause melting of a sufficient portion of the fabric to fill the interstices between the fibers of the fabric and the fabric is then rapidly cooled to a temperature below the melting temperature of the fabric.
摘要翻译：一种保护性，耐冲击的材料和方法，该材料包括具有至少0.4GPa的强度和至少5GPa的弹性模量的热塑性聚合物纤维的织物和设置在纤维之间的间隙中的聚合物材料的基体，基体的弹性模量在0.2至3×10 6 psi的范围内。聚合物纤维可以是聚乙烯，聚丙烯，尼龙，聚乙烯醇和聚对苯二甲酸乙二醇酯。在第二实施例中，矩阵是从织物得到的。制造材料的方法包括提供对预定类型的能量透明并具有预定熔融温度的熔融聚合物材料的基体，将具有高于基体的熔融温度的熔解温度的聚合物纤维的织物放置在基质中，对布置在基质中的织物施加1000至6000psi的压力，然后将织物和基体固结所需的最短时间提高到织物的熔融温度，并将固结的织物和基体快速冷却至温度低于织物的熔化温度。根据第二实施例，提供如第一实施例中的聚合物纤维的织物，其如第一实施例中那样被操作以使足够部分的织物熔化以填充织物的纤维之间的间隙和然后将织物快速冷却至低于织物熔融温度的温度。

4. 发明授权

US5935651A High strength, high modulus continuous polymeric material for durable, impact resistant applications 失效
标题翻译：高强度，高模量连续聚合物材料，适用于耐用，耐冲击的应用
公开(公告)号：US5935651A
公开(公告)日：1999-08-10
申请号：US521154
申请日：1995-08-29
申请人： Paul Klocek , William J. MacKnight , Richard J. Farris , Christian Lietzau
发明人： Paul Klocek , William J. MacKnight , Richard J. Farris , Christian Lietzau
IPC分类号： B29C70/22 , B29C70/34 , B29C70/46 , B32B27/02 , B32B27/04 , B32B27/36 , B05D5/00
CPC分类号： B29C70/22 , B29C70/34 , B29C70/46 , B32B27/02 , B32B27/04 , B29K2995/0026 , B29L2031/3456 , Y10S428/911 , Y10S428/918 , Y10T428/24124 , Y10T428/24132 , Y10T428/24364 , Y10T428/24694
摘要： A protective, impact resistant material and method, the material comprising a fabric of thermoplastic polymeric fibers having a strength of at least 0.4 GPa and an elastic modulus of at least 5 GPa and a matrix of polymeric material disposed in the interstices between the fibers, the matrix having an elastic modulus in the range 0.2 to 3.times.10.sup.6 psi. The polymeric fibers can be gel spun polyethylene, polypropylene, nylon, polyvinyl alcohol and polyethylene terephthalate. In a second embodiment, the matrix is derived from the fabric. The method of making the material comprises providing a matrix of melted polymeric material transparent to energy of a predetermined type and having a predetermined melting temperature, placing a fabric of polymeric fibers having a melting temperature higher than the melting temperature of the matrix in the matrix, applying a pressure of 1000 to 6000 psi to the fabric disposed in the matrix, then raising the temperature to the melting temperature of the fabric for the minimum time required to cause consolidation of the fabric and the matrix and rapidly cooling the consolidated fabric and matrix to a temperature below the melting temperature of the fabric. In accordance with a second embodiment there is provided a fabric of polymeric fibers as in the first embodiment which is operated upon as in the first embodiment to cause melting of a sufficient portion of the fabric to fill the interstices between the fibers of the fabric and the fabric is then rapidly cooled to a temperature below the melting temperature of the fabric.
摘要翻译：一种保护性，耐冲击的材料和方法，该材料包括具有至少0.4GPa的强度和至少5GPa的弹性模量的热塑性聚合物纤维的织物和设置在纤维之间的间隙中的聚合物材料的基体，基体的弹性模量在0.2至3×10 6 psi的范围内。聚合物纤维可以是聚乙烯，聚丙烯，尼龙，聚乙烯醇和聚对苯二甲酸乙二醇酯。在第二实施例中，矩阵是从织物得到的。制造材料的方法包括提供对预定类型的能量透明并具有预定熔融温度的熔融聚合物材料的基体，将具有高于基体的熔融温度的熔解温度的聚合物纤维的织物放置在基质中，对布置在基质中的织物施加1000至6000psi的压力，然后将织物和基体固结所需的最短时间提高到织物的熔融温度，并将固结的织物和基体快速冷却至温度低于织物的熔化温度。根据第二实施例，提供如第一实施例中的聚合物纤维的织物，其如第一实施例中那样被操作以使足够部分的织物熔化以填充织物的纤维之间的间隙和然后将织物快速冷却至低于织物熔融温度的温度。

5. 发明授权

US5573824A High strength, high modulus continuous polymeric material for durable, impact resistant applications 失效
标题翻译：高强度，高模量连续聚合物材料，适用于耐用，耐冲击的应用
公开(公告)号：US5573824A
公开(公告)日：1996-11-12
申请号：US241218
申请日：1994-05-11
申请人： Paul Klocek , William J. MacKnight , Richard J. Farris , Christian Lietzau
发明人： Paul Klocek , William J. MacKnight , Richard J. Farris , Christian Lietzau
IPC分类号： B29C70/22 , B29C70/34 , B29C70/46 , B32B27/02 , B32B27/04 , B32B27/36
CPC分类号： B29C70/22 , B29C70/34 , B29C70/46 , B32B27/02 , B32B27/04 , B29K2995/0026 , B29L2031/3456 , Y10S428/911 , Y10S428/918 , Y10T428/24124 , Y10T428/24132 , Y10T428/24364 , Y10T442/2615
摘要： A protective, impact resistant material and method, the material comprising a fabric of thermoplastic polymeric fibers having a strength of at least 0.5 GPa and an elastic modulus of at least 25 GPa and a matrix of polymeric material disposed in the interstices between the fibers, the matrix having an elastic modulus in the range 0.2 to 3.times.10.sup.6 psi. The polymeric fibers can be gel spun polyethylene, polypropylene, nylon, polyvinyl alcohol and polyethylene terephthalate. In a second embodiment, the matrix is derived from the fabric. The method of making the material comprises providing a matrix of melted polymeric material transparent to energy of a predetermined type and having a predetermined melting temperature, placing a fabric of polymeric fibers having a melting temperature higher than the melting temperature of the matrix in the matrix, applying a pressure of 1000 to 2000 psi to the fabric disposed in the matrix, then raising the temperature to the melting temperature of the fabric for the minimum time required to cause consolidation of the fabric and the matrix and rapidly cooling the consolidated fabric and matrix to a temperature below the melting temperature of the fabric. In accordance with a second embodiment there is provided a fabric of polymeric fibers as in the first embodiment which is operated upon as in the first embodiment to cause melting of a sufficient portion of the fabric to fill the interstices between the fibers of the fabric and the fabric is then rapidly cooled to a temperature below the melting temperature of the fabric.
摘要翻译：一种保护性，耐冲击的材料和方法，该材料包括具有至少0.5GPa的强度和至少25GPa的弹性模量的热塑性聚合物纤维的织物和布置在纤维之间的间隙中的聚合物材料的基体，基体的弹性模量在0.2至3×10 6 psi的范围内。聚合物纤维可以是聚乙烯，聚丙烯，尼龙，聚乙烯醇和聚对苯二甲酸乙二醇酯。在第二实施例中，矩阵是从织物得到的。制造材料的方法包括提供对预定类型的能量透明并具有预定熔融温度的熔融聚合物材料的基体，将具有高于基体的熔融温度的熔解温度的聚合物纤维的织物放置在基质中，对布置在基质中的织物施加1000至2000psi的压力，然后将织物和基体固结所需的最短时间提高到织物的熔融温度，并将固结的织物和基体快速冷却至温度低于织物的熔化温度。根据第二实施例，提供如第一实施例中的聚合物纤维的织物，其如第一实施例中那样被操作以使足够部分的织物熔化以填充织物的纤维之间的间隙和然后将织物快速冷却至低于织物熔融温度的温度。

6. 发明授权

US07354990B2 Purified polymeric materials and methods of purifying polymeric materials 有权
公开(公告)号：US07354990B2
公开(公告)日：2008-04-08
申请号：US11183714
申请日：2005-07-18
申请人： Robert John Hossan , Christian Lietzau , Matthew Frank Niemeyer , Mukund Parthasarathy
发明人： Robert John Hossan , Christian Lietzau , Matthew Frank Niemeyer , Mukund Parthasarathy
IPC分类号： C08F6/00
CPC分类号： C08G65/46 , C08L25/00 , C08L25/06 , C08L71/10 , C08L71/12 , G11B7/2536 , Y10T428/2982 , C08L2666/14 , C08L2666/04
摘要： A method is disclosed to purify a polymeric material by filtering a melt comprising poly(arylene ether) and poly(alkenyl aromatic) through a melt filtration system. The method provides a filtered polymeric composition having reduced levels of particulate impurities. The filtered polymeric composition prepared is suitable for use in data storage media applications.

7. 发明申请

US20050250932A1 Purified polymeric materials and methods of purifying polymeric materials 有权
公开(公告)号：US20050250932A1
公开(公告)日：2005-11-10
申请号：US11183714
申请日：2005-07-18
申请人： Robert Hossan , Christian Lietzau , Matthew Niemeyer , Mukund Parthasarathy
发明人： Robert Hossan , Christian Lietzau , Matthew Niemeyer , Mukund Parthasarathy
IPC分类号： B29D17/00 , B29K71/00 , C08L25/06 , C08L71/00 , C11D17/00 , D01D1/10
CPC分类号： C08G65/46 , C08L25/00 , C08L25/06 , C08L71/10 , C08L71/12 , G11B7/2536 , Y10T428/2982 , C08L2666/14 , C08L2666/04
摘要： A method is disclosed to purify a polymeric material by filtering a melt comprising poly(arylene ether) and poly(alkenyl aromatic) through a melt filtration system. The method provides a filtered polymeric composition having reduced levels of particulate impurities. The filtered polymeric composition prepared is suitable for use in data storage media applications.

8. 发明申请

US20050064129A1 Purified polymeric materials and methods of purifying polymeric materials 有权
标题翻译：纯化聚合物材料和纯化聚合物材料的方法
公开(公告)号：US20050064129A1
公开(公告)日：2005-03-24
申请号：US10922194
申请日：2004-08-19
申请人： Jiawen Dong , Hua Guo , Robert Hossan , Christian Lietzau , Vijay Mhetar
发明人： Jiawen Dong , Hua Guo , Robert Hossan , Christian Lietzau , Vijay Mhetar
IPC分类号： B29C47/38 , B29C47/60 , B29C47/68 , B29D17/00 , B29K71/00 , B32B3/02 , C08G65/46 , C08L25/02 , C08L25/06 , C08L71/00 , C08L71/10 , C08L71/12 , C11D17/00 , D01D1/10
CPC分类号： C08L71/10 , C08G65/46 , C08L25/02 , C08L25/04 , C08L71/12 , G11B7/2536 , Y10T428/2982 , C08L2666/18 , C08L2666/04
摘要： A method is disclosed to purify a polymeric material by filtering a melt comprising poly(arylene ether) and poly(alkenyl aromatic) through a melt filtration system. The method provides a filtered polymeric composition having reduced levels of particulate impurities. The filtered polymeric composition prepared is suitable for use in data storage media applications.
摘要翻译：公开了一种通过熔融过滤系统过滤包含聚（亚芳基醚）和聚（链烯基芳族化合物）的熔体来纯化聚合物材料的方法。该方法提供具有降低的颗粒杂质含量的过滤的聚合物组合物。所制备的经过滤的聚合物组合物适用于数据存储介质应用。

9. 发明授权

US08791181B2 Reinforced poly(phenylene ether)-polysiloxane block copolymer composition, and article comprising same 有权
标题翻译：增强聚（亚苯基醚） - 聚硅氧烷嵌段共聚物组合物及其制品
公开(公告)号：US08791181B2
公开(公告)日：2014-07-29
申请号：US13781792
申请日：2013-03-01
申请人： Christian Lietzau , Sho Sato
发明人： Christian Lietzau , Sho Sato
IPC分类号： C08K5/523
CPC分类号： C08K5/52 , C08G77/46 , C08K3/013 , C08K3/04 , C08K3/22 , C08K3/30 , C08K3/32 , C08K3/34 , C08K3/346 , C08K3/40 , C08K5/521 , C08K5/523 , C08K5/5399 , C08K7/14 , C08K7/20 , C08K7/28 , C08K2003/222 , C08K2003/3036 , C08L71/12 , C08L83/12 , C08K3/0033 , C08L85/02 , C08K5/524 , C08L53/025 , C08L23/06
摘要： A reinforced poly(phenylene ether)-polysiloxane block copolymer composition includes specific amounts of a poly(phenylene ether)-polysiloxane block copolymer reaction product, a flame retardant, and a reinforcing filler. The composition exhibits a desirable balance of flame retardancy, heat resistance, and stiffness relative to a corresponding poly(phenylene ether) composition, and it is useful to fabricate articles including fuser holders for electrophotographic copiers.
摘要翻译：增强的聚（苯醚） - 聚硅氧烷嵌段共聚物组合物包括特定量的聚（亚苯基醚） - 聚硅氧烷嵌段共聚物反应产物，阻燃剂和增强填料。组合物相对于相应的聚（苯醚）组合物显示出阻燃性，耐热性和刚度的理想平衡，并且可用于制造包括用于电子照相复印机的定影器保持器的制品。

10. 发明申请

US20100179290A1 POLY(ARYLENE ETHER) ARTICLES AND COMPOSITIONS 有权
标题翻译： POLY（ARYLENE ETHER）文章和组成
公开(公告)号：US20100179290A1
公开(公告)日：2010-07-15
申请号：US12353995
申请日：2009-01-15
申请人： Christian Lietzau , Vijay R. Mhetar , Abhijit Namjoshi , Geuch Zijlma
发明人： Christian Lietzau , Vijay R. Mhetar , Abhijit Namjoshi , Geuch Zijlma
IPC分类号： C08L53/00
CPC分类号： C08L71/12 , C08L23/0815 , C08L25/06 , C08L53/02 , C08L67/04 , F24S10/502 , F24S10/73 , Y02E10/44 , C08L2666/02 , C08L53/025
摘要： A profile extruded article includes a composition that is formed by melt-kneading particular amounts of a poly(arylene ether), a polystyrene-poly(ethylene-butylene)-polystyrene triblock copolymer, a homopolystyrene, and a polysalicylate. The article is particularly useful in the fabrication of solar collectors for low cost solar energy systems.
摘要翻译：型材挤出制品包括通过熔融捏合特定量的聚（亚芳基醚），聚苯乙烯 - 聚（乙烯 - 丁烯） - 聚苯乙烯三嵌段共聚物，均聚苯乙烯和聚水杨酸酯而形成的组合物。该文章在制造用于低成本太阳能系统的太阳能收集器方面特别有用。

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