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1. 发明授权

US07186765B2 Method for preparation of stable bitumen polymer compositions 失效
标题翻译：稳定沥青聚合物组合物的制备方法
公开(公告)号：US07186765B2
公开(公告)日：2007-03-06
申请号：US10888563
申请日：2004-07-09
申请人： James R. Butler , Kevin P. Kelly , Paul Buras
发明人： James R. Butler , Kevin P. Kelly , Paul Buras
IPC分类号： C08L95/00
CPC分类号： C08L95/00 , C08L2666/02 , C08L25/00 , C08L33/00 , C08L2666/04 , C08L53/00 , C08L2666/08
摘要： The present invention provides a method for preparing an asphalt and thermoplastic elastomer composition. The process comprises heating an asphalt cut in a stirred tank to a temperature sufficient to allow the stirring of the asphalt in the tank. A thermoplastic elastomer or rubber is added to the asphalt while continuing to stir the asphalt. The mixture is stirred at a speed and for a period of time sufficient to increase the distribution of the elastomer into the asphalt. The stirring speed is reduced and the temperature is increased to add crosslinking agents to the tank. Stirring is continued for a period of time sufficient to improve the distribution of the crosslinking agent dispersion in the asphalt. Crosslinking agents include compositions of mercaptobenzothiazole, zinc oxide and elemental sulfur; compositions of mercaptobenzothiazole, zinc oxide, and mixed polythiomorpholine; and compositions of zinc 2-mercaptobenzothiazole and dithiodimorpholine.
摘要翻译：本发明提供一种制备沥青和热塑性弹性体组合物的方法。该方法包括将在搅拌槽中切割的沥青加热到足以允许在罐中搅拌沥青的温度。在沥青中继续搅拌沥青时，加入热塑性弹性体或橡胶。将混合物以足以增加弹性体分配到沥青中的速度搅拌一段时间。搅拌速度降低，温度升高，向罐中加入交联剂。搅拌持续一段时间，足以改善沥青中交联剂分散体的分布。交联剂包括巯基苯并噻唑，氧化锌和元素硫的组合物; 巯基苯并噻唑，氧化锌和混合多硫代吗啉的组成; 和2-巯基苯并噻唑锌和二硫代二吗啉的组合物。

2. 发明授权

US06927245B2 Dispersing agent and method for the delivery of cross-linking agent to polymer modified asphalt compositions 失效
标题翻译：用于将交联剂递送到聚合物改性沥青组合物的分散剂和方法
公开(公告)号：US06927245B2
公开(公告)日：2005-08-09
申请号：US10454001
申请日：2003-06-04
申请人： Paul Buras , James R. Butler
发明人： Paul Buras , James R. Butler
IPC分类号： C08J3/00 , C08L95/00
CPC分类号： B01F17/0064 , C08L95/00 , C08L2666/02
摘要： The present invention provides a dispersing agent that facilitates the delivery of a cross-linking agent to polymer modified asphalt. The present invention further includes a composition comprising a liquid hydrocarbon, the dispersant and cross-linking agent, and methods of preparing the composition and of preparing cross-linked polymer modified asphalt composition.
摘要翻译：本发明提供一种促进交联剂向聚合物改性沥青输送的分散剂。本发明还包括包含液体烃，分散剂和交联剂的组合物，以及制备该组合物和制备交联聚合物改性沥青组合物的方法。

3. 发明授权

US06767939B2 Method for preparation of stable bitumen polymer compositions 失效
标题翻译：稳定沥青聚合物组合物的制备方法
公开(公告)号：US06767939B2
公开(公告)日：2004-07-27
申请号：US10140317
申请日：2002-05-07
申请人： James R. Butler , Kevin P. Kelly , Paul Buras
发明人： James R. Butler , Kevin P. Kelly , Paul Buras
IPC分类号： C08L9500
CPC分类号： C08L95/00 , C08L2666/02 , C08L25/00 , C08L33/00 , C08L2666/04 , C08L53/00 , C08L2666/08
摘要： The present invention provides a method for preparing an asphalt and thermoplastic elastomer composition. The process comprises heating an asphalt cut in a stirred tank to a temperature sufficient to allow the stirring of the asphalt in the tank. A thermoplastic elastomer or rubber is added to the asphalt while continuing to stir the asphalt. The mixture is stirred at a speed and for a period of time sufficient to increase the distribution of the elastomer into the asphalt. The stirring speed is reduced and the temperature is increased to add crosslinking agents to the tank. Stirring is continued for a period of time sufficient to improve the distribution of the crosslinking agent dispersion in the asphalt. Crosslinking agents include compositions of mercaptobenzothiazole, zinc oxide and elemental sulfur; compositions of mercaptobenzothiazole, zinc oxide, and mixed polythiomorpholine; and compositions of zinc 2-mercaptobenzothiazole and dithiodimorpholine.
摘要翻译：本发明提供一种制备沥青和热塑性弹性体组合物的方法。该方法包括将在搅拌槽中切割的沥青加热到足以允许在罐中搅拌沥青的温度。在沥青中继续搅拌沥青时，加入热塑性弹性体或橡胶。将混合物以足以增加弹性体分配到沥青中的速度搅拌一段时间。搅拌速度降低，温度升高，向罐中加入交联剂。搅拌持续一段时间，足以改善沥青中交联剂分散体的分布。交联剂包括巯基苯并噻唑，氧化锌和元素硫的组合物; 巯基苯并噻唑，氧化锌和混合多硫代吗啉的组成; 和2-巯基苯并噻唑锌和二硫代二吗啉的组合物。

4. 发明授权

US07384468B2 Asphalt/aggregate composition of enhanced adhesion 失效
标题翻译：沥青/骨料组合增强附着力
公开(公告)号：US07384468B2
公开(公告)日：2008-06-10
申请号：US11010612
申请日：2004-12-13
申请人： James R. Butler , William Lee , Paul Buras
发明人： James R. Butler , William Lee , Paul Buras
IPC分类号： C08L95/00 , C09D195/00
CPC分类号： C08L95/00 , C08L2666/74
摘要： An asphalt/aggregate composition having enhanced adhesion characteristics and its preparation. An asphalt base material is heated to a molten state in order to permit mixing of the asphalt with added components. A heavy metal soap is incorporated into the asphalt base material to enhance the adhesion of the asphalt base material with an aggregate component which is mixed with the asphalt base material to provide an asphalt/aggregate blend. The asphalt and aggregate can be blended together in a mixing chamber to provide a fluid asphalt/aggregate concrete which is then dispensed on a substrate surface or the asphalt base material and aggregate components can be separately applied to the substrate surface to provide the ultimate asphalt/aggregate concrete. The heavy metal soap is a C14-C18 heavy metal soap such as zinc stearate. Zinc oxide may also be added to the asphalt base material in an amount which is less than the amount of zinc stearate. The asphalt base material may be polymer-modified asphalt and may incorporate a crumb rubber component to provide a rubber-modified asphalt.
摘要翻译：具有增强的粘合特性及其制备的沥青/骨料组合物。将沥青基材料加热至熔融状态，以使沥青与添加的组分混合。沥青基材中加入重金属皂以增强沥青基材与沥青基料混合的聚集体组分的粘附性，从而提供沥青/骨料混合物。沥青和骨料可以在混合室中混合在一起，以提供流体沥青/骨料混凝土，然后将其分配到基材表面上，或者将沥青基体材料和骨料组分分别施加到基材表面以提供最终的沥青/ 骨料混凝土重金属皂是C 14-14 -C 18重金属皂，例如硬脂酸锌。也可以将氧化锌以少于硬脂酸锌的量添加到沥青基材中。沥青基材料可以是聚合物改性沥青，并且可以加入碎屑橡胶组分以提供橡胶改性沥青。

5. 发明授权

US06441065B1 Method for preparation of stable bitumen polymer compositions 失效
标题翻译：稳定沥青聚合物组合物的制备方法
公开(公告)号：US06441065B1
公开(公告)日：2002-08-27
申请号：US09712672
申请日：2000-11-14
申请人： Cyril Chevillard , Paul Buras , Kevin P. Kelly , James R. Butler
发明人： Cyril Chevillard , Paul Buras , Kevin P. Kelly , James R. Butler
IPC分类号： C08L9500
CPC分类号： C08L95/00 , C08L2666/04 , C08L53/00
摘要： The present invention provides a method for preparing an asphalt and thermoplastic elastomer composition. The process comprises preparing a crosslinking elastomer concentrate that is added to a heated asphalt cut in a stirred tank and then aged to improve SHRP high temperature grading. The crosslinking elastomer concentrate is prepared by adding thermoplastic elastomer and crosslinking agents to a suitable carrier oil, preferably an aromatic oil such as Hydrolene H series. This concentrate is maintained at a temperature that promotes association between the crosslinking agents and the elastomer for a time sufficient for association to substantially complete. In one embodiment, the associating time is in excess of 2 hours up to 24 hours. The asphalt is heated to a temperature sufficient to allow the stirring of the asphalt in the tank. The crosslinking thermoplastic elastomer concentrate is added to the asphalt while continuing to stir the asphalt. The mixture is stirred at a speed and for a period of time sufficient to increase the distribution of the elastomer into the asphalt. Stirring is continued for a period of time sufficient to improve the distribution of the crosslinking thermoplastic elastomer in the asphalt. The composition is then aged as a liquid for 12 to 48 hours to increase the SHRP high temperature grade.
摘要翻译：本发明提供一种制备沥青和热塑性弹性体组合物的方法。该方法包括制备交联弹性体浓缩物，其加入到在搅拌槽中切割的加热沥青中，然后老化以改善SHRP高温分级。交联弹性体浓缩物通过将热塑性弹性体和交联剂加入到合适的载体油，优选芳香油如氢化氢H系列中来制备。该浓缩物保持在促进交联剂和弹性体之间缔合的温度足以与基本上完全结合的时间。在一个实施方案中，缔合时间超过2小时至24小时。将沥青加热到足以允许在罐中搅拌沥青的温度。将交联热塑性弹性体浓缩物加入到沥青中，同时继续搅拌沥青。将混合物以足以增加弹性体分配到沥青中的速度搅拌一段时间。继续搅拌足以改善交联热塑性弹性体在沥青中的分布的时间。然后将组合物作为液体陈化12至48小时以增加SHRP高温等级。

6. 发明授权

US08802911B2 Process for ethylbenzene production 有权
公开(公告)号：US08802911B2
公开(公告)日：2014-08-12
申请号：US13868505
申请日：2013-04-23
申请人： James R. Butler
发明人： James R. Butler
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C2529/70 , Y02P20/584 , C07C15/073
摘要： A method of producing an alkylaromatic by the alkylation of an aromatic with an alkylating agent, such as producing ethylbenzene by an alkylation reaction of benzene, is disclosed. The method includes using an H-beta catalyst to minimize process upsets due to alkylation catalyst deactivation and the resulting catalyst regeneration or replacement. The H-beta catalyst can be used in a preliminary alkylation reactor that is located upstream of the primary alkylation reactor. The H-beta catalyst used in a preliminary alkylation reactor can reduce the deactivation of the catalyst in the primary alkylation reactor.

7. 发明授权

US08785705B2 Use of a co-feed in the coupling of toluene with a carbon source 有权
标题翻译：在甲苯与碳源的偶联中使用共同进料
公开(公告)号：US08785705B2
公开(公告)日：2014-07-22
申请号：US13457500
申请日：2012-04-27
申请人： Sivadinarayana Chinta , Joseph L. Thorman , James R. Butler
发明人： Sivadinarayana Chinta , Joseph L. Thorman , James R. Butler
IPC分类号： C07C15/46 , C07C15/073
CPC分类号： C07C2/862 , C07C2/864 , C07C2521/02 , C07C2529/06 , C07C2529/08 , C07C15/073 , C07C15/46
摘要： A process for making styrene is disclosed that includes providing toluene, a co-feed, and a C1 source to a reactor containing a catalyst, reacting toluene with the C1 source in the presence of the catalyst and the co-feed to form a product stream containing ethylbenzene and styrene. The co-feed can be selected from the group of water, carbon monoxide, hydrogen, and combinations thereof.
摘要翻译：公开了一种制备苯乙烯的方法，其包括向含有催化剂的反应器提供甲苯，共进料和C1源，在催化剂和共进料存在下使甲苯与C1源反应以形成产物流含乙苯和苯乙烯。共进料可以选自水，一氧化碳，氢气及其组合。

8. 发明授权

US08742190B2 Dilute ethylene alkylation of benzene 有权
标题翻译：苯稀释乙烯烷基化
公开(公告)号：US08742190B2
公开(公告)日：2014-06-03
申请号：US13178091
申请日：2011-07-07
申请人： James R. Butler
发明人： James R. Butler
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C2523/10 , C07C2529/06 , C07C2529/08 , C07C2529/70 , C07C15/073
摘要： Methods of forming ethylbenzene are described herein. In one embodiment, the method includes contacting dilute ethylene with benzene in the presence of an alkylation catalyst to form ethylbenzene, wherein such contact occurs in a reaction zone containing a gaseous phase and recovering ethylbenzene from the reaction zone.
摘要翻译：本文描述了形成乙苯的方法。在一个实施方案中，该方法包括在烷基化催化剂存在下使稀乙烯与苯接触以形成乙苯，其中这种接触在含有气相的反应区中发生并从反应区回收乙苯。

9. 发明授权

US08734737B2 Production of EB from toluene and methane 有权
标题翻译：从甲苯和甲烷生产EB
公开(公告)号：US08734737B2
公开(公告)日：2014-05-27
申请号：US13604760
申请日：2012-09-06
申请人： James R. Butler , Joseph E. Pelati
发明人： James R. Butler , Joseph E. Pelati
IPC分类号： B01J8/04
CPC分类号： C07C15/46 , C07C2/66 , C07C2/84 , C07C5/48 , Y10S585/921 , Y10S585/943 , C07C15/073
摘要： A process for making ethylbenzene and/or styrene by reacting toluene with methane is disclosed. In one embodiment the process can include reacting toluene with methane to form a product stream comprising ethylbenzene and further processing the ethylbenzene to form styrene in an existing styrene production facility.
摘要翻译：公开了通过使甲苯与甲烷反应制备乙苯和/或苯乙烯的方法。在一个实施方案中，该方法可以包括使甲苯与甲烷反应以形成包含乙苯的产物流，并进一步处理乙苯以在现有的苯乙烯生产设备中形成苯乙烯。

10. 发明授权

US08710286B2 Oxidative coupling of hydrocarbons as heat source 有权
标题翻译：碳氢化合物作为热源的氧化偶联
公开(公告)号：US08710286B2
公开(公告)日：2014-04-29
申请号：US12416074
申请日：2009-03-31
申请人： James R. Butler
发明人： James R. Butler
IPC分类号： C07C2/78
CPC分类号： C07C4/025 , C07C2/82 , C07C5/327 , C07C11/04 , C07C15/46
摘要： A process for the coupling of hydrocarbons and utilizing the heat energy produced by the reaction is disclosed. In one embodiment the process can include reacting methane with oxygen to form a product stream containing ethane and further processing the ethane to ethylene in an existing ethylene production facility while using the heat energy produced by the reaction within the facility.
摘要翻译：公开了一种用于偶联烃并利用由反应产生的热能的方法。在一个实施方案中，该方法可以包括使甲烷与氧反应形成含有乙烷的产物流，并且在现有乙烯生产设备中进一步处理乙烯至乙烯，同时使用由设备内的反应产生的热能。

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